射线透射性

It is very difficult to eliminate these influence factors completely by conventional treatment. Surface properties and surface treatment of ultrafine red phosphorus and MMT and their interface properties with polymer matrices were studied in this thesis. The results were characterized by GC, FTIR, XRD, DTA, TG, XPS, UV, SEM, TEM and other physical and chemical methods. The main contents are as following: 1. The study of factors influencing ultrafine red phosphorus's invariability and phosphine liberation indicated red phosphorus undergone oxidation and dismutation reaction in air, and trace ion of iron, copper and nickel fastened water absorption and oxidation, in which the effect of copper ion was the most, while aluminium and zinc ion could slow down red phosphorus'oxidation, and silver ion had the best effect on red phosphorus moisture absorption. Inhibitors such as aluminium hydroxide, magnesium hydroxide, organic phenol and ferrous potassuim cyanide had a good effect on reducing red phosphorus moisture absorption and restraining phosphine liberation.

本文围绕纳微米材料的表面处理及其在高聚物基体中的应用这一主题，系统地研究了超细红磷和蒙脱土两种常见材料的表面特性、表面处理方法及其与高聚物基体的界面特性，通过气相色谱、红外光谱、X射线衍射、差热、热重、X射线光电子能谱仪、紫外光谱、扫描电镜、透射电镜等现代分析仪器以及其它物理、化学方法对实验结果进行了表征和分析，全文主要内容如下： 1、对影响超细红磷安定性的因素以及磷化氢的缓释研究表明：红磷在空气中发生缓慢氧化、歧化反应，微量的铜、铁、镍等金属离子增加了它的吸水和氧化速度，其中铜离子的作用最为明显，而铝、锌等离子减慢了红磷的氧化速度，银离子对减少红磷的吸湿性效果最好。

The company's main products: color detection instruments: Glossiness Miriam, Miriam color spectrophotometry, standard light source for color light box, transmissioní°Miriam, Miriam orange peel, fresh young tester; surface coating physical properties testing instruments: Coating thickness, wet film thickness, temperature tracker, surface humidity instrument, dewpoint meter, roughness instrument, electric spark pinhole leak detectors; Detect mechanical properties of surface coating equipment: zoned grid, and pencil hardness tester , impact tester, hardness testing sticks, Latvia Law / hydraulic adhesion tester, abrasion tester, cylinder / cone bending tester, cups sudden device, surface tension instruments, scratch pen, indentation hardness tester, etc.; paint coating equipment dedicated category: fineness board, drying time recorder, wet adhesion tester, paint ohmmeter, PH, the coating device, mixer, bead mill, mixer, spray gun, putty detector Miriam, white tester, iron cobalt colorimeter, moisture titrator; viscosity-type equipment: Viscosity Cup, density cup, bubble viscosity tube viscometer, infiltration cup rheometer, viscosity units conversion meter; laboratory standard consumables: Mitsubishi pencil tests, 3M adhesive tape test, RCA tape, rubber, the hiding power test paper for color tubes, microscopes dedicated LED ring light source, transfer ink knife and ink scraper, brush, Color Card, gray cards, zirconia beads, glass beads, pieces of cement mortar, the standard of fly ash, the standard viscosity fluid, stopwatch, chemical industry-standard compilation of manuals, paint paint testing manual; test standard Material: tin plate, steel plate, aluminum sheet, asbestos-cement pressure plate, Eterpan, glass, maple panels, MDF, copper film, polyester film, copper; measuring meter and optical instruments: digital calipers, micrometer, dial gauge a high scale, depth gauge, thickness gauge, diameter gauge, gauge block, magnifiers, microscopes, projectors, video measuring instrument; environmental test equipment: oven, constant temperature and humidity box, hot and cold circulating water bath, salt spray test chamber, high temperature resistance furnace, fluorescent UV aging chamber, xenon lamp aging chamber; electronics equipment: infrared thermometer, multimeter, clamp sheet, thermal imager, temperature and humidity meter; anti-static instruments: static tester, surface resistivity device, flat-panel monitor, anti-static footwear tester, wrist strap tester, body Tester; other types of instruments and equipment: torque tester, temperature and humidity recorder, push pull, the vibrometer, speed instrument, analytical balance, industrial Scale Units, dust particle counter, X-ray fluorescence coating thickness measurement and elemental composition analyzer, and so on.

