对重

Molecularly imprinted polymer using quercetin as template molecules, methacrylic acid as functional monomers, ethylene glycol dimethacrylate as crosslinking agent were prepared, and the binding sites of MIP were selectively modified with diazomethane.The effects of template molecule concentration, solvent and diazomethane usage on modification were discussed.

以槲皮素为模板分子，甲基丙烯酸为功能单体，乙二醇二甲基丙烯酸酯为交联剂，制备了分子印迹聚合物，并以重氮甲烷为修饰剂，对MIP的结合点进行了选择性修饰，探讨了模板分子浓度、溶剂及重氮甲烷用量等对修饰效果的影响。

Herein, we report the enantioselective total syntheses of slagenins A-C and their antipodes. Starting from readily available ethyl -4-chloro-3-hydroxy-butanonate, elongation of the carbon chain with diazomethane, followed by oxidation of the given α-diazoketone using distilled DMD, afforded a key intermediate α-ketoaldehyde .

本文从方便易得的-4-氯-3-羟基-丁酸乙酯出发，经重氮甲烷延伸碳连、DMD氧化相应的α-重氮酮，制得α-酮醛；该化合物与尿素在氢氟酸作用下，以协同方式非对映选择性的直接构建了cis-四氢呋喃并[2，3-d]咪唑啉-2-酮双环结构，进而合成了天然产物slagenins A、B、和C的对映体。

At first transcriptions of Angela"s classroom discourse have been categorized to show the teacher"s three identities, and then they have been further analyzed in the analytical framework from the perspectives of self reference, modality, topic analysis, politeness and exchange structure, to explore the ways she constructs her identities discursively.

首先，通过对该教师的课堂话语进行分类从而确定该教师所构建的三重身份。然后，主要运用Fairclough的社会身份话语分析模式对她的课堂话语从自我称谓、情态语、话题、礼貌原则和话语交换结构等方面进行剖析，揭示该教师各重身份的话语建构过程。

The results showed that when the concentration of Pb(superscript 2+) was lower than 400 mg/L, effect on the germination root length, bud length, root weight, bud weight, the root activity and the proline content of the garden balsam were not obvious.

结果表明，当Pb(上标 2+)浓度低于400mg/L时，对凤仙花种子的发芽率、发芽势、幼苗的根长、芽长、根重、芽重、根系活力及脯氨酸含量影响不大，当Pb(上标 2+)浓度为800mg/L时，对凤仙花种子才开始表现出明显的抑制作用。

The completely diagonalized Hamiltonian matrixes of order 120 of 3d3/3d7 ions configuration in the trigonal symmetry have been established by irreducible representation method and group theory,taking into account spin-orbit interaction and spin-spin interaction.The ground-state energy levels,the zero-splitting parameter and Jahn-Teller effect of ruby crystal were calculated with the matrixes.

应用不可约张量方法和群的理论构造了三角对称晶场中考虑自旋-轨道相互作用，自旋-自旋相互作用的3d3/3d7离子的可完全对角化的120阶微扰哈密顿矩阵，利用该矩阵计算了红宝石晶体的基态能级、零场分裂参量和Jahn-Teller效应，研究了自旋-轨道的自旋二重态对基态能级的贡献，证明其二重态对基态能级的贡献是不可忽略的，理论计算值与实验值相符合。

This project also obtained several limit theorems for some important dependent random variables and stochastic processes, such as the Strassen law of the iterated logarithm for negatively dependent random variables, strong limit theorems for mixing random vectors in Banach spaces, sample path properties for two-parameter fractional Wiener processes, and so on.

