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Based on the previous literatures, the following major innovation works were carried out in this dissertation:(1) The derivatization reaction conditions of ephedrine and pseudoephedrine with sensitive derivation reagent in aqueous system were studied and two new methods were developed for the assay of them by microemulsion electrokinetic chromatography and micellar electrokinetic chromatography with LIF detection. The sensitivity and analysis times were greatly improved compared with the previous reports;(2) A new method of CZE with indirect LIF detection was developed for the simultaneous determination of six coumarin compounds (esculin, esculetin, isofraxidin, genistein, naringin and sophoricoside) with fluorescein as the probe. The proposed method enlarges the application range of LIF detector, and provides new approach for the analysis of certain compounds difficult to derivatize;(3) Based on the above research, an MEKC with indirect LIF detection method for the simultaneous determination of adenine and guanine in DNA extracts from fungus, maize and soybean was established;(4) A new method for the investigation of the complexes formed between human serum albumin and ampicillin sodium under the simulated physiology conditions using laser light scattering technique was developed.

该论文在综述前人工作的基础上,开展了如下未见文献报道的创新性的研究工作:(1)使用灵敏的衍生试剂对麻黄碱和伪麻黄碱在水体系中的衍生反应条件进行了系统研究,建立了微乳电动色谱-激光诱导荧光检测法和胶束电动色谱—激光诱导荧光检测法测定麻黄碱和伪麻黄碱的灵敏分析新方法,与以前的报道相比,灵敏度和分析时间均有很大改善;(2)使用荧光素钠作为背景荧光试剂,建立了同时分析测定六种黄酮类化合物(秦皮甲素、秦皮乙素、异秦皮定、染料木素、柚皮苷和槐角苷)的毛细管区带电泳—间接激光诱导荧光检测新方法,扩大了激光诱导荧光检测的应用范围,对难衍生化合物的分离分析提供了一种新思路和新途径;(3)以荧光素钠作为背景荧光试剂,建立了一种用于同时测定食品提取DNA中的腺嘌呤和鸟嘌呤含量的胶束电动色谱—间接激光诱导荧光检测新方法;(4)用动态和静态激光散射法研究了模拟生理条件下人血清白蛋白与氨比西林钠盐相互作用所形成的复合物,为药物分子与蛋白质的相互作用、药代动力学等的研究提供了一种新思路。

Operating modal analysis is a new technology of modal analysis. The operating modal parameters obtained only by responses of operating machinery or ambient excitation accord with the real operating situations and the boundary conditions, and illustrate the real dynamic behavior of the operating machine.

工作模态分析方法是一种新的模态分析技术,利用工作状态或环境激励下的响应信号识别出的工作模态参数符合实际工况及边界条件,能真实的反映结构在工作状态下的动力学特性。

Some key part is ameliorated to meet the demands of working. This thesis mainly includes:(1) Analysing the working principle of the spring operateing mechanism, expatiating the character of the mechanism;(2) With the design aim of the spring operating mechanism, accomplishing the design of ZW□-12/630-20 outdoor HV vacuum breaker based on the systemic design theory of the spring operating mechanism, which includes spring mechanism of open-close switch; cam mechanism based on the principle of power balance; buckle-off mechanism with force-minished device; ratchet wheel mechanism with number-increased detent;(3) In the design on the spring operating mechanism for the outdoor vacuum breaker, using the air cushion device with speed controller to ensure the steady working of the spring operating mechanism;(4) Accoding the problem of daily maintenance for HV circuitbreaker, giving some effective steps of daily maintenance.

论文工作主要包括以下几个方面:(1)从真空断路器弹簧操动机构的功能原理出发,详细分析了该机构的工作原理,阐述了机构工作的基本特性;(2)根据工程实际提出了真空断路器弹簧操动机构的设计目标,在系统分析弹簧操动机构设计理论的基础上,完成了ZW□-12/630-20型户外真空断路器弹簧操动机构的设计工作,其中包括真空断路器弹簧操动机构的分合闸弹簧机构的设计;以输出力特性曲线设计机构理论演化出的功率平衡原则为基础的凸轮机构的设计;带有减力机构的滚动摩擦扣结方式的脱扣机构设计;根据实际情况增加了棘爪数量的棘轮机构设计;(3)在真空断路器弹簧操动机构的设计中,引入了速度控制模式空气缓冲器,对惯性负载起到了良好的自动缓冲效果,从而保证了真空断路器弹簧操动机构稳定、有效地运行,保证了真空断路器的动作质量;(4)针对目前真空断路器运行过程中存在的问题,提出了有效的日常维护措施。

