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A ratio spectra derivative spectrophotometry for simultaneous determination of quaternary mixture of aminopyrine, phenobarbital, caffeine and phenacetin was studied.

提出了可应用于四元混合体系同时测定的比光谱-导数分光光度法，阐述了该方法的基本原理，并将其应用于氨基比林、苯巴比妥、咖啡因和非那西丁四元混合体系中各组分的同时测定。

In addition, the stability of ternary Cu 〓complexes polypyridyl=1, 10-phenanthroline (Phen , pyrido [3, 2-f] [1, 7] phenanthroline , 1, 4, 8, 9-tetraazatriphenylene , dipyrido [3, 2-a: 2'3'-c] phenazine , imidazo phenanthroline and 2-phenylimidazo phenanthroline , NTP=ATP and UTP was studied by potentiometric pH titration in water at temperature 15℃, 25℃ and 35℃, and in 30% and 50% aqueous dioxane solution at 25℃.

另外，用pH电位滴定法研究了多吡啶芳香配体polypyridyl配合物Cu〓（PL=1，10-邻菲咯啉、吡啶并[3，2-f][1，7]邻菲咯啉、1，4，8，9-四氮三联苯、二吡啶并[3，2-a∶2'3'-c]吩嗪和2-苯基咪唑并邻菲咯啉或咪唑并邻菲咯啉）在不同温度（15℃、25℃和35℃）水溶液及30%和50%二氧六环-水混和溶剂（25℃）中的稳定性。

An unstable important intermediate ,2- methoxymethyl-hydroquinone which is very easy to oxidize and polymerize, and its precursors were first synthesized, a...

第一、二条合成线路前人未见报导，从中得到了四个苯并呋喃类衍生物，并详细地探索了环化反应的条件。

Four new types of pyrimidine derivatives introduced directly by nitrogen-containing benzoheterocycles were designed and synthesized.

设计并合成了四种苯并含氮杂环取代的嘧啶类新化合物，它们的结构经 MS，IR和1 H NMR分析得到确

There are also two types of IPTligands in crystal 2. With two bidentate carboxylates, one acts as bridging ligandconnecting neighboring 〓 tetrahedral core along c axia to form ladderlike long chain.

且间苯二甲酸根配体可以分为两类：第一类配体中每个羧酸根连接四核锌四面体结构中的四条边并沿c轴方向连接邻近的四面体结构单元形成梯形长链。

Tetrahydroisowuinolin derivatives and phthalide derivatives were designed and synthesized on the basis of a PDE4 inhibitor pharmacophore model set up through computer simulation. Some tetrahydroisowuinolin derivatives synthesized were evaluated on their activity against PDE4 for study on the structure-activity relationship.(7-cyclopentyloxy)-6-methoxy-3,4-dihydroisoquinolin-2(1H)-yl(4-hydroxy-3-methoxyphenyl)methanone (155) and Methyl 7--6-methoxy-2-(4-methoxy- benzoyl)-1-phenyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylate (170) showed good activity against PDE4, which were chosen as the lead compounds to design and synthesize another analogs in order to develop selective PDE4 inhibitors with better activity.

分别设计合成了以四氢异喹啉和氨基苯酞为骨架的两类小分子杂环化合物，并对部分四氢异喹啉衍生物测试了其相关的生物活性，初步确定了其构效关系，发现了两个对PDE4有较好抑制活性的先导化合物(7-cyclopentyloxy)-6-methoxy-3，4-dihydroisoquinolin-2(1H)-yl(4-hydroxy-3-methoxyphenyl)methanone (155)和Methyl 7--6-methoxy-2-(4-methoxy- benzoyl)-1-phenyl-1，2，3，4-tetrahydroisoquinoline-3-carboxylate (170)。

A general novel synthetic method to Symmetrically or unsymmetrically 2,3,6,7- substituted thieno[2,3-d:5,4-d\']dipyrimidine-4,5(3H,6H)-diones and 2-substituted benzothieno[3,2-d] pyrimidin-4(3H)-dione by utilizing aza-Wittig reaction was proposed firstly. This synthetic method has the advantage of easily accessible starting material, mild condition and good yields.

具体研究内容如下：1、首次研究了应用aza-Wittig反应方法合成2，3，6，7-对称与不对称四取代噻吩并[2，3-d；5，4-d\']双嘧啶-4，5(3H，6H)-二酮以及2-取代苯并噻吩并[3，2-d]嘧啶-4(3H)-酮衍生物的通用新方法，该方法原料易得，条件温和，收率较高。

We also summarized some effects which controlled their self-assembly behaviors.In chapter four, a series of PPEs with identical conjugated backbone but different side chains were synthesized and their two-dimensional assembly structure and chain foldings were studied by STM.

主要包括两方面内容：第四章，我们合成了一系列具有相同主链不同侧链的聚苯炔共轭聚合物，并在高定向热解石墨和辛基苯溶液的两相界面，采用STM在分子尺度观察了共轭聚合物链的二维组装结构及其链折叠的情况。

We also summarized some effects which controlled their self-assembly behaviors.In chapter four, a series of PPEs with identical conjugated backbone but different side chains were synthesized and their two-dimensional assembly structure and chain foldings were studied by STM.

主要包括两方面内容：第四章，我们合成了一系列具有相同主链不同侧链的聚苯炔共轭聚合物，并在高定向热解石墨和辛基苯溶液的两相界面，(来源：ABCd7论文94网www.abclunwen.com)采用STM在分子尺度观察了共轭聚合物链的二维组装结构及其链折叠的情况。

This research utilized the method of organic synthesis, researching different amounts and positions of hydroxy-substituted benzoic acid and serotonin into amide reaction, so as to produce a series of polyhydroxy substituted N-benzoylserotonin derivatives (compound 1-10). Accordingly, this study conducts the following four tests. I. The activity of antioxidant and the experiment of ability to scavenge DPPH free radical, II. The ability of overall antioxidant—the activity of TEAC, III. The activity test of inhibit Tyrosinase, and IV. The study of absorbing UV / VIS Spectrophotometers. This study use trolox, arbutin, and octyl salicylate as the control groups, and to test the ability of anti-oxidation, the activity of inhibit Tyrosinase, and the ability of absorbing UV. This research ultimately intends to investigate the applied value of those compounds into cosmetics.

本研究主要利用有机合成的方法，将不同数量及不同位置的羟基取代苯甲酸化合物与色洛冬宁进行醯胺化反应后，得到一系列的多羟基取代之N-色洛冬宁苯甲醯胺衍生物（化合物1 ~ 10），进行四种不同活性测试方法：一、清除DPPH自由基能力抗氧化活性测试；二、总抗氧化能力活性测试；三、抑制酪胺酸酶活性美白测试；四、紫外线／可见光光谱仪吸收测试，并以水溶性维生素E、熊果素、水杨酸辛酯当作对照组，探讨其抗氧化能力、抑制酪胺酸酶的活性能力与吸收紫外线能力，再进一步探讨其应用於化妆品上的价值。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。