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The liquid-liquid equilibrium binodal curves and the tie-line data of an epoxy cotton seed oil/acetic acid/water ternary system.

测定了环氧棉籽油-醋酸-水三元系分别在30℃,40℃,50℃,60℃下的液-液平衡双结点曲线,以及在40℃,50℃,60℃下的液-液平衡系线数据;分别应用物料衡算法和系线中点轨迹法对实验数据进行了检验。

The headspace gas chromatography was used to determin the ethanal content in the production process of bottle grade PET chip.

论述了瓶级聚酯切片生产过程中,采用顶空气相色谱法测试切片中乙醛含量的称样量、样品处理、颗粒度、顶空热平衡时间、热平衡温度、标定及其他顶空测量参数的优化。

These compounds are of substantial interest both inviewpoints of theory and practical applications, mainlyunder the stimulus to achieve synthetic models either foractive sites of iron-sulfur proteins or for transitionmetal catalysts. This thesis describes the synthesis, structures andconformations of 51 new iron-sulfur cluster complexes,which have been characterized by elemental analysis andstandard spectroscopic methods. In addition, single-crystalX-ray diffraction analyses were performed for 4 representa-tive new compounds. Reactivities of μ-〓 with mono- and di- Grig-nard reagents derived intermediates toward various organicelectrophilic substrates were studied, along with complexa-tion of arynyl-containing iron-sulfur clusters by 〓Thus, several bridged, non-bridged, monomeric, dimeric,homonuclear, heteronuclear iron-sullfur and iron-sulfur co-balt-carbon cluster complexes were synthesized. A novelreaction and convenient route for the synthesis in highyield of tetranuclear iron complexes 〓 containing atetracoordinated sulfur atom was discovered, whereas aplausible mechanism based on experimental results was propo-sed for the formation of the new cluster type.

鉴于有机铁硫原子簇化学在基础理论发展和应用方面的重要意义,因此我们开展了这一课题的研究,并取得以下主要成果: 1、本文共合成了51个新有机铁硫及含钴碳簇基的有机铁硫原子簇配合物,除用元素分析,NMR,IR,MS法表征其结构和构象外,还用X-光衍射技术测得四个代表性配合物的单晶结构和构象; 2、我们业已发现炔基Grignard试剂同〓可形成一种&开环&与&闭环&中间物的平衡混合物,研究该平衡混合物同各种亲电试剂的反应; 3、研究发现了一种可高产率地形成〓含〓四配位硫挛合簇的新化学反应并对此反应提出了—种有趣的反应机理; 4、首次由1,4-二溴丁烷双Grignard试剂与〓制得一种新型铁硫簇双硫阴离子活性中间体,并进而研究了它的亲核反应性能; 5、找到了通过〓的光化学反应来合成簇合物〓-〓的一条有实用价值的新路线。

In order to supply basic thermodynamic data for the separation design of acetyl acetone from the isomerization reaction of isopropenyl acetate,vapor-liquid equilibrium data of isopropenyl acetate-acetyl acetone system under 101.3 kPa was measured using Ellis equilibrium still.

为了给乙酸异丙烯酯异构化生产乙酰丙酮工艺的产物分离设计提供基础热力学数据,用埃利斯平衡蒸馏器测定了101.3 kPa下乙酸异丙烯酯-乙酰丙酮体系的汽液平衡数据,结果表明,该二元体系未形成共沸物,实验数据通过了Herrington面积法的热力学一致性检验。

Methods: We use head-space GC method, chromatographic conditions are carried out as following: the flexibility quartzose capillary column, the temperature of column is 90℃, injection temperature is 150℃, equivalence temperature is 80℃ and time is 30 mins, quantization imp temperature is 90℃, transfer line temperature is l00℃.

采用顶空法,在极性弹性石英毛细柱上进行各组分分离,效果良好。柱温:90℃,进样口温度150℃,顶空瓶平衡温度80℃,平衡时间30分钟,定量环温度90℃,传输线温度100℃。

The metastable phase equilibrium of the quaternary system Na(superscript +)∥Cl(superscript -), CO3(superscript 2-), B4O7(superscript 2-)-H2O was studied at 273 K by isothermal evaporation method, the solubility and density of the equilibrium solution of this system were determined and the metastable equilibrium phase diagram was plotted in line with the experimental data. The phase diagram of the system consists of three univariant curves, three crystallization fields and one invariant point.

采用等温蒸发法研究简单四元体系Na∥Cl,CO3(上标 2-),B4O7(上标 2-)-H2O273K时的介稳相平衡,并测定该体系273K平衡液相中各组分的溶解度及密度,该体系的介稳相图和密度组成图显示:该四元体系在273K时的相图由3条溶解度单变量线、3个结晶区及1个共饱和点组成。

Firstly,based on the WR Sexton method,the method and mathematic models of supplementing the sub-idle rotating component characteristics is presented.Secondly,the turbofan windmilling high-low pressure rotor co-working equations and the whole engine co-working equations are established.lastly,a turbofan engine windmilling characteristics under various windmilling conditions are simulated and analyzed.

首先,基于不可压流理论,附以可压缩效应修正的指数法发展了补充慢车转速以下部件特性的计算模型和计算程序;其次,根据流量连续、压力平衡、功率平衡、燃烧室进出口总温相等及转速相等等约束条件建立了风车状态时涡扇发动机高低压转子及整机的共同工作方程;最后发展了具有一定计算精度的涡扇发动机风车状态特性计算模型和程序,并以某型涡扇发动机为例,计算分析了不同飞行条件下发动机的风车特性,从计算结果看,其趋势是合理的。

Voltage of capacitance in this circuit can be resolved厉adding a balance coil.

法。采用平衡绕组可以彻底解决电容电压不平衡。

A comparison of the computation results with traditional results for methane combustion proves that the new method more convenient and efficient.

热力系统平衡态的计算不论是对火焰发展的计算结果还是实验结果都是指示其正确与否的标准,与传统计算平衡态方法相比,元素势能法更简便易行,并且更精确。

However, this is not just limited to casters -- a team of 5 thumpers + 3 monks is equally imbalanced because the team can ONLY fight 8v8 as a pressure team.

然而,并不是说这种不平衡仅局限于施法者,一个由5锤战和3僧侣的团队同样不平衡因为这个队伍只能作为一个整体打压力团战术。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。