The main findings of the empirical analysis include: 1 The decisions concern the choices of auto ownership, mode to work, and auto use were made simultaneously and interrelatedly. 2 The decline in correlation between the choices of auto ownership and use as the number of vehicle increase indicated that to own multi-vehicles in not necessary due to the demand for auto use. 3 Both price elasticity and income elasticity for auto ownership are low. This evidence implies that auto has become a kind of necessity for household. Therefore, the effect of decreasing the tendency of auto growth by means of increasing the cost of owning auto would not be significant. The price elasticities of auto use are between -0.48 and -0.78. 4 There are same underlying factors influencing auto ownership, mode to work, and auto use including: parking time at residential location, accessibilities to work location by auto and transit, auto use unit cost, and the percentage of auto use for work. These factors indicate a direction for the formatting of future automobile policies.

本研究以台湾地区之家户个体资料从事实证分析,实证分析之主要结论如下:1小汽车持有数量、工作者工作运具选择、与小汽车使用量等选择间确有相关与联立性存在;2小汽车持有数量选择与小汽车使用量选择间之相关性会随小汽车持有数量的增加而降低,显示选择持有多部小汽车并非完全基於小汽车使用之需要;3小汽车持有之价格弹性与所得弹性均偏低,显示小汽车已成为民生必需品,欲以提高小汽车持有成本之价格手段来抑制小汽车持有,并无法竟其功,小汽车使用需求之价格弹性则在-0.48与-0.78间;4影响小汽车持有数量、工作者工作运具、与小汽车使用量等选择主要之相关或共同因素包括:家户附近停车状况、私人运具与大众运输工具之工作可及性、小汽车单位使用成本、与小汽车工作使用比率等,以上这些影响因素可为日后小汽车相关政策的研拟提供一方向。

A modified method bibed on the classical target factor analysis,refeed to as calibration working mains-TFA,waS used to perform a simultaneous determination-of a single or several mixture samples of food pigment s by confirming a corresponding calibration working matrix.

采用由目标因子分析法改进形成的校准工作矩阵法,对多组分食用合成色素混合体系进行同时测定。该法通过确认一个相应的校准工作矩阵即可对单个或多个混合样品的各组分进行同时直接测定。对七种三组分食用色素样品(各组分浓度在4.32~21.00μg/ml)的分析,各组分的回收率在97.93%~104.80%之间。与传统的目标因子分析法比较,此法特别适用于定性组成及定量范围基本清楚的混合样品的例行分析

Strip limit minimum rollable gauge and minimum rollable gauge considering productivity are analyzed and derived using new rolling pressure model, work roll surface temperature rise formulae is derived on the basis of mill stand thermal balance. The affecting factors of work roll surface temperature and the influences on the choice of roll size are discussed.

本文从轧机结构设计、力能参数计算、强度设计计算等方面综合论述了辊系参数设计计算的基本理论,在理论上提出了采用考虑粘着摩擦的混合摩擦模型和考虑轧件的弹性变形计算冷轧薄板轧制压力的方法,推导并以冷轧机实测轧制压力验证了轧制压力新模型;应用新的轧制压力模型分析并推导了轧件极限最小可轧厚度和考虑生产率的最小可轧厚度公式;根据工作机座热量平衡原理推导了工作辊温升公式,分析了工作辊温度的影响因素,研究了工作辊温升对轧辊参数选择的影响。

Through simulation and computation, some critical values to contral interferences are obtained. These values have directive significance to the design and deployment of WRAN.(4) New methods to measure and analyze spectrum aredevelopedAccording to the shortages of previous spectrum measurements, new methods to measure spectrum occupancy in wide-band and multi-point synchronously is proposed in this dissertation, and the tests last a whole week; the relativities of licensed services are considered when test points are selected. More importantly, data mining and in-depth analysis are carried out with the huge amounts of test data, and a channel analysis method using Channel Vacancy Duration and Service Congestion Rate are proposed. The spectrum relativities of 3-dimension in time, space and frequency are researched also. The correlativity between channel state and history information is discoved, and which will provide the scientific basis to channel modeling, spectrum analysis and decision of CR users.

