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The solvents commonly used in the solvothermal synthesis include alcohols (such as methanol, ethanol, isopropanol, alcohol, ethylene glycol, glycerine, etc.), amines (such as hexamethylenediamine, dimethylformamide, triethanolamine), Acetonitrile and Propionitrile, the differences of functional groups, varieties of kinds together with a wide differences of polarity, dielectric constant and boiling point of organic solvents greatly increase the diversities of the product.

溶剂热合成常用的溶剂有醇类(如甲醇、乙醇、异丙醇、正丁醇、乙二醇、甘油等),胺类(如己二胺、二甲基甲酰胺、乙醇胺),乙腈和丙腈等,有机溶剂由于带有不同的官能团,种类繁多,具有不同的极性、介电常数、沸点等,大大增加了合成产物的多样性。

In this paper, 4-4-(trifluoromethoxy benzoyl cyclohexyl-3, 5-diaminobenzoate with a large branch chain, pyromellitic dianhydride and 4-(4-aminobenzyl) benzenamine were used to synthesize polyimides. The effect of monomer charge order on pretilt angle was investigated for the first time when PIs were used as LC alignment layer, and the effect of diamine mole ratio on pretilt angle was studied. The thermal stability of the pretilt angle was discussed.

文章用均苯四酸二酐、4,4'-二胺基二苯甲烷和具有较大支链的4-(4-苯甲酰基)环己基-3,5-二胺基苯甲酸酯等单体制备聚酰亚胺,首次研究了单体加料顺序对液晶预倾角的影响,同时也研究了二胺配比对液晶预倾角的影响问题,并探讨了预倾角的热稳定性等问题。

Make comprison of SGS concerning lathering power and foam stability. Test shows that N,N'-Difatty acid acyl hexamethylene-diamine-ethylene sulfonate(SGS-12)has better lathering performance and foam stability.

对SGS系列双子表面活性剂的起泡性能和稳泡性能进行了比较,其中N,N'-双月桂酰基己二胺二乙基磺酸钠(即SGS-12)具有更好的起泡性和稳泡性。

The main by-product s and their separation and recovery technologies were discussed for cyclohexanone gas-phase Beckmann rearrangement.

探讨环己酮肟气相Beckmann重排主要副产物及其分离回收方法,研究1-氮杂-2-乙氧基-1-环庚烯、1,3,4,5-四氧吖庚因-2-酮及其同分异十句体等副产物回收利用生成已内酰胺的方法。

The Beckmann rearrangement of cyclohexanone oxime, phosphorus pentoxide (P_2O_5) and dimethyl formamide raction system into caprolactam was studied.

研究了以环己酮肟、五氧化二磷(P_2O_5)、二甲基甲酰胺组成的反应体系进行Beckmann重排制备己内酰胺工艺,考察了不同溶剂、催化剂用量、温度、浓度及水分含量对重排反应的影响。

Then we applied these chrial ligands to asymmetric borane reduction of w-bromoacetophenone and diketones.

将其应用于前手性单酮及二酮的还原中,其中双方酰化脯氨酸在1,6-二苯基-1,6-己二酮的还原反应中可获得最高为90%的ee值。

Anti-TB bone was made of reconstituted bone xenograftcombined with 4 antituberculosis drugs ( Isoniazide, Rifampicin, Pyrazinamide, Ethambutol ) at certain concentration and encapsulated by gelatin and polycaprolactone.

采用明胶和聚己内酯复合包裹法将异烟肼、利福平、吡嗪酰胺和乙胺丁醇等4种抗结核药物按一定浓度和配比与重组合异种骨复合,制备抗结核骨。

The dosage of immobilized lipase of Enterobacter agglomerans is 1000 U, methanol as acyl receptors(alcohol:oil molar ratio is 3:1,3 times add),5 mL n-hexane,180 r/min,35℃,48 h,and the conversion rate was 91%.

硅藻土固定化成团肠杆菌脂肪酶用量为1000 U,甲醇为酰基受体,甲醇与油摩尔比为3:1,3次等量加入,5 mL正己烷,180 r/min,35℃反应48 h,转化率到91%。

We found that hexanoic acid and octanoic acid are insufficiently soluble (with solubilities of 9.68 and 0.68 mg ml21, respectively, in water) to produce any growth modification in L-asparagine monohydrate crystallization.

我们发现,己酸和辛酸在水中不能充分溶解(溶解度分别为9.68和0.68mg/ml,水溶液中),这一特性使它们对L -天冬酰胺单水合物结晶的生长起修饰作用。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。