随机环境中的随机变量与随机过程的研究在国内外相当活跃，本项目主要研究它们的极限性质，着重研究了随机风景中随机变量与随机过程的极限性质，主要取得了以下几个结果：首先对简单对称的Kesten-Spitzer随机游动在低阶矩的条件下给出了强逼近，大大减弱了前人要求任意阶矩的条件，然后对独立风景中的一般随机变量给出了强逼近的一般性结果，由此导出在风景和随机变量都只具有低阶矩的条件下的独立但不同分布、混合相依变量的强逼近，在只有弱高于二阶矩的条件下得到了重相对数律和弱收敛；给出了连续时间参数的Brown风景中Brown运动和稳定风景中稳定过程的滞后增量和连续模等精确样本轨道性质；同时给出了一些重要的相依随机变量和过程的若干极限定理，如负相关随机变量的Strassen重对数律、抽象空间上混合相依变量的一些强极限定理成立的充分必要条件、两参数分数Wiener过程的样本轨道性质等。

The protocol for the detections of all the AIV isolates, the H5-subtype and the optimization of reactions were studied with a H5-subtype reference isolate BSG1. A 229bp-band of AIV specific and a 380bp-band of H5 subtype specific were amplified individually with the designed primers of AIV specific and H5-subtype specific respectively by the developed RT-PCR technique from isolate BSG1. A double-PCR was also developed which can detect all the AIVs and identify the H5-subtype AIVs. The results of specificity experiment showed that there was no specific band could be amplified with the samples of Newcastle disease virus, infectious bronchitis virus, infectious laryngotracheitis virus, egg drop syndrome virus and infectious bursal disease virus.

结果应用通用引物可从BSG1毒株扩增到与预计大小相符的229bp AIV特异性片段，应用H5亚型鉴定引物则可从BSG1毒株扩增到与预计大小相符的380bp H5亚型特异性片段；在此基础上建立了可检测所有AIV毒株以及可同时进行H5亚型毒株鉴定的二重RT-PCR方法；检测方法的特异性试验结果表明，该方法对新城疫病毒、传染性支气管炎病毒、传染性喉气管炎病毒、产蛋下降综合症、传染性法氏囊病毒无交叉反应；检测方法的敏感性试验结果表明，通用引物扩增、H5亚型特异性引物扩增以及二重PCR扩增反应的组织样品总RNA的最低检出量分别为0.0217μg、0.0217μg和2.17μg；对20份临床样品检测中，有10份为AIV阳性，其中有5份为H5亚型病毒阳性。

Three QTLs detected for maximum adventitious root length in solution culture, total root dry weight in both solution culture and paper culture accounted for about 20%, 23% and 13% of the total variations, respectively.

其中溶液培养中的最长不定根长、总根干重和旱作培养中的总根干重检测到的QTLs位点对总变异的贡献率分别为 2 0 %、2 3 %和 13 %左右；旱作培养中的最长不定根长、不定根数、根冠比和溶液培养中的根冠比仅检测到上位性位点，对表型变异的贡献率在 12 %～ 61%之间。

In the experiment, the study on result of measurement of COD by potassium dichromate method has been conducted in the aspect of impact and application scope, proposing the method of measuring low COD in waste water of high chlorine and putting forward new comment on its influence factor.

本试验采用重铬酸钾标准法对COD测定结果的影响程度与适用范围进行了探索，提出了用低浓度重铬酸钾氧化法测定含高氯根废水中低COD的方法，对其影响因素提出新的看法。

On the basis of nonlinear FEA code ANSYS/LS-DYNA, rail rolling process of universal rolling unit were simulated by 3D large deformation thermal-mechanical coupled elastic-plastic FEM. And the deformation shape of the work piece, deformation parameters and cross dimensions for each pass were obtained and stress,stain distribution and metal flow in rolling process of typical passes were analyzed in detail. Analyzed typical pass stress and strain distribute, rolling stress and deforming in universal pass last groove in detail,discussed the effect regularity of residual stress distribution and size to safely using rail, detailed to expound universal pass to railhead tread circular arc process.

本文基于ANSYS/LS-DYNA非线性显式有限元软件，以60kg/m的重轨为研究对象，采用全三维弹塑性热力耦合的有限元方法研究了重轨在万能轧机组中的变形过程，得到了轧件在孔型中的延伸情况、各道次轧件的变形参数，分析了典型道次的应力、应变分布，并详细分析了全万能成品孔型中轧件受力和变形情况，讨论了残余应力的分布及大小对钢轨安全使用的影响规律，详细地阐述了全万能成品孔型对轨头踏面圆弧的加工过程。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。