对硫磷

The Quadratic-Orthogonal-Rotation-Combination is used to analysis the effect of Nitrogen, Phosphate,Kainite, Sulphur, Lemon acid and BR in this study.

本试验采用二次正交旋转组合设计对氮、磷、钾、硫、柠檬酸、油菜素内酯进行分析。

Results show that, by using thionyl chloride and N,N-dimethyl formamide as chlorinating reagent and dichloromethane as solvent and taking -15℃ as reaction temperature, Z-iomer crystals with pale white color and stable to temperature can be obtained with an overall yield of 70%.

以2-（2-氨基噻唑－4-基）－2-甲氧亚氨基乙酸为原料，经盐酸化、氯代等反应合成了Z-2-（2-氨基噻唑－4-基）－2-甲氧亚氨基乙酰氯盐酸盐；氯代时以用亚硫酰氯和N，N-二甲基甲酰胺的混合物代替五氯化磷作氯化剂，并考察了温度和溶剂对氯代产物中Z-异构体和E-异构体收率的影响。

CH3OH could attack the phosphor atom in 1,3,2-dioxaphopholane of compiound (1) to give O-methyl O-hydroxyethyl-O-phthalimidoethyl thiophosphate in 85% yield; in the presence of potassium hydroxide aryl selenol could attack the carbon atom in 1,3,2-diox-aphopholane of the cyclic phospholipid conjugate of N^1-(2-furanidyl)-N^3--5-fluorouracil to give the corresponding product of ring-opening in high yields.

在室温下，以异丙醇作溶剂，苯硒酚与化合物2不反应。在氢氧化钾存在下，以异丙醇／水作溶剂（体积比20：1，在室温下，硒酚可以有效地进攻中化合物2中1，3，2-二氧磷杂环戊烷中的碳原子生成相应的开环产物。按照这一反应条件，顺利实现了硒酚对N^1-（2-呋喃基）-N^3-羟烷基-5-氟脲嘧啶硫代环甘油磷脂缀合物的亲核开环，生成甘油骨架的端碳原子上带有芳硒基新颖的磷脂核苷缀合物。

O-(1-Arylseleno-3-azido)isopropyl-O-2-(N3-tegafur)alkyl thiophosphate (3a～3f) were obtained via nu-cleophilic ring-opening of sodium azide to 2a～2f in dry DMF at room temperature, and their antitumor activities were tested.

以无水N，N-二甲基甲酰胺作溶剂，室温下，叠氮化钠中对2a～2f进行亲核开环，得到O-(1-芳硒基-3-叠氮基)异丙基-O-2-(N3-替加氟)乙基硫代磷酯。

The thermal decomposition kinetics of the N , N′-bis(5,5-dimethyl-2-phospha-2-thio-1,3-di- oxan-2-yl)ethylenediamine in air were studied by TG-DTG techniques. The kinetic parameters of the decomposition process for the title compound in the two main thermal decomposition steps were calculated through the Friedman and Flynn-Wall-Ozawa methods and the thermal decomposition mechanism of DPTDEDA was also studied with the Coats-Redfern and Achar methods.

以TG-DTG为手段，研究了 N ， N ′-二(5，5-二甲基-2-磷杂-2-硫代-1，3-二噁烷-2-基)乙二胺在空气中的热分解动力学，利用Friedman法、Flynn-Wall-Ozawa法对DPTDEDA进行了动力学分析，求出了该物质两个主要的热分解阶段的热分解动力学参数，同时利用Coats-Redfern法、Achar法研究了该物质的热分解机理。

Since its establishment 10 years, has the gold, platinum palladium, iron, manganese, copper, lead and zinc, bauxite, rare earth, coal, phosphorus, pyrite, glauberite, bentonite, asbestos, gypsum, quartz sandstone and limestone , Sand shale, granite, marble and building materials Bittern, mineral water, hot springs and many other items were assessed.

公司成立十年以来，已对金、铂钯、铁、锰、铜、铅锌、铝土、稀土、煤、磷、硫铁矿、钙芒硝、膨润土、石棉、石膏、石英砂岩、石灰石、砂泥岩、花岗石、大理石建材及盐卤、矿泉水、温泉等众多项目进行了评估。

Chlorpyrifos mehtyl with different dosages of 3,5,10 mg/kg compared with malathion 15 mg/kg in grain silo,each contented 40 thousand kilograms of rice was studied.To be sprayed by machine when loading to silo and to be observed two years through all experiment,the effective control to sitophilus zeamais of chlorpyrifos mehtyl 5 mg/kg can be protected more than six months,and 10 mg/kg over one year.

报道了甲基毒死碑(化学名称为二甲基O-3，5，6-三氯-2-吡啶基硫逐磷酸酯)3、5、10 mg/kg不同剂量，以防虫磷15 mg/kg作比较，在立筒库星仓内，每筒40000 kg稻谷，机械喷雾法处理，储藏二年，经生物测定对玉米象药效，甲基毒死蜱5 mg/kg可达半年以上，10 mg/kg可达一年以上防护期。

It is researched about the department of thiobacillus ferrooxidans and soaking phosphorus by experimentations.

本文主要是通过实验对氧化亚铁硫杆菌的分离纯化以及浸磷的初步研究。

The oil-saving agent has simple ingredients, does not contain any metal salt as well as halogen, nitrogen, sulfur, phosphor and the like, and does not cause damage to equipment and environment.

这种节油剂成分简单、不含任何金属盐、不含卤素及氮、硫、磷等元素，不会对设备和环境造成危害。

Melting point 3410 ℃, boiling point 560 ℃, relative density of 1935, F the external electronic structure of 5d46s2, in the chemical reaction time is very easy to lose 1-6 electronic, but also can get 1-2 electronic, so oxidation number of 0,± 1,± 2, 3, 4 , 5 and 6, with 6 price of the most stable compounds, such as WO3 does not dissolve in water, the air will form in the tungsten trioxide thin protective layer of tungsten, tungsten with fluorine at room temperature, chemical combination, red hot when there is no moisture and Bromine iodide together, red hot when you can and water reaction WO3, at room temperature reaction of tungsten with aqua regia, but the hot concentrated hydrochloric acid and sulfuric acid can only be played with its weak response, but molten nitrate, nitrite, too Hydrogen peroxide, sulfur steam, steam and other phosphorus can play intense reaction, high temperature can not be carbon, boron and silicon reaction of binary compounds, widely used in industrial tungsten steel and tungsten carbide, pure tungsten filament is used to the system, and X-ray tube Tube heating components, semiconductor components can be prepared tungsten silicide, tungsten industrial production is white or black tungsten ore tungsten ore refining.

熔点3410℃，沸点560℃，相对密度1935，F外围电子结构为5d46s2，在化学反应时很容易丢掉1—6个电子，也能得到1—2个电子，所以氧化数为0、±1、±2、＋3、＋4、＋5和＋6，以＋6价化合物最稳定，如WO3不溶于水，空气中的钨会形成薄层三氧化钨保护层，钨能与氟在室温下化合，红热并无潮气时能与溴、碘化合，红热时还能和水反应生成WO3，室温下钨可与王水反应，但热的浓盐酸和硫酸只能与其起微弱反应，但对熔融的硝酸盐、亚硝酸盐、过氧化氢、硫蒸汽、磷蒸汽等能起激烈反应，高温下不能与碳、硼和硅反应生成二元化合物，工业上广泛使用钨钢和碳化钨，纯钨用来制灯丝、电子管和X射线管的发热元件，硅化钨可制半导体元件，钨工业生产是将白钨矿石或黑钨矿石精炼。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。