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Another approach in enhancing the light extraction efficiency of AlGaInP LED was accomplished using a surface roughening process. In this process, the Au(170 nm)/AuBe(260 nm)/Au(170 nm) ohmic contact layers were first deposited on the GaP window layer. After the alloy annealing process (480°C for 10 min), the Be atoms will diffuse into the GaP top layer and form non-uniform clusters. The LED samples were then immersed into a mixture 3H3PO4:1H2O2:1H2O solution for 6 min, resulting in a rough GaP surface. The luminous intensity of the AlGaInP LED can increase from 42 to 50 mcd, that is, an 18% enhancement can be achieved via the present non-photolithography surface roughening process.Keywords: LED, AlGaInP, Cu substrate, Reflector, Surface roughening

在实验的第二部份是开发磷化镓窗口层之粗化制程,我们是藉由正面金/铍欧姆接触电极之熔合制程,使铍扩散至磷化镓层,同时利用铍渗入磷化镓造成之特殊组成,可形成不均匀之蚀刻阻挡,而在磷化镓表面形成粗化,我们发现480℃、10分钟的熔合制程,加上浸泡磷化镓蚀刻溶液6分钟,可将四元发光二极体之发光亮度由42 mcd 提升到50 mcd,经由此无光罩粗化制程可将亮度提升18%,明显提升磷化铝铟镓发光二极体之外部量子效率。

Tetraploid embryos could be produced by electrofusion at the stage of two-cell embryos, which could develop to blastocysts followed by fusion of cytoplasm and nucleus and cleavage in vitro. During the fusion of cytoplasm, the DNA methylation levels of the fused embryos are as high as these of two-cell diploid embryos in vivo Then the embryos are rapidly demethylated when the nucleus begin to fuse, resulting in the lowest DNA methylation levels when the nucleus are fused completely. After that, the DNA methylation levels of the fused embryos are gradually increased until the morula stage. However, whereas an asymmetric distribution of DNA methylation is established in vivo-derived blastocysts with a higher methylation level in the inner cell mass than that in the trophectoderm, we can not detect the asymmetric distribution in most in vitro-derived tetraploid blastocysts.

结果表明:利用电融合方法制备的小鼠四倍体胚胎在体外培养体系中经历细胞质融合、细胞核融合及细胞继续分裂发育直到囊胚期的过程,在细胞质融合的时候胚胎卵裂球同体内体外培养二倍体胚胎一样,呈现高度甲基化状态;在细胞核开始融合的时候,甲基化水平急速下降,在细胞核完全融合的时候甲基化水平达到最低点;随着胚胎继续分裂,胚胎甲基化水平逐渐增加,在桑葚胚期甲基化水平最高;但是囊胚期四倍体胚胎内细胞团同滋养层细胞甲基化荧光信号没有差别,这与体内体外培养二倍体囊胚内细胞团细胞甲基化荧光强度高于滋养层细胞甲基化荧光强度不同。

Tetraploid embryos could be produced by electrofusion at the stage of two-cell embryos, which could develop to blastocysts followed by fusion of cyto-plasm and nucleus and cleavage in vitro. During the fusion of cytoplasm, the DNA methylation levels of the fused embryos are as high as these of two-cell diploid embryos in vivo Then the embryos are rapidly demethylated when the nucleus begin to fuse, resulting in the lowest DNA methylation levels when the nucleus are fused completely. After that, the DNA methy-lation levels of the fused embryos are gradually increased until the morula stage. However, whereas an asymmetric distribu-tion of DNA methylation is established in vivo-derived blastocysts with a higher methylation level in the inner cell mass than that in the trophectoderm, we can not detect the asymmetric distribution in most in vitro-derived tetraploid blastocysts.

结果表明:利用电融合方法制备的小鼠四倍体胚胎在体外培养体系中经历细胞质融合、细胞核融合及细胞继续分裂发育直到囊胚期的过程,在细胞质融合的时候胚胎卵裂球同体内体外培养二倍体胚胎一样,呈现高度甲基化状态;在细胞核开始融合的时候,甲基化水平急速下降,在细胞核完全融合的时候甲基化水平达到最低点;随着胚胎继续分裂,胚胎甲基化水平逐渐增加,在桑葚胚期甲基化水平最高;但是囊胚期四倍体胚胎内细胞团同滋养层细胞甲基化荧光信号没有差别,这与体内体外培养二倍体囊胚内细胞团细胞甲基化荧光强度高于滋养层细胞甲基化荧光强度不同。

Tetraploid embryos could be produced by electrofusion at the stage of two-cell embryos, which could develop to blastcysts fellowed by fusion of cytoplasm and nucleus and cleavage in vitro.After fusion of cytoplasm, the DNA methylation levels of the fused embryos was very high as well as two-cell diploid embryos in vivo.Then the embryos was rapiddly demethylated when the nucleus begin to fuse, resulting the lowest DNA methylation levels when the nucleus fused completely.After that, the DNA methylation levels of fused embryos were gradually increased until the blastocysts stage.However, whereas an asymmetric distribution of DNA methylation was established in an vivo-derived blastocysts with a higher methylation level in the inner cell mass than in the trophectoderm, in most vitro-derived tetraploid blastocysts, we can not detect the asymmetric distribution.

