对苯二胺

So it has made the great progress. The method studied in this research from o-Dichlorobenzene is a ideal route to synthesize 2,4- dichlorofluorobenzene, which has temperate condition easy to control,safe process,low cost and good quality of products; The method of Phase transfer catalysis fluorination without solvent is better than present technology in presence of DMSO as solvent in many aspects; In a word,it is worth being promoted by the domestic correlative factories.

本课题所研究的以邻二氯苯为原料的2，4-二氯氟苯合成路线反应条件温和，工艺容易控制，生产安全，而且产品质量好，是比较理想的合成路线；以季胺盐为催化剂的无溶剂相转移催化氟化法与溶剂法相比具有明显的优势；通过实验确定的工艺条件对工业化生产有重要的指导意义，可提高以邻二氯苯为原料的工艺路线的市场竞争力。

Off-line HPLC coupled with MS gives the result that 4-chlorophenyl urea and 2-chloro-N-(4-chlorophenyl) benzamide are two photoproducts. In comparison with their retention times and UV specta with those of standards, some other photoproducts identified are 2-chloro benzamide, 4-chlorophenyl urea and 4-chloro aniline.

收集光解产物各级分，采用直接进样法在MS上测得其中的二种光解产物为对氯苯基脲和N-邻氯苯甲酰胺：通过与标样在同样HPLC条件下的保留时间和UV吸收光谱相对照，证明产物中存在有邻氯苯甲酰胺、对氯苯基脲和对氯苯胺等。

Taking 4-bromobenzaldehyde, acetic, benzaldehyde and ammonium acetate as major raw material, the 4, 5-bis(4-bromophenyl)-2-phenyl-1H-imidazole was synthesized by means of catalysis, oxidation and Debus cycloaddition reaction.

以对溴苯甲醛为原料通过催化，氧化生成1，2-二（4'-溴苯基）乙二酮，再以其与苯甲醛、醋酸胺和醋酸通过德布斯法合成2-苯基－4，5-二（4'-溴基苯基）咪唑。

To synthesize the octreotide, Phe-Leu-Glu-Glu-Leu and C_(15)H_(31)-CO-Lys-Thr -Thr-Lys-Ser peptides, the strategies are as followings: Fmoc- group as protective group for α-NH_2; TBTU, DIEA and HOBt as coupling reagent; and ethanedithiol -phenol - thioanisole - H_2O - TFA ( 2.5:5:5:5:82.5 , V/V ) as cleaving solution.

采用Fmoc固相合成法，以苯并三哗四甲基脲四氟硼酸盐、二异丙基乙胺和1-羟基苯骈三氮唑为缩合剂；苯酚—乙二硫醇—苯甲硫醚—水—三氟乙酸(5：5：2.5：5：82.5，V/V)为切割试剂，合成了奥曲肽、Phe-Leu-Glu-Glu-Leu及C_(15)H_(31)-CO-Lys-Thr-Thr-Lys-Ser三种小分子多肽，并对奥曲肽的合成规模进行了放大。

Control of QR barnyardgrass was also studied in this paper. Butachlor, cyhalofop-butyl, oxyfluorfen, pretilachlor, mefenacet and oxyfluorfen plus quinclorac gave adequate control of QR barnyardgrass, however, butachlor in combination with quinclorac and quinclorac plus piperonyl butoxide or agrco were not effective for control of QS barnyardgrass.

本论文还对QR稗草的治理进行了研究，结果表明：丁草胺、千金、果尔、扫茀特、苯噻草胺单剂及果尔和二氯喹啉酸混用能有效的防治二氯喹啉酸抗性稗草，而丁草胺和二氯喹啉酸混用、二氯喹啉酸和增效醚及二氯喹啉酸和表面活性剂蜡混用不能有效的防治QR稗草。

The effects of imidization method,coagulation bath and temperature were studied on the structure and separation performance of polyimide membrane,prepared by using pyromellitic dianhidride and 4,4′-oxydianiline as raw materials.

针对以均苯四甲酸二酐和4， 4′-二氨基二苯醚为原料合成聚酰亚胺的过程，研究了亚胺化方法、凝胶浴组成与温度等条件对膜的结构和分离性能的影响。

Ultra-thin freestanding polyimide films of 100 nm thickness were formed by sequential evaporation of 4,4'-diaminodiphenyl ether and pyromellitic dianhydride precursor monomers followed by a thermal treatment of 150 ℃ 1 h and 350 ℃ 2 h.

采用分层蒸镀法，在玻璃基片上依次蒸镀二氨基二苯醚和均苯四甲酸二酐两种单体，然后在空气环境中对样品进行不同温度和时间的热亚胺化处理，使二者在交界面上反应生成聚酰亚胺。

They were two new compounds, [cyclo(Pro-Val-Phe-Phe-Pro-Val-Phe-Ser-Leu),7],[2-N-(1-methoxycarbonylethyl)guanosine, 10], and eight known compounds,(p-hydroxybenzoic acid, 1),(methyl succinate, 2),(russulaceramide, 3),(phenylalanine, 4),(guanine, 5),(β-carboline, 6),(uridine, 8), and (adenosine, 9). All the compounds were isolated from Amanita exitialis for the first time.

分别为：对羟基苯甲酸(p-hydroxybenzoic acid，1)、丁二酸二甲酯(methyl succinate，2)、神经酰胺(russulaceramide，3)、苯丙氨酸（phenylalanine，4）、鸟嘌呤核苷(guanine，5)、β-咔啉(β-carboline，6)、环（脯氨酸-缬氨酸-苯丙氨酸-苯丙氨酸-脯氨酸-缬氨酸-苯丙氨酸-丝氨酸-亮氨酸） [cyclo(Pro-Val-Phe-Phe-Pro-Val-Phe-Ser-Leu)，7]、尿嘧啶核苷(uridine，8)、腺嘌呤核苷(adenosine，9)、2-N-(1-甲氧羰基乙基)鸟苷[2-N-(1-Methoxycarbonylethyl)guanosine， 10]。10个化合物均为首次从致命鹅膏中分离得到，其中化合物7和10为新化合物。

Cellulose benzoate,the degree of substitution of which was calculated from the content of C determined by element analysis,was prepared from microcrystalline celluloseand benzoyl chloride under heterogeneous condition and characterized by FT-IR and~1H-NMR.

研究了微晶纤维素和苯甲酰氯在多相条件下合成制备纤维素苯甲酸酯的反应，通过元素分析所得碳的质量百分含量计算了产物的取代度，并系统研究了吡啶与N，N-二甲基乙酰胺或与三乙胺混合反应溶剂、苯甲酰氯与纤维素羟基的摩尔比r、反应温度和反应时间对D S的影响，用FT-IR和1H-NM R对产物进行了表征。

Tris-(1-aziridinyl)- phosphine oxide and 2-[bis-(2-chloroethyl)-amino]-tetrahydro-1, 3, 2-oxazaphospholidine-2-oxide(Ⅲ, B-518) possess inhibitory action against a variety of animal tumours and have been used clinically. Recently, bis-(1-aziridinyl)-phosphinyl carbamic acid ethyl ester(Ⅱ, AB-100) was found to possess significant activity with low toxicity on experimental animal tumours.

双(2-氯乙基)氨基磷酰二氯与乙烯亚胺在脱水苯或对氧六环中并在三乙胺的存在下进行缩合，生成N，N-双(2-氯乙基)-N′，N-二乙烯基-磷酰胺；与双巯基或双氨基化合物作用，则生成相应的环状磷酰胺、磷酰胺酯以及磷酰胺硫代酯氮芥类化合物。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。