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Sodium thiosulfate and carbon disulfide were used as sulfur sources in water and absolute alcohol systems, respectively.

在水溶液体系和乙醇溶液体系中,于常温常压下不加入任何催化剂,用γ射线辐照技术可以成功制备出纳米ZnS晶体,其中硫代硫酸钠和二硫化碳分别为上述两体系的硫源。

To obtain new functional aromatic polymer material, the reaction of acenaphthene with nitrobenzene under high active catalyst of AlCl3 was investigated at room temperature and ambient atmosphere.

为制备更多新型功能高分子中间体,研究了高活性lewis酸AlCl3催化作用下,苊与硝基苯在温和条件常温常压下的反应。

To obtain new functional aromatic polymer intermediates, the coupling reaction of acenaphthene catalyzed by inorganic salts, such as AlCl3, FeCl3, ZnCl2 and ionic liquid(Cl/FeCl3) was investigated at room temperature and ambient atmosphere.

为合成新型功能高分子中间体,分别研究了在AlCl3, FeCl3, ZnCl2等无机盐和Cl/FeCl3离子液体催化作用下,苊在温和条件常温常压下的偶联反应。

Acenaphthene was dehydrogenated to afford acenaphthylene by photochemical reaction with N bromosuccinimide in benzene with the addition of quinoline at room temperature and atmospheric pressure was studied.

在常温常压下,以苯作为溶剂,加入喹啉,使苊与N-溴代丁二酰亚胺发生光化学脱氢反应生成苊烯。

It was showed, the acid value and the peroxide value increased with heating time in normal condition.

结果表明,在常压条件下,随加热时间加长,酸价和过氧化值呈线性增大。

Through the steps such as acidify, filteration, extraction , distillation and vacuum distillation, the product is seperated from compounds.

通过酸化、过滤、萃取、常压蒸馏和减压蒸馏等后处理手段,将产物分离出来。

With the H3PW12O40/Al2O3 as catalyst, the conditions of preparing acrolein from glycerol were studied in a continuous fixed bed reactor.

同时利用常压连续流动的固定床反应器考察该催化剂对甘油制备丙烯醛的工艺条件,重点考察了催化剂的种类、杂多酸的负载量、反应温度等条件对反应的影响。

Meanwhile the process conditions of catalyst on preparing acrolein with glycerol were investigated by using continuous-flow fixed bed reactor. The effects of conditions of catalyst sorts, loading of heteropoly acid, reaction temperature etc.

同时利用常压连续流动的固定床反应器考察该催化剂对甘油制备丙烯醛的工艺条件,研究了催化剂的种类、杂多酸的负载量、反应温度等条件对反应的影响。

Synthesis of Butyle Acylate with acrylic acid and butyl alcohol at the catalysis of ethand by heteropoly acid in reduced pressure distillation were described in this paper.

由于丙烯酸正丁酯沸点较高,在常压下蒸馏易发生自身聚合反应而影响产率,所以采用减压蒸馏以降低其沸点。

The optimal conditions were found as follows: reaction temperature 90℃, reaction time 50 min, the molar ratio of catalyst to diethyl adipate 1.1:1, providing 99.5% yield.

结果表明,各试验因素的影响效能为反应温度(反应时间(催化剂用量;最佳合成条件为反应温度90℃,反应时间50 min,催化剂与原料的摩尔比为1.1:1,在此条件下,常压合成目标物的产率可以达到99.5%。

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