己酸

Then the catalysts of high activities were selected to be used in the preparation of mixed dibasic acid dimethyl esters.Mixed dibasic acids are byproducts of hexanedioic acid. In this article DBE were synthesized.

己二酸生产过程中副产大量的混合二元酸，本文选用DBA和甲醇为原料，分别采用磷钨杂多酸、PW_(12)/C和PW_(12)/SiO_2为催化剂，合成了绿色环保高沸DBE。

The polyesters with terminal hydroxyl groups were prepared by condensation polymerization of adipic acid with 1,4-butanediol or ethylene glycol and, in some cases, a little amount of propylene glycol. The polyurethane thermoplastics were then prepared with the polyester, 4,4'-diphenylmethane diisocyanate and 1,4-butanediol.

采用己二酸、乙二醇(或加入少量1，2-丙二醇)和1，4-丁二醇制备了端羟基聚酯，并用该聚酯和4，4'-二苯基甲烷二异氰酸酯、1，4-丁二醇制备了聚酯型热塑性聚氨酯；考察了NCO/OH值、聚酯分子量等因素对热塑性聚氨酯的物理机械性能的影响。

A series of segmented thermally stimulated shape-memory polyurethanes, which consist of polyethylene adipate glycolas the soft segment and 4,4'-diphenylmethane diisocyanate-1,4-butanediol-DPA(which consists of ring components) as the hard segment were synthesized by one-step polymerization.

以聚己二酸乙二醇酯二醇为软段、4，4' -二苯基甲烷二异氰酸酯 1，4 丁二醇含环状结构的扩链剂DPA为硬段，采用一步聚合法制备了一种具有热致形状记忆功能的多嵌段聚氨酯弹性体。

All the complex series based on 4',4''-dicarboxy-1,6-diphenoxyhex- ane (C6-2COOH) and 4',4''-dicarboxy-1,10-diphenoxydecane (C10-2COOH) possessed higher melting and clearing points, usually showed soft crystal or crystalline smectic phases and crystal polymorphs except C10-2COOH/ p -PhBPy complex displaying also an enantiotropic nematic phase, while the complexes based on 4,4'-dicarboxy-α,ω-diphenoxy tetraethyleneglycol ether (C8O4-2COOH) with a longer flexible spacer exhibited monotropic fluidic smectic SmA and/or nematic phases.

研究表明，分别具有较短的6或10个亚甲基的烷烃间隔基的双苯甲酸衍生物4'，4''-二羧酸-1，6-二酚氧基己烷(C6-2COOH)和4'，4''-二羧酸-1，10-二酚氧基癸烷(C10-2COOH)的系列复合物具有较高的熔点和清亮点，一般都只出现结晶近晶相和多晶型转变现象。

The effect factors of ethyl linolenate separation by silver nitrate adsorption column were studied.

研究了负载型硝酸银吸附柱分离亚麻酸乙酯过程中的影响因素，考察了载体类型、溶剂种类(石油醚、正己烷、超临界CO2)等对亚麻酸乙酯分离效果的影响。

Furthermore,The results show that alumina is more suitable for the separation of ethyl linolenate than the widely used silica gel, and the supercritical fluids is a good solvent than organic solvent because of its adjustability by changing the extraction conditions.

研究结果表明，超临界流体分离效果优于石油醚和正己烷等有机溶剂，氧化铝载体分离效果优于硅胶，超临界流体结合硝酸银吸附柱分离亚麻酸乙酯具有较好的效果，可得到纯度约95%的亚麻酸乙酯，其工业应用前景诱人。

The experiment results indicate that the solvents (including n-hexane, ligarine, supercritical CO_2) and carriers all have great effects on the separation of ethyl linolenate from fatty acid ethyl ester mixture.

研究结果表明，超临界流体分离效果优于石油醚和正己烷等有机溶剂，氧化铝载体分离效果优于硅胶，超临界流体结合硝酸银吸附柱分离亚麻酸乙酯具有较好的效果，可得到纯度约95%的亚麻酸乙酯，其工业应用前景诱人。

Considering the functions of metal-organic frameworks and the synthesis conditions, we designed and synthesized six metal-organic frameworks based on rare earths by choosing multidentate organic carboxylate ligand, H3CTC, and using mild solvent vapor conditions.

在第二章中，我们利用半刚性的多齿有机羧酸配体——1，3，5-环己三酸与稀土金属元素合成了七个三维具有开放骨架结构的金属有机骨架晶体材料，由于稀土元素在光学和磁学方面的特殊性能，所获得的金属有机骨架材料不仅具有较好的吸附和储存性质，而且拥有金属中心赋予的独特的光学和磁学性能。

The grafting of polycaprolcatone on starch by ring-opening polymerization of e -caprolactone was initiated from the starch hydroxyl functions in the presence of a catalyst such as stannous octoate Sn(0ct2, Dibutyltin dilaurate or titanium tetrabutoxide. The grafting ration could reach 16%. IR, X-ray diffraction and DSC were used to investigate the grafting-polymer.

在辛酸亚锡Sn(Oct_2、二月桂酸二丁基锡和钛酸丁酯等催化剂作用下，淀粉羟基引发己内酯单体进行配位聚合，淀粉接枝率可以达到16％，并通过红外光谱、X—ray衍射及DSC等测试手段对反应产物进行了表征。

The extraction of Pr3+was studied by using heptane containing bis(2-ethylhexyl)phosphinic acid in sodium perchlorate,chloroacetic acid and citric acid medium ,respectively.

研究了二(2-乙基己基)膦酸(PIA-8)的庚烷溶液分别在高氯酸钠、氯乙酸、柠檬酸介质中对Pr3+的萃取。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。