4提出了频谱测量与分析的新方法针对以前频谱测量工作存在的不足,本文提出了多点同时广域频谱测量方法,测量工作持续了一周的时间,同时考虑了测量地点的选取和频谱授权业务之间的相关性;对测量得到的海量数据进行了数据挖掘和深度分析,提出了使用信道空闲时间(Channel VacancyDuration,CVD)和业务拥塞率(Service Congestion Rate,SCR)进行信道分析的方法,研究了频谱之间的时间、空间、和频率三维立体的相关性,发现了信道状态和历史信息的关联性,为CR用户的信道建模、频谱分析和决策提供了科学的理论依据。

Main research works are as follows:(1) Numerical simulation of turbulent flow and combustion in power plant furnace (2) Numerical simulation of fire spread and crown fire in forest fire behave (3) Numerical simulation of burning process of large space building (4) Numerical simulation of three-dimensional fluid flow of satellite cabin in microgravity environment (5) Numerical simulation of burning process of multi-rooms It shows that the ability of FAC3 and FZ code is strong and the code is widely used for practical problems.

研究工作主要涉及以下几个方面:(1)电站煤粉锅炉流场的数值分析(2)林火行为中火蔓延和树冠火等特性的数值研究(3)大空间建筑火灾烟气流动过程的数值分析(4)微重力条件下卫星密封舱内部流场的数值分析(5)多室火灾过程的数值分析研究工作表明,FAC3和FZ程序的功能较强,通用性较好,可对多种热过程现象进行数值模拟,在一定程度上讲,即可用于科学研究,又可用于实际工程问题,并具有广泛的应用前景和推广价值。

And then, the influencing rule between the key factors to plug queue speed and working reliability of this set is ascertained, and the variety range of these factors is made, and the theoretic analysis correctness is validated by a great deal of experiments, and the key problem of improving the transplanting speed is solved. So the foundation is set for its practical use.

进一步通过对其关键部件的运动和受力情况分析,掌握了各主要工作参数对钵苗排队速度和工作可靠性的影响规律,确定了各工作参数的工作范围,并通过大量试验验证了理论分析的正确性,解决了提高栽植速度的关键问题,为其实用化打下了基础。

The math model of the movement,flux and control system of position pump was established by analyzing its working principle,and its hydraulic system simulation model was established based on AMESim.The pressure and flux pulsation of the position pump was analyzed,and the pressure and flux was calculated by simulation when there are sign of wear for the position pump and system flux change.

分析了恒压力轴向柱塞泵的工作原理,推导并建立了液压泵压力流量和压力调节机构的数学模型,并在此基础上以AMESim工程软件为平台建立了轴向柱塞泵的仿真模型,分析了压力流量脉动状况并对液压泵在内部磨损和系统流量变化两种情况下的压力流量进行了仿真计算,对两种情况下泵的工作情况进行分析比较,为液压脉动抑制和故障分析提供了参考。

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Finally, according to market conditions and market products this article paper analyzes the trends in the development of camera technology, and designs a color night vision camera.

最后根据市场情况和市面上产品的情况分析了摄像机技术的发展趋势,并设计了一款彩色夜视摄像机。

Only person height weeds and the fierce looks stone idles were there.

只有半人深的荒草和龇牙咧嘴的神像。

This dramatic range, steeper than the Himalayas, is the upturned rim of the eastern edge of Tibet, a plateau that has risen to 5 km in response to the slow but un stoppable collision of India with Asia that began about 55 million years ago and which continues unabated today.

这一引人注目的地域范围,比喜马拉雅山更加陡峭,是处于西藏东部边缘的朝上翻的边框地带。响应启始于约5500万年前的、缓慢的但却不可阻挡的印度与亚洲地壳板块碰撞,高原已上升至五千米,这种碰撞持续至今,毫无衰退。