射线透射性

It is very difficult to eliminate these influence factors completely by conventional treatment. Surface properties and surface treatment of ultrafine red phosphorus and MMT and their interface properties with polymer matrices were studied in this thesis. The results were characterized by GC, FTIR, XRD, DTA, TG, XPS, UV, SEM, TEM and other physical and chemical methods. The main contents are as following: 1. The study of factors influencing ultrafine red phosphorus's invariability and phosphine liberation indicated red phosphorus undergone oxidation and dismutation reaction in air, and trace ion of iron, copper and nickel fastened water absorption and oxidation, in which the effect of copper ion was the most, while aluminium and zinc ion could slow down red phosphorus'oxidation, and silver ion had the best effect on red phosphorus moisture absorption. Inhibitors such as aluminium hydroxide, magnesium hydroxide, organic phenol and ferrous potassuim cyanide had a good effect on reducing red phosphorus moisture absorption and restraining phosphine liberation.

本文围绕纳微米材料的表面处理及其在高聚物基体中的应用这一主题，系统地研究了超细红磷和蒙脱土两种常见材料的表面特性、表面处理方法及其与高聚物基体的界面特性，通过气相色谱、红外光谱、X射线衍射、差热、热重、X射线光电子能谱仪、紫外光谱、扫描电镜、透射电镜等现代分析仪器以及其它物理、化学方法对实验结果进行了表征和分析，全文主要内容如下： 1、对影响超细红磷安定性的因素以及磷化氢的缓释研究表明：红磷在空气中发生缓慢氧化、歧化反应，微量的铜、铁、镍等金属离子增加了它的吸水和氧化速度，其中铜离子的作用最为明显，而铝、锌等离子减慢了红磷的氧化速度，银离子对减少红磷的吸湿性效果最好。

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GAPⅡa's agglutination form was observed by scan electron microscope and transmission electron microscope. There were mainly empty and different size globoid form among other forms such as chip, needle and alveolus.

通过扫描电镜和透射电镜观察，GAPⅡa聚集态主要以大小不一的空心球状形式分布于其他如片层、针状和蜂窝状形式之间。X-射线衍射分析结果表明经冻干得到的GAPⅡa粉末结晶度不高，但在结晶区其分子的规整性较高。

In addition, molecular orientation behaviors induced by shearing, electric field and magnetic field were investigated. The space group of the monomers A3EO7 and A9EO7 were determined as P2〓2〓2 and P112/m by means of electron diffraction and X-ray diffraction. Liquid crystalline properties of the monomer and the polymer were studied using DSC, variable X-ray diffraction, TEM and polarized optical microscope. Both monomers exhibit monotropic liquid crystalline behavior, and they also give a metastable phase on the cooling process. The polymer PA9EO7 shows enantiotropic liquid crystalline properties. Thus the rigid polymer backbone is not a fatal defect that completely distorts the packing arrangement of the mesogenic moiety in the side chain liquid crystalline polyacetylene.

结合电子衍射倾转方法和粉末X射线衍射技术，确定了两个液晶小分子A3EO7和A9EO7的晶胞参数和空间群，采用Cerius〓模拟软件，运用分子模拟的方法给出了小分子在晶胞中的排列方式；利用DSC、变温X射线衍射技术和透射电子显微镜研究了小分子和聚合物的液晶态，单体A3EO7和A9EO7表现出单向液晶性质，并且在降温过程中都表现出一个亚稳液晶相或亚稳结晶相，聚合物PA9EO7具有双向液晶性；采用偏光显微镜和X射线平板照相技术，研究了剪切和电场对聚合物分子取向的影响，在不同的液晶态，剪切作用对聚合物PA9EO7具有不同的诱导取向结果，直流电场可以诱导聚合物联苯液晶基元沿施加电场方向取向。

The metallograph, x-ray diffraction, TEM, EMPA and XPS technigues were used to research the microstructure, phase structure, microhardness, composition, Valence of composed elements, internal stress of coatings, and to measure the wear-resistance and resistance to high-temperature oxidation, too.

文中应用金相分析、X-射线衍射法、透射电镜、电子探针显微分析法和X-射线光电子谱法等手段研究了N膜的显微组织、相结构、显微硬度、膜层成分、组成元素的价态和膜层内应力等性能；还测定了铝合金表面的N膜的耐磨性和抗高温氧化性能。

Scanning electron microscopy,transmission electron microscopy,circular dichroism and small-angle X-ray diffraction were used to analyze the aggregation mode of CSG in the organogel phase.A hierarchical self-assembly model was proposed to explain the transition from molecular to primary and secondary structure.It is shown from our results that CSG can aggregate into a micellar fibril nanostructure with high length-to-width ratio which is bundled and entangled to form a three-dimensional(3D) network that immobilize the fluid component probably by surface tension.Moreover,sol-gel polymerization of tetraethoxysilane was carried out using CSG in the gel phase.

通过扫描电镜(ScanningElectron Microscopy，SEM)、透射电镜(Transmission Electron Microscopy，TEM)、圆二色谱(Circular Dichroism，CD)和小角X—射线衍射仪(Small-angle X-rayDiffraction，SAXRD)考察CSG分子自组装行为结果表明，CSG形成的聚集体具有多级结构：首先CSG通过手性堆叠自组装形成直径在9—10nm的细纳米纤维，这些细的纳米纤维再以不规则的六方堆积的方式进行排列，构成直径在40—100nm的粗纳米纤维(即细纳米纤维的&捆束&)，最后粗纳米纤维互相粘连形成三维网络状结构，使有机溶剂&固定&，从而形成凝胶；以CSG有机凝胶为模板，四乙氧基硅烷为前体，通过溶胶—凝胶聚合的方法制备了直径大约为100nm的二氧化硅纳米管。3。

Diffusion mechanism,microstructure and optical properties of Ag/Si multilayerson annealing have been investigated by in situ X-ray diffraction,high-resolutiontransmission electron microscopy and UV-VIS-NIR spectrophotometer,Siliconatoms diffusing along silver grain boundaries is suggested as the main diffusionmechanism.

采用原位X—射线衍射、高分辨透射电镜截面观察和光吸收谱测试等手段研究了退火过程中Ag/Si多层膜的扩散、结构演变及光学性质变化，并与可固溶性金属/Si系多层膜进行了比较。揭示了Si原子沿Ag晶界的扩散为主要的扩散机制。

By transmission electron microscope, selected area electron diffraction, powder X-ray diffraction, differential scanning calorimeter as well as self-devised drainage, the effects of metals on grindability, material size, hydrogen storage capacity and hydriding-dehydriding properties are emphatically researched. Fe、Co、Ni were added in pretreatment process of anthracite and the effects of the added metals are researched, also, the action mechanism of metals is discussed on the basis of experimental results.

通过透射电镜、选区电子衍射，X射线衍射、差式扫描量热分析以及自行设计的排水装置等分析测试手段，着重研究了储氢材料中金属对其可磨性、粒度大小、储氢密度、吸放氢性能等的影响，在无烟煤的预处理过程中添加了Fe、Co、Ni三种金属，研究了所添加金属对材料储氢的影响，并在实验结果的基础上探讨了储氢材料中金属的作用机理。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。