并四苯

In this paper the optimal conditions for sublimate crystallization refining of pyromellitic dianhydridewas studied,and on the basis of PMDA equilibrium vapor pressure under the contant temperature,the mathematical correlation for sublimate crystallization conditions was deduced.

研究了均苯四酸二酐凝华结晶精制的最佳条件，并以均酐在定温下的平衡蒸汽压为基础，推导出凝华结晶条件数学关系式。

The catalytic activity for the hydrogenation of tetralin was examined with a fixed-bed continuous-flow reactor operating at 4.0MPa. The sulfur tolerance was tested with a feed of 200μg/g sulfur in the form of 4, 6-dimethyldibenzothiophene.

以四氢萘加氢为探针反应，4，6-二甲基二苯并噻吩为硫源，在固定床反应器中考察了催化剂的活性和耐硫性。

First, the geometry optimization for 1-phenyldibenzophosphole and triphenylphosphine were carried out using quantum chemical AM1 method.

用量子化学AM1方法优化了1-苯基二苯并膦和三苯基膦的几何构型，比较了两种化合物的电子结构和空间结构，发现PDBP作为羰基合成铑膦催化剂的配体要优于三苯基膦；系统研究了PDBP的合成方法，其最佳合成条件为：在无水无氧的条件下，采用二乙胺锂与溴化四苯基膦摩尔比为3，反应温度为22 ℃，反应5 h，反应后酸化， pH值为1～2，产物收率可达到85％～88％。

Unoxidated and oxidized wheat stalks were extracted sequentially with CS2, benzene, methanol, acetone and THF, and the extraction solutions were analyzed with GC/MS. The relative contents and compositions of fractional extracts of un-oxidized and oxidized wheat stalks were compared.

采用二硫化碳、苯、甲醇、丙酮和四氢呋喃对未氧化和氧化的麦秆进行分级萃取，比较麦秆各级萃取物的相对含量和组成差异，并对各级萃取物的组成进行GC/MS分析。

C NMR, IR, GC MS and TG combined with some techniques including solvent extraction method, TPO and structure characterization were applied to determine the components of the deposit on the coked β zeolite catalyst after reaction for 8?000 h in pilot plant scale. It was shown that the composition of the deposit ...

用13CNMR ，IR ，GC MS ，TG等手段，并结合溶剂萃取法、TPO和结构分析等方法，确定了改性β沸石催化剂上沉积物的主要成分是多异丙基苯和四氢化萘，且主要分布在沸石孔道内；同时，快速升温后恒温烧炭的效果优于慢速升温后恒温烧炭的效果

On this basis, chosing 15w germicidal lamp with radiation centred at 253. 7nm or 15w blacklight fluorescent lamp with radiation centred at 365nm as the light source respectively, the destruction effects of trace impurities in water by photocatalytic oxidation method using TiO〓 as an immobile phase have been investigated, and the effects are contrasted with photolysis. The investigation is mounted into Phenol aqueous solution, Hydroquinone and Humic Acid aqueous solutions、three representative halohydrocarbons coexisting in main water、the comprehensive index removal of varied trace organic pollutants in main water、the removal of residual chlorine and the disinfecting action, etc..

在此基础上，选择主波长253.7nm的紫外线杀茵灯或主波长365nm的蓝黑管紫外线荧光灯作为光源，研究了TiO〓膜固定相光催化氧化法去除水中微污染物的效果，包括苯酚水溶液、对苯二酚水溶液和腐植酸水溶液的光催化氧化以及自来水中共存的三种典型的氯代烃水溶液三氯甲烷、四氯化碳和四氯乙烯的混合光催化氧化、自来水中有机物总体去除效果以及光催化去除自来水中余氯的作用和光催化的消毒作用等，并进行了光解对比实验。

This paper studied four pretreatment methods by adding three different retention time organochlorine pesticides(α-BHC、Dieldrin、pp′-DDT) to fish sample and making different concentration(0.01、0.1、1),then using GC-ECD determinate its recoveries.

研究了用气相色谱——电子捕俘器法测定鱼肉中有机氯农药的四种不同前处理方法。通过向鱼样中加入三种不同保留时间的有机氯农药(α—六氯苯、狄氏剂、滴滴涕)，并测定三种不同浓度(0.01、0.1、1)时加标回收率。

The results indicated that the total hydrodesulfurization ratio of sulfur-containing compounds of FCC gasoline was 86.3%, sulfide and tetrahydrothiophene were completely conversed, the hydrodesulfurization ratio of mercaptans was 96.6%, the hydrodesulfurization ratio of thiophene was 78.8%, the hydrodesulfurization ratio of alkyl-substituted thiophene was 85.8%, the hydrodesulfurization ratio of benzothiophene was 81.4% The conversed products of 3-methylthiophene were including little sulfur specie, isomerized sulfur specie (2-methylthiophene) and larger sulfur specie (2, 5-dimethylthiophene, 2,4-dimethylthiophene, 2,3-dimethylthiophene).

结果表明FCC汽油硫化物总脱硫率为86.3%，其中，硫醚和四氢噻吩的转化率都达到100%，硫醇硫转化率96.6%，噻吩硫转化率78.8%，烷基噻吩转化率85.8%，苯并噻吩转化率81.4%。3-甲基噻吩在OTA催化剂上的转化产物中含有小分子，异构硫化物（2-甲基噻吩），以及大分子异构硫化物（如2，5-二甲基噻吩、2，4-二甲基噻吩和2，3-二甲基噻吩）。

Chapter 2: Four kinds of condensations of aromatic amine with benzaldehyde derivatives were obtained by solid phase synthesis. Their structures were identified by element analysis and 1H NMR spectroscopy. Their SHG properties, fluorescent and thermochromic properties were also tested.

第二章：通过室温固相反应合成了四类苯甲醛缩芳胺希夫碱衍生物，用元素分析和核磁共振对其结构进行了确定，并测试了它们的非线性性质、荧光性质以及热致变色性质。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。