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Polymerization was carried out between dimethyl adipate and triamine with the same mole ratio in the reactor. Acid dyeable additive can be obtained under the conditions of transesterification temperature 180~220℃, polycondensation temperature 240~270℃,pressure40~50Pa, The infrared analysis results showed that at the position of 1639cm^(-1), there was an obvious characterisitc peak of amide bond.

己二酸二甲酯与三胺按等量比在反应釜中进行聚合,在酯交换温度180~220℃,缩聚温度240~270℃,压力40~50Pa条件下即可获得酸性染料可染添加剂。

In this article, the solubility datas of solid-liquid phase equilibrium were measured, then the theory of solid-liquid phase equilibrium of succinic acid, glutaric acid and adipic acid in various solvents were studied, finally the separation,recovery and reuse methods of mixed dibasic acids were carried on a systemetical research.

本文在测定固液平衡溶解度数据,并进行丁、戊、己三种二元酸在各种溶剂中固液相平衡理论研究的基础上,对混合二元酸的分离回收方法和三种酸的再利用方法进行了系统研究。

Lactide, glycolide or caprolactone, biodegradable polyester and diisocyanate as materials are first bulk melt polymerized to prepare the degradable polymer with thermal deformation transforming temperature of about 37 deg.c. The obtained material is processed at temperature over melting temperature so as to shape into spiral rack, applied with stress at temperature higher than Ttrans to form shape easily operational handling and frozen to eliminate stress into the product.

本发明以丙交酯、乙交酯或己内酯,生物可降解聚酯及二异氰酸酯为原料,通过本体熔融聚合制备得到热致形变温度转化点在37℃左右的可降解高分子材料,将得到的材料在熔融温度以上进行加工、赋形制作成用于不同管腔内的螺旋管状支架;在T>T trans 条件下施加应力,加工为便于手术操作的形状;冷冻定型消除应力,即得产品。

Lower temperature,lower effecitve alkali charge and shorter time resulted in a pulp with lower HexA content and higher screened yield.

较低的蒸煮温度、较低的有效碱用量和较短的保温时间有利于降低纸浆中己烯糖醛酸的含量,且纸浆的细浆得率也较高。

The formation of microemulsion system containing emulsifier,acrylamide,2-ethyltrimethyl ammonium chloride,sodium-2-acrylamido-2-methyl-propane-sulfonate and hexamethylene was studied.

对复配乳化剂(span+tw een)、丙烯酰胺、(2-甲基丙烯酰氧乙基)三甲基氯化铵、2-丙烯酰胺基-2-甲基丙磺酸钠和环己烷组成的微乳液体系进行了研究,研究了单体总质量浓度、AM摩尔含量和阴阳离子单体配比改变对形成微乳液需要的适宜H LB值和最小乳化剂用量的影响。

Tetrachloroterephthalic acid was prepared by chlorinating terephthalic acid, oleumsolvent and iodine catalyst. Tetrachloroterephthalic acid was acylated by sulphurous oxychloride in the presence of DMF to form tetrachloroterephthaloyl chloride. The acyl chloride product was fluorinated by potassium fluoride and esterified by methanol to synthesize dimethyl tetrafluoroterephthalate. The ester was reduced with potassium borohydride and lithium chloride to give tetrafluoroterephthalyl alcohol. The above product was bromated in the hydrobromic acid to obtain 4-bromomethyl-2,3,5,6-tetrafluoro-benzene methanol. 4-Methyl-2,3,5,-6-tetrafluorobenzene ethanol was obtained by reducing the bromide with magnesium. In the exist of DCC and DMAP, tefluthrin was got by the condensation reaction between 4-methyl-2,3,5,6-tetrafluoro-benzene methanol and-(1RS,3RS)- 3-(2- chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethyl cycolpropanecar-boxylate acid.

对苯二甲酸与氯气在碘存在下以发烟硫酸为溶剂进行氯化制备四氯对苯二甲酸;再以DMF为催化剂与二氯亚砜反应生成四氯对苯二甲酰氯;以氟化钾为氟化剂,环丁砜为溶剂置换氟化,再与甲醇酯化得到四氟对苯二甲酸甲酯;以KBH4-LiCl为还原剂二甲醚为溶剂反应制得四氟对苯二甲基苄醇;以氯苯为溶剂在溴化氢溶液中溴化得到溴化产物;在乙醇溶液中经镁粉还原得到4-甲基-2,3,5,6-四氟苄醇;甲基苄醇与功夫酸在催化剂二环己基碳二亚胺和4-二甲氨基吡啶作用下缩合得到七氟菊酯,总收率达43.6%。

Those biodegradable materials finally form into CO2 and H2O via culture of tricarboxylic acid cycle, which can be excreted from lung, kidney, and skin. Hydroxyacetic acid is a metabolic product of amino acids. Therefore, velocity of bioldegradable materials can be controlled in vivo. The recent contraception focuses on discover a sustained release system of biodegradable materials.

生物可降解材料包括聚乳酸、聚ε-己内酯、乳酸-羟基乙酸共聚物等,这些材料有很好的生物相容性,植入体内后可经生物降解成乳酸单体,经三羧酸循环后最终成为CO2和H2O,经肺、肾、皮肤排泄,羟基乙酸也是机体氨基酸代谢产物,而且生物可将解材料在体内降解速度是可控的,用生物降解聚合物作为药物载体的缓释避孕系统是目前材料学以及避孕节育研究的一大重点。

The cell suppression ratio and surviving ratio were detected respectively under conditions of simple hypoxia, or 5mmol/L glucose complicated with hypoxia. The mRNA levels of key enzymes that are involved in regulating glyco-metabolism were detected, including the mRNA levels of pyruvate-kinase, hexokinase, succinic dehydrogenase and isocitric dehydrogenase, and the activity of lactate dehydrognase.

以SMMC-7721人肝癌细胞和L02正常肝细胞作为研究对象,分别在单纯缺氧及加葡萄糖缺氧条件下,观察细胞生长,并检测糖代谢关键酶:丙酮酸激酶(pyruvate-kinase, PK)、己糖激酶(hexokinase, HK)、琥珀酸脱氢酶(succinic dehydrogenase, SDH)、异柠檬酸脱氢酶(isocitric dehydrogenase, IDH) mRNA表达水平和乳酸脱氢酶(lactate dehydrogenase, LDH)活性。

The details and results are summarized below:(1)An ABC style three component cascade reaction of aromatic aldehydes, aromatic amines and diethyl malonic ester or cyclohexanone has been developed.

论文从苯炔和亚胺出发,设计并系统研究了4种新的多组分串联反应,主要内容和结果如下:(1)发展了一种芳醛、芳胺和丙二酸二乙酯或环己酮的ABC型三组分串联反应。

As we have learned, alkyl of oxygen of silicon of system of 2 methylic link, oneself the product such as 2 acid, TDI already was turned over by Department of Commerce dumping investigation.

据了解,二甲基环体硅氧烷、己二酸、TDI等产品已被商务部反倾销调查。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。