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Methods: Lecithin and the sucrose ester-phospholipids liposome were prepared using the ethyl ether injection method by mixing sucrose ester with lecithin, sphingomyelin and cholesterol according to different lipids ratio.

按不同比例将乙酸异丁酸蔗糖酯与卵磷脂、鞘磷脂和胆固醇混合,溶于乙醚中,然后注入pH7.2的PBS缓冲液中,制成卵磷脂脂质体及蔗糖酯-卵磷脂脂质体。

The preparation of 2,2-dimethyl-3-hydroxy propanal from the condensation of formaldehyde and i-butyraldehyde by using triethylamine as catalyst was studied.

异丁醛和甲醛为原料,三乙胺为催化剂,羟醛缩合法合成了2,2-二甲基-3-羟基丙醛。

D. of the catalyst increased, i. e. the acid volume of the catalyst increased, the conversion for isobutene and the selectivity for trimer increased also, while the selectivity for dimer decreased, and the selectivity for tetramer was almost unchanged.

D。增加时,即催化剂的酸量增加时,异丁烯的转化率和三聚物的选择性也增加,但二聚物的选择性降低,四聚物的选择性则几乎没有变化。

The catalytic system composed of NHPI and transition metal ion can catalyze effectively ethane into acetic acid,cyclane into dicarboxylic acid,toluene into benzoic acid,alkene into epoxide,alkyne into acetylenic ketone,and amide into imide;NHPI used alone can catalyze adamantane to be carbonylated,hydrogen peroxide prepared by oxidization alcohol;NHPI combined with as...

NHPI与过渡金属离子组成的催化体系能高效地催化乙烷氧化为乙酸、环烷烃氧化为二元羧酸、甲苯氧化为苯甲酸、烯烃氧化为环氧化物、炔烃氧化为炔酮、酰胺氧化为酰亚胺;NHPI单独使用能催化金刚烷发生氧化羰基化反应、催化氧化醇制取过氧化氢;NHPI与有机助催化剂如偶氮二异丁腈、溴化季铵盐、蒽醌和醇等也能催化分子氧氧化反应。

No Cl2 was used in this process therefore the synthesis was environment benign and the content of chlorine was lower than 30×10-6.The effects of the compositions,temperature,avera...

实验考察了配料比、温度、聚异丁烯相对分子质量以及反应时间对产物性能的影响,确定了最佳工艺条件。

The factors which affect the average molecular weight of the polymer of AM and DMDAAC were investigated. The optimal reaction conditions are as follows: the concentration of monomer AM was 30%, while DMDAAC was 5%; the reaction temperature was 30℃, the amount of initiators at the low temperature stage was 0.05‰(compared to the weight of the monomers joining the polymerization), while V-50 was 0.025‰, the weight ratio of potassium persulphate to sodium bisulphite is 1:1, the amount of carbamide was 40‰, and complexing agent was 0.05‰, besides, aerate nitrogen gas for 8min, then the high molecular weight polymer (M=1.217×10^7) could be got after 16h reaction.

研究了影响AM与DMDAAC共聚物的平均分子量的因素,得到了优化条件为:单体浓度为30%,DMDAAC与AM摩尔比为5:95,聚合温度为30℃,低温段引发剂用量为0.05‰,K2S2O8与NaHSO3质量比为1:1,偶氮二异丁基脒盐酸盐(V-50)用量为0.025‰,尿素用量为40‰,乙二胺四乙酸二钠(EDTA-2Na)用量为0.05‰,在此优化条件下聚合反应16h后得到分子量为1.217×10^7的阳离子型聚丙烯酰胺。

Because glial cell activation could also be involved in the development of opioid tolerance in rats, the authors studied the antinociceptive effects of ibudilast and morphine in different models of coadministration.

由于大鼠神经胶质细胞的激活也被证实与阿片样物质耐受性的产生有关,作者研究了异丁司特和吗啡在不同的共同给药模型中的镇痛作用。

Coadministration of ibudilast with morphine did not attenuate the development of morphine tolerance.

同时给予异丁司特和吗啡并不能减弱吗啡耐受性的产生。

It is an extraction and separation system of potential industrial applications.This dissertation studies on the liquid-liquid equilibrium of water/ ethanol/ isobutanol system in detail, and investigated the partition coefficients for dipotassium glycyrrhizinat in the system.

本文对由水+乙醇+异丁醇组成的水+混合溶剂萃取体系的液液相平衡关系做了较为详细的研究,并探讨了该体系对甘草酸二钾的萃取分配规律。

The temperature affects partition of dipotassium glycyrrhizinat but the effect is minor. On the same time pH has major impact on the partition of dipotassium glycyrrhizinat. The coefficient is eight times higher when pH reaches 2. The improved Diamond-Hsu model can be used to correlate the partition coefficient of dipotassium glycyrrhizinat in the system of water/ethanol/isobutanol. The result of Infrared and TG analysis indicate the extraction product has the same characteristic features with dipotassium glycyrrhizinat.

结果表明:体系的初始点越靠近临界点,甘草酸二钾的分配系数越大;温度对甘草酸二钾的分配有~定的影响,但分配系数随温度变化不大;pH值对甘草酸二钾的分配有较大的影响,在pH=2附近,分配系数高出其他位置达8倍;改进的Diamond-Hsu模型可以用于关联甘草酸二钾在水+乙醇+异丁醇体系中的分配系数;红外和TG分析结果表明萃取产物与甘草酸二钾样品的性质特征相同。

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