巯基

It is found that the sample stained with silver methenamine instead of mercaptoacetic acid-osmium can prevent the false phenomena caused by the inappropriate use of mercaptoacetic acid.

摘 要：本文将六亚甲四胺银染色法作为加工毛发的电子染色剂得到较好的电子显微图像，并系统地比较了用巯基乙酸-锇法染色的羊毛样品和用六亚甲四胺银染色的人发样品的超微结构，认为对深加工过的毛发样品用六亚甲四胺银法替代巯基乙酸-锇法染角蛋白，可以防止巯基乙酸使用不当引起的假象。

objective to observe the effect of unithiol for the treatment of arsenic apicitis.methods sixty-three patients received therapy with 5% unithiol and the therapeutic effect was retrospectively analyzed.results 59 of 63 teeth were cured with the cure rate 92%; no effect was observed in 4 cases.conclusion unithiol can be effectively used for the treatment of arsenic apicitis.

目的 观察二巯基丙磺酸钠治疗砷性根尖炎的疗效。方法 63例患者患牙63颗接受5%二巯基丙磺酸钠治疗，回顾分析其疗效。结果 63颗患牙经本药治疗后59颗显效，占93.7%；4颗无效。结论二巯基丙磺酸钠可有效并安全用于治疗砷性根尖炎。

A series of sulfonated poly(arylene thioether/ether phosphine oxide)s was prepared by direct polycondensation of sBFPPO and BFPPO with the diphenol-type or dimercapto-type monomers such as hydroquinone, bisphenol-A, 4,4'-biphenol, 4,4'-diphenol (6F), 1,5-dihydroxynaphthalene, 4,4'-dihydroxybiphenyl, and 4,4'-thiobisbenzenethiol, respectively.

将BFPPO与sBFPPO分别与多种二羟基或二巯基单体，如对苯二酚、双酚A、4，4'-二苯酚、双酚F、1，5'-二羟基萘、4， 4'-二羟基二苯硫醚和4，4'-二巯基二苯硫醚，直接共聚制备了一系列磺化聚芳醚三苯基氧膦，侧重考察了二羟基和二巯基单体结构单元对产物的耐氧化性能的影响。

The method comprises following steps: reacting hydroxylation carbon nano-tube successively with reagent containing halogen and hydrosulphide to prepare sulfhydryl carbon nano-tube; reflowing the sulfhydryl carbon nano-tube and platinum salts in polyatomic alcohol, processing in hydrogen atmpsphere to obtain sulfhydryl anchoring platinum / carbon nano-tube catalyst; reflowing the sulfhydryl carbon nano-tube successively with the hydrochloroauric acid and the platinum salts in polyatomic alcohol, processing in hydrogen atmpsphere to obtain sulfhydryl anchoring platinum-gold / carbon nano-tube catalyst.

本发明将市售羟基化碳纳米管先后与含卤试剂和氢硫化物反应得到巯基化碳纳米管。再将巯基化碳纳米管与铂盐在多元醇中回流，氢气氛中处理得到巯基锚固铂/碳纳米管催化剂。将巯基化碳纳米管依次与氯金酸和铂盐在多元醇中回流，氢气氛中处理得到巯基锚固铂-金/碳纳米管催化剂。

This work shows that mercapto acctic acid can be fixed on the conducting polypyrrole film electrode by one-step or two-step method.

通过将巯基乙酸作为一种支持电解质，将巯基固定在导电聚吡咯薄膜电极上，从而制得巯基—聚吡咯薄膜修饰电极，该修饰电极保持了巯基的螯合性能，并具有良好的稳定性。

A polar sensitive probe with selective marks prepared by the invention can be used for compounds comprising mercapto. Owning to the introduction of the maleimide group, the probe can be used for the measurement and research of marks of biomacromolecules that comprise the mercapto and adjacent regional polarity change situations of the mercapto, in particular to the research of the selective marks of the mercapto and the adjacent regional polarity change situations of the mercapto in protein.

本发明制备出一种能够用于含有巯基的化合物的选择性标记的极性敏感探针，该探针由于马来酰亚胺基团的引入，可以用于含有巯基的生物大分子的标记及巯基附近区域极性变化情况的测定和研究，特别是蛋白质中巯基的选择性标记和巯基附近极性变化情况的研究。

As mercapto -function group has strong sorption on methyl mercury, an experiment was conducted to reveal the effect of the substances containing mercapto -groups on transfer and transform of mercury in soil by adding wool whose decomposed products consisting of abundant mercapto -composition.

巯基对汞特别是甲基汞有强烈的吸附作用，本试验通过对土壤添加富含巯基官能团的羊毛，初步研究含巯基物质在土壤环境中对土壤汞迁移转化作用的影响。

The serum selenium is first digested by microwave treatment and then chemically purified before analysis by using sulphydryl cotton. The optimum conditions were found to b as follows:(1) The sulphydryl cotton column is prewashed with 5 mol/L hydrochloric acid;(2) Se is desorbed by adding 1 mL of concentrated nitric acid and (3) the optimum amount of sulphydryl cotton is 0.14 g. This preconcentration step is required in order to remove matrix-interfering elements, such as Na, Mg, K and Ca.

采用微波消解－巯基棉分离对人血清样品进行前处理，通过对巯基棉分离血清中硒的条件优化，结果表明，柱条件为5mol/L HCl、解脱Se条件为1mL重蒸HNO3、巯基棉最佳用量为0.14g时，能够有效分离出人血清样品中的Na、Mg、K、Ca等碱金属和碱土金属，同时硒的回收率最高，达到92%以上。

All of the tripodal schiff base ligands and their complexes were characterized.

以三乙醇胺、巯基苯胺、巯基乙胺为初始原料，设计合成了六个三脚架结构的化合物，其合成路线如下：三乙醇胺与氯化亚砜反应得到三(2-氯乙基)胺(1)，然后与巯基苯胺或巯基乙胺在碱性条件下反应生成三脚架结构的三{[2-(2-氨基苯基)硫代]乙基}胺(2)或三{[2-(2-氨基乙基)硫代]乙基}胺(3)，然后再与水杨醛、2-甲酰基-8-羟基喹啉(8)、2-甲酰基-8-苄氧基喹啉(7)反应得到六种新型的含硫西佛碱化合

Typically,0.2 mmol of cd solution, and 0.4 mmol of mpa solution were mixed in a 40 ml solution and the ph of the solution was 二氰基丙酸乙酯 to 10.0 by solution was palced in a three-necked flask and was deaerated.

通常情况下， 0.2浓度的镉环硫乙烷，和0.4浓度的mpa的混合溶液中40巯基丙酸甲酯溶液和ph值的溶液是调整，以10.0的溶液放置在是在三制作乙酸钙中，并除去溶液中的气体。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。