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The GC/MS analysis indicated that the volatile compounds from the plant leaves which is easy to be damaged by Tetraychus vienneis include relative large amounts of cis-3-hexenyl ester acetic acid, cis-3-hexenyl ester butanoic acid and alpha-famesene.

结果表明,植物叶片中的挥发性物质得到了很好的分离,受山楂叶螨危害严重的植物的完好叶片中的挥发性物质均含有顺-3-己烯-1-醇乙酸酯、顺-3-己烯-1-醇丁酸酯和α-法呢烯,且含量较大。

Among 3 cultivars, B17 occupied the least green odor contents of aromatic constituents, such as 2-hexen-1-ol acetate, butanoic acid 3-hexenyl ester and butanoic acid 3-hexenyl ester, hut had the most fruity, flowery and woody odors such as β-Ionone, 1-nonanol, Acetic acid octyl ester, Methyl benzoate, Ethyl benzoate and theaspirane, which showed that B 17 was superior to the 2 other cultivars in aroma quality.

不同品种的杨桃果实中的所含的香气成分及含量不同,B17杨桃含乙酸-反-2-己烯酯、丁酸-反-2-己烯酯、丁酸-反-3-己烯酯等青香型酯类最低而含β-紫罗兰酮、1-壬醇、乙酸辛酯苯甲酸甲酯、苯甲酸乙酯、茶螺烷等花香型、果香型及木香型成分最高,因而其香气品质要优于B10和新加坡红肉种。

Objective To establish a HPLC method for determination of diethylstilbestrol and chloramphenicol in compound diethylstilbestrol cream .

目的用高效液相色谱法同时测定复方己烯雌酚乳膏中己烯雌酚和氯霉素的含量。

The industrial manufacturing technique, the trend of development of neohexene ,and the characteristics of these production technique were reviewed and analyzed in the paper, particularlyabout the selective dimerization of isobutylene and metathesis of βdiisobutylene with ethylene were introduced.

对新己烯生产技术的现状和今后的发展趋势进行了综述,分析了由异丁烯和乙烯生产新己烯的技术特征,讨论了烯烃二聚工艺和催化剂、烯烃复分解工艺及相应的催化剂,指出了各种工艺的优势和不足。

The result was compared with oxidations of cyclohexene without irradiation and at irradiation without catalyst.

另外,本文还研究了各种类型的催化剂在中压汞灯下光催化环己烯的氧化反应,结果表明,无论上述的哪种催化剂,在中压汞灯下光催化环己烯氧化反应,都得不到环氧环己烷,生成的产物主要为水和二氧化碳。

A method has been developed to determine residual stilbenes such as diethylstilbestrol, dienestrol and hexestrol in animal tissues using solid phase extraction and gas chromatography-mass spectrometry.

建立了动物组织中己烯雌酚、己二烯雌酚和己烷雌酚残留量的气相色谱-质谱分析方法。

The experiment results show that the yield of hexane catalyzed by the nano-fibrous catalyst was 4.7 times higher than that of PdCl_2/γ-Al_2O_3 catalyst. The hydrogenation ofα-tetradecylene, cyclohexene, nitrobenzol and styrene by the nano-fibrous catalyst was also studied, the selectivity to primary products of the hydrogenation of cyclohexene, nitrobenzol and styrene was 100%.

苯乙烯-丙烯腈共聚物负载纳米钯超细纤维形态催化剂在常温,氢气压力101.3Pa下催化α-己烯加氢时表现出很高的活性,催化剂PSAN-Pd10催化氢化α-己烯选择生成正己烷的产率在150 min就达到87%以上,与无机物负载的催化剂相比,加氢效果有显著提高,并且催化剂的重复使用性较好。

In the absence of organic solvent and phase-transfer catalyst, the catalytic oxidation of cyclohexene to adipic acid with aqueous 30% hydrogen peroxide by weight can be efficiently catalyzed by tungstenic acid/inorganic acidic ligand.

以钨酸/无机酸性配体为催化体系,在无有机溶剂和相转移剂的情况下,催化过氧化氢(质量分数30%)氧化环己烯合成己二酸。结果表明,以钨酸/磷酸催化氧化环己烯的催化效果最优。

The synthesis of alkylcyclohexylbenzoic acid: take the synthesis of ethylcyclohexylbenzoic acid as a typical example. With the AlCl3 as the catalyst, cis+trans acetylcyclohexylbenzene is synthesized from the reaction of acetyl chloride, cyclohexene and benzene.

烷基环己基苯甲酸的合成研究:主要研究了乙基环己基苯甲酸的合成,以乙酰氯、环己烯、苯为原料,三氯化铝为催化剂,合成乙酰基环己基苯,用水合肼、氢氧化钾、一缩二乙二醇经过高温加热还原羰基(Wolff-黄鸣龙还原),将所得到的乙基环己基苯用乙酰氯进行傅克酰基化得到乙基环己基苯乙酮,所得中间体经过处理之后直接得到反式产物,将反式异构体的乙酰基氧化得到反式烷基环己基苯甲酸。

With this aim, two different haptens mono- O -3-carboxypropyl- diethylstilbestrol and mono- O -carboxymethyldiethylstilbestrol with carboxylic group that preserve the molecular structure character of diethylstilbestrol were synthesized. The haptens were conjugated with the carrier proteins bovine serum albumin by mixed-anhydride method for immunogen and conjugated with ovalbumin by active ester method for coating antigen.

首先,两种保留己烯雌酚特征结构并具有活性基团的半抗原正丁酸己烯雌酚单醚、乙酸己烯雌酚单醚被合成;然后采用混合酸酐法将半抗原与BSA偶联制备成免疫原,采用活性酯法将办抗原与OVA偶联制备了包被原。

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