公司主营产品：外观颜色检测仪器：光泽度仪、分光色差仪、标准光源对色灯箱、透射雾影仪、桔皮仪、鲜映性测试仪；表面涂层物理性能检测仪器：涂层测厚仪、湿膜测厚仪、炉温跟踪仪、表面湿度仪、露点仪、粗糙度仪、电火花针孔检漏仪；表面涂层机械性能检测仪器设备：划格器、铅笔硬度计、冲击试验仪、硬度试验棒、拉脱法/液压式附着力试验仪、耐磨耗试验机、圆柱/圆锥弯曲试验仪、杯突仪、表面张力仪、划痕笔、压痕硬度计等；涂料油漆类专用仪器设备：细度板、干燥时间记录仪、湿附着力耐擦洗试验仪、油漆电阻计、PH计、涂膜器、混合机、珠磨机、搅拌机、喷枪、腻子测定仪仪、白度仪、铁钴比色计、水份滴定仪；粘度类仪器设备：粘度杯、密度杯、气泡粘度管、粘度计、渗透杯、流变仪、粘度单位换算计；实验室标准消耗品：三菱测试铅笔、3M测试胶带、RCA纸带、橡皮条、遮盖力测试纸、对色灯管、显微镜专用LED环型光源、调墨刀、墨铲、狼毫刷、色卡、灰卡、锆珠、玻璃珠、水泥砂浆块、标准粉煤灰、标准粘度液、秒表、化学工业标准汇编手册、涂料油漆测试手册；测试级标准基材：马口铁板、钢板、铝板、石棉水泥加压板、埃特板、玻璃板、枫木面板、中纤板、紫铜片、聚酯膜、铜棒；量具量仪及光学仪器：数显卡尺、千分尺、千分表、高度尺、深度规、厚度规、内径规、量块、放大镜、显微镜、投影仪、影像测量仪；环境测试设备：烘箱、恒温恒湿箱、冷热循环水浴、盐雾试验箱、高温电阻炉、荧光紫外老化试验箱、氙灯老化试验箱；电子类仪器：红外测温仪、万用表、钳形表、热像仪、温湿度仪；防静电仪器：静电测试仪、表面电阻仪、平板监测仪、防静电鞋袜测试仪、手腕带测试仪、人体综合测试仪；其他类仪器设备：扭力测试仪、温湿度记录仪、推拉力计、测振仪、转速仪、分析天平、工业台秤、尘埃粒子计数器、 X-射线荧光涂层测厚和元素成分构成分析仪，等等。

GAPⅡa's agglutination form was observed by scan electron microscope and transmission electron microscope. There were mainly empty and different size globoid form among other forms such as chip, needle and alveolus.

通过扫描电镜和透射电镜观察，GAPⅡa聚集态主要以大小不一的空心球状形式分布于其他如片层、针状和蜂窝状形式之间。X-射线衍射分析结果表明经冻干得到的GAPⅡa粉末结晶度不高，但在结晶区其分子的规整性较高。

In addition, molecular orientation behaviors induced by shearing, electric field and magnetic field were investigated. The space group of the monomers A3EO7 and A9EO7 were determined as P2〓2〓2 and P112/m by means of electron diffraction and X-ray diffraction. Liquid crystalline properties of the monomer and the polymer were studied using DSC, variable X-ray diffraction, TEM and polarized optical microscope. Both monomers exhibit monotropic liquid crystalline behavior, and they also give a metastable phase on the cooling process. The polymer PA9EO7 shows enantiotropic liquid crystalline properties. Thus the rigid polymer backbone is not a fatal defect that completely distorts the packing arrangement of the mesogenic moiety in the side chain liquid crystalline polyacetylene.