结果表明:利用电融合方法制备的小鼠四倍体胚胎在体外培养体系中经历细胞质融合、细胞核融合及细胞继续分裂发育直到囊胚期的过程,在细胞质融合的时候胚胎卵裂球同体内体外培养二倍体胚胎一样,呈现高度甲基化状态;在细胞核开始融合的时候,甲基化水平急速下降,在细胞核完全融合的时候甲基化水平达到最低点;随着胚胎继续分裂,胚胎甲基化水平逐渐增加,在囊胚期甲基化水平最高;但是囊胚期四倍体胚胎内细胞团同滋养层细胞甲基化荧光信号没有差别,这与体内体外培养二倍体囊胚内细胞团细胞甲基化荧光强度高于滋养层细胞甲基化荧光强度不同。

Secondary pollution might be produced in the weak zone while conventional acidify because of halfway flowback under poor producing energy. Thief zones can obtain superfluous acidizing fluid because of the permeability contrast between layers of prominent interlamination antinomy, which can induce collapse in the thief zone and invalid acidification in the less permeable layers.

低压油气层常规酸化时由于地层能量低,导致残酸溶液无法彻底返排而引起地层的二次污染;层间矛盾突出的地层,由于渗透率差异,酸液将优先进入高渗地层,导致高渗透层进酸量多,从而过度酸化引起坍塌,低渗透层则由于进酸量少而达不到酸化的目的。

This article that focuses on the systematic and in-depth research in the current primal problem about abnormal burst pressure reservoir depress burst pressure has procured following main fruits:1 It forms the method which could obtain massive vertical static state mechanics parameters.2 In a foundation of acquisition of rock mechanics parameters,apply bent lamella that as mechanical model along with characteristic of actual geologic characteristics to analysis curvature for anticlinal strcture, get homologous tectonic stress value throug relation between the curvature and stress and different principal curvature in anticlinal structure,consequently set up laminational stress model for anticline reservoir. The block lamination for existed fracturing date has formed method of setting up mechanical model of lamination terrestrial stress by abtaining the block tectonic stress coefficients which are got by complex utilization test, laboratory test and fracturing date playback.3 Analysesing the main reason which lead to high burst pressure by considering the characteristic of reservoir geology,reservoir,and rock mechanics and reservoir damage,etc.Establishing burst pressure quantitative prediction model which provide gist for depressing construction risk and optimizing construction craft under the condition of open hole completion ,gun-perforated completion and damaged reservoir.4 Provding theoretical basis for interpreting acidification pretreatment which could depress busrt pressure by finding the relation between the influencing factors and rock machanics parameters and analysing the factors that have effect on rock mechanics parameters. Expounding the mechanism of reaction of mixed monomineral and acid from the angle of microcosmic element, evaluating quantitatively acid sensilility of different kinds of mineral effectively, and determing the first-order reaction dynamical equation of each mineral.5 Revealing rock mechanics property chage as a result of acid flooding in different condition by sandstone traumata experiment in different temperatures which combined with rock mechanics triaxial stress experiment.6 Associating damage mechanics with sandstone acidizing, established sandstone damage mechanics model in the foundation of the recognition on the rock mechanics parametric variation which is caused by acid-rock reaction in both macroscopic view and microscopic view ,also demonstrated those processes and quantitative estimated the acid busrt pressure to direct the site operation.

本文针对目前异常破裂压力储层降低破裂压力的主要问题展开较为系统和深入的研究,取得了以下主要成果:1形成了利用测井资料,结合室内岩芯测试结果,获取静动岩石力学参数的相关性特征,从而获得纵向上大量静态力学参数的方法。2在获取了岩石力学参数的此基础上,利用弯曲薄板作为力学模型,结合区块实际地质特征对背斜构造进行曲率分析,通过曲率与应力的关系,利用背斜构造不同部位的主曲率求得相应的构造应力值,从而建立起背斜储层的分层应力模型;对已有压裂资料的区块分层,形成了综合利用测试、室内实验、压裂资料反演获得该区块构造应力系数,建立起分层地应力的力学模型的方法。3综合考虑储层地质、油藏、岩石力学特性和储层伤害等因素,分析造成高破裂压力的主要原因,综合利用岩石力学、弹性力学等知识,建立了裸眼完井、射孔完井条件下以及储层受到伤害后的储层破裂压力定量预测模型,为降低施工风险和优化施工工艺提供了依据。4完成了物性、岩性影响岩石力学参数的因素分析,找出了各影响因素和岩石力学参数之间的关系,为从机理上解释酸化预处理降低破裂压力提供了理论基础;从微观元素的角度阐述了单矿物与酸反应的机理;并在此基础上,有效评价了各种矿物的酸敏感性,定量确定了岩石中各矿物的一级反应动力学方程。5完成了不同温度下的酸液类型、酸液浓度、注酸量等一系列砂岩损伤实验,结合岩石力学三轴应力实验,系统揭示了在不同条件下注酸而引起的岩石力学性质变化。6将损伤力学与砂岩酸化相结合,在宏观、微观两个方面认识酸岩反应引起岩石力学参数变化基础上,建立了砂岩损伤力学模型,并对其进行验证,在此基础上定量计算酸化后的破裂压力,有效指导现场施工

The trivalent chromium passivation film based on zincate plating obtained has compact structure with no obvious crack, and excellent anticorrosion performance. Different compositions are detected from the surface to inner film, the surface mainly contains Cr2O3-Cr3-ZnO compound, the inner (1030 nm to surface) composes of Cr2O3-ZnO-Zn.The forming process of passivation film possibly consists of four steps which are zinc dissolution, basic area appearance, gelatiniform film forming and converting to passivation film.