结合电子衍射倾转方法和粉末X射线衍射技术，确定了两个液晶小分子A3EO7和A9EO7的晶胞参数和空间群，采用Cerius〓模拟软件，运用分子模拟的方法给出了小分子在晶胞中的排列方式；利用DSC、变温X射线衍射技术和透射电子显微镜研究了小分子和聚合物的液晶态，单体A3EO7和A9EO7表现出单向液晶性质，并且在降温过程中都表现出一个亚稳液晶相或亚稳结晶相，聚合物PA9EO7具有双向液晶性；采用偏光显微镜和X射线平板照相技术，研究了剪切和电场对聚合物分子取向的影响，在不同的液晶态，剪切作用对聚合物PA9EO7具有不同的诱导取向结果，直流电场可以诱导聚合物联苯液晶基元沿施加电场方向取向。

The metallograph, x-ray diffraction, TEM, EMPA and XPS technigues were used to research the microstructure, phase structure, microhardness, composition, Valence of composed elements, internal stress of coatings, and to measure the wear-resistance and resistance to high-temperature oxidation, too.

文中应用金相分析、X-射线衍射法、透射电镜、电子探针显微分析法和X-射线光电子谱法等手段研究了N膜的显微组织、相结构、显微硬度、膜层成分、组成元素的价态和膜层内应力等性能；还测定了铝合金表面的N膜的耐磨性和抗高温氧化性能。

Scanning electron microscopy,transmission electron microscopy,circular dichroism and small-angle X-ray diffraction were used to analyze the aggregation mode of CSG in the organogel phase.A hierarchical self-assembly model was proposed to explain the transition from molecular to primary and secondary structure.It is shown from our results that CSG can aggregate into a micellar fibril nanostructure with high length-to-width ratio which is bundled and entangled to form a three-dimensional(3D) network that immobilize the fluid component probably by surface tension.Moreover,sol-gel polymerization of tetraethoxysilane was carried out using CSG in the gel phase.

通过扫描电镜(ScanningElectron Microscopy，SEM)、透射电镜(Transmission Electron Microscopy，TEM)、圆二色谱(Circular Dichroism，CD)和小角X—射线衍射仪(Small-angle X-rayDiffraction，SAXRD)考察CSG分子自组装行为结果表明，CSG形成的聚集体具有多级结构：首先CSG通过手性堆叠自组装形成直径在9—10nm的细纳米纤维，这些细的纳米纤维再以不规则的六方堆积的方式进行排列，构成直径在40—100nm的粗纳米纤维(即细纳米纤维的&捆束&)，最后粗纳米纤维互相粘连形成三维网络状结构，使有机溶剂&固定&，从而形成凝胶；以CSG有机凝胶为模板，四乙氧基硅烷为前体，通过溶胶—凝胶聚合的方法制备了直径大约为100nm的二氧化硅纳米管。3。

Diffusion mechanism,microstructure and optical properties of Ag/Si multilayerson annealing have been investigated by in situ X-ray diffraction,high-resolutiontransmission electron microscopy and UV-VIS-NIR spectrophotometer,Siliconatoms diffusing along silver grain boundaries is suggested as the main diffusionmechanism.

采用原位X—射线衍射、高分辨透射电镜截面观察和光吸收谱测试等手段研究了退火过程中Ag/Si多层膜的扩散、结构演变及光学性质变化，并与可固溶性金属/Si系多层膜进行了比较。揭示了Si原子沿Ag晶界的扩散为主要的扩散机制。

By transmission electron microscope, selected area electron diffraction, powder X-ray diffraction, differential scanning calorimeter as well as self-devised drainage, the effects of metals on grindability, material size, hydrogen storage capacity and hydriding-dehydriding properties are emphatically researched. Fe、Co、Ni were added in pretreatment process of anthracite and the effects of the added metals are researched, also, the action mechanism of metals is discussed on the basis of experimental results.

通过透射电镜、选区电子衍射，X射线衍射、差式扫描量热分析以及自行设计的排水装置等分析测试手段，着重研究了储氢材料中金属对其可磨性、粒度大小、储氢密度、吸放氢性能等的影响，在无烟煤的预处理过程中添加了Fe、Co、Ni三种金属，研究了所添加金属对材料储氢的影响，并在实验结果的基础上探讨了储氢材料中金属的作用机理。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