结果表明:锌酸盐镀锌层的三价铬钝化膜表面结构致密、无明显裂纹,具有较好的耐腐蚀性能;这种钝化膜表层与里层的组成不同,表层的组成为Cr2O3-Cr3-ZnO共混物;里层(离表层10~30 nm处)的主要组成为Cr2O3-ZnO-Zn共混物;钝化膜的成膜过程可能包括镀锌层的溶解、碱性薄层的形成、胶状膜的形成和胶状膜转化成钝化膜4个步骤。

The psammoma body mineralization in meningioma is a common type of mineralizationThe analysis of the mineral composition may provide some support information in finding the reason of happening and developing of the diseaseThis paper focuses on the concentric layered structure mineralization in meningiomas, using mineralogical methods, such as HRSEM, ESEM, EDAX, EPMA, HRTEM, XRD and FTIR to systematically investigate the mineral composition, structure and shape of the minerals in psammoma bodies in meningiomasWe have devised a method for preparing the silicon wafer sheet which was used for the ESEM insitu observations and analysisIn this study, we first got the ESEM and HRTEM images of the initial mineralization phase of meningiomasThese images showed that in the early stage of psammoma body mineralization in meningiomas, many mineralized balls composed of octocaphosphate were precipitated on the collagen fibersThese balls continued to grow and aggregate, and were gradually hydrolyzed to become the dahlliteThe continued development of mineralization resulted in the mineralized collagen fibersThe study revealed that the concentric layered structure of the psammoma bodies in meningiomas is formed by the spiral arrangement of the mineralized collagen fibers on which the mineralized grains precipitated.

砂粒体矿化是脑膜瘤中常见的矿化类型,对其形成机理和矿物成分的分析可能会对肿瘤发生、发展的研究提供辅助信息。该研究选取人脑膜瘤中的砂粒体矿化作为研究对象,采用偏光显微镜、环境扫描电镜及能谱、X射线衍射仪、高分辨透射电镜和电子探针对样品的形貌、结构和成分进行测试分析,并以此为依据探讨脑膜瘤中砂粒体的形成机理。研究结果表明矿化的初期为沉淀在胶原纤维上的矿化小球,成分为磷酸八钙;矿化小球不断生长聚集,并逐步水解为碳羟磷灰石晶体,矿化的不断发展致使胶原纤维也发生矿化。砂粒体的同心层状构造是由螺旋状排列的矿化胶原纤维及沉淀在其上的矿化颗粒组成的集合体,而不是多数研究中所述:砂粒体是以坏死细胞残骸为中心由内至外的同心层沉淀。

At the phonological level, foregrounding is fulfilled through the reoccurrence of the identical sound. Nonce-formations, abbreviations, blends and sense-shift attain lexical foregrounding, and the frequent use of the shorts words and numbers also functions. At the syntactic level, foregrounded features are embodied in the frequent use of active voice and quotations, and also the peculiar use of the tenses. Foregrounding at the semantic level principally turns up in the news headlines. It is the use of metaphor, synecdoche, metonymy and pun that helps to bring the potential of the linguistic elements into full play.

从语相层来看,体育新闻报道通过对标点符号的特殊使用、拼写的变异以及排版方式来实现前景化;从音位层来看,前景化靠对同一音素的复现来实现;从词汇层来看,新词的创造、词汇的缩略、混成及旧词新义等实现了对常规语言的偏离,此外,频繁使用短小词和数字也将报道推向前景;句法层上,体育新闻报道则通过对主动语态、引语等的频繁使用和时态的特殊用法来实现前景化;语义层的前景化主要集中在新闻标题中暗喻、提喻、转喻及双关等的使用。

The only difference was that the total content of Cr in passivated film on electrodeposited zinc alloys was higher.

它们的区别在于:合金镀层钝化膜中总铬量较高,膜层完整、致密,镀层/钝化膜界面存在铁系金属的富集层,这是锌基合金镀层钝化膜具有高耐蚀性的主要原因。

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The reasons of iron ions content overproof in grade Ⅱ desalting water system,such as variation water quality,contamination of regenerant , operation adjustment of pretreatment system and switching operation of bed were discussed.

对二级脱盐水系统中铁离子含量超标的原因,如来水水质发生波动、再生剂受到污染、预处理系统操作调整、床体运行切换等进行了论述。

You were hired to drum up new business, so go and do it.

公司雇你招徕新业务,你就做你的事好了。

Who is in possession of this?

这是谁的?