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Novel chitosan derivative with long alky groups as the hydrophobic moieties and carboxymethyl groups as the hydrophilic moieties was synthesized. The chemical structure of N-octyl-O, N-carboxymethyl chitosan was characterized via FTIR, 1H NMR and elemental analysis. The physical properties were analyzed with wide angle X-ray diffraction and differential scanning calorimetry.

以天然可生物降解的壳聚糖为原料,通过在壳聚糖6位羟基上引入羧甲基,在2位氨基上引入疏水烷基链,制得N-辛基-O,N-羧甲基壳聚糖两亲性衍生物,分别用FTIR、1H NMR和元素分析等技术对其结构进行表征,用广角X射线衍射和差示扫描量热法对具物理性质进行分析,并考察其在各种溶剂中的溶解性能及其对难溶性药物的增溶能力。

It was observed that the influence of bud and its position on the healing process of grafting unions using hardwood sectioning method, and found that:(1) bud of a scion and its position to the graft unions have no influence on callusing formation of the isolation layers, and the early differentiation of cambia;(2) a scion bud closer to the grafting union would promote the formation of more compacted callus cells and the earlier formation of callus bridges;(3) conduit differentiation in grafting unions of lower-bud scions was later than that of other treatments.

利用滑动切片法对芽子有无及芽位对嫁接愈合过程的影响进行了观察,发现:(1)接芽有无及芽位对隔离层及愈伤组织形成和形成层的早期分化没有影响;(2)芽或去芽的芽位距接口近,可以促进愈伤组织的紧密连接,即愈伤组织桥的形成;(3)低位芽枝嫁接体中导管分化较晚,而其它处理导管的分化几乎是同时发生的,而且导管首先出现于愈伤组织薄壁细胞中。

The four aspects are mainly optimized in this thesis: ABC classification is combined with fuzzy evaluation, which is applied in the inventory classification of automotive parts, and a right model is established for the classification management; the stock is controlled with order point and multistage programming and the flow charts are designed for reducing the inventory cost and assuring the smooth produ

论文主要从四个方面开展优化工作:将ABC分类法与模糊评判法结合,应用到汽车零部件库存分类中,建立合理的库存分类模型,实现货物的分类管理;应用订货点法和多阶段规划法进行库存量的控制,设计方法流程图,实现降低库存成本、保证生产流畅通的目的;以精益管理思想为指导原则建立全新的仓储作业流程,以此提高管理的信息化水平,提高工作效率;应用储位编码方法对货位进行编码,在作业流程中添加分配库位模块,实现货物智能存取功能。

Four research results in the research are provided on the basis of wholly absorbed attention behavior performance including eyes-gazing, concentration as well as completion of orders, attention-testing performance, and multiple attention-testing performance. The collected materials are analyzed throughvisual analyze and Tryon's C statistic. The results of this research are as follows: 1. Attention-training maintains and give rise to samples' attention behavior. 2. Attention-training makes samples' attention-testing performance better. 3. Attention-training has generalization effects on samples' self-instruction and strategies for monitoring and behavior. 4. Attention-training has different effects on samples of different genders.

本研究以专心注意行为表现、自编注意力测验表现、多向度注意力测验表现及班级教师访谈问卷四项结果作为依据,所得的资料以目视分析法及C统计进行分析,所得研究结果如下:一、三位受试者之C统计值达显著(P1.65),显示注意力训练对受试者的专心注意行为具有提升与维持效果;二、三位受试者在四项分测验中,有三项测验之C统计值达显著(P1.65),显示注意力训练对受试者在注意力测验的注意力表现具有提升效果;三、由班级教师访谈问卷分析中得知注意力训练对受试者的自我指导、监控策略与行为具有迁移效果;四、由自编注意力测验结果分析显示,注意力训练对不同性别学生能显现不同的训练效果。

Methods One hundred footprints of 56 children who were cerebral palsy with talipes valgus in the hospital-community-family-based rehabilitation mode were divided into light, middle and heavy types, and they were counted with two footprint-based approaches, and the two approaches were compared with chi-square criterion, and the dependability on consequence of the footprint and lateral X-rays in weight loading were analyzed.

选取56例采用医院-社区-家庭网络化康复模式流程进行康复治疗的脑瘫患儿,其临床诊断的100只外翻足取其足印图,然后应用三线法与比值法将100只外翻足印图划分为轻、中、重度并计数,再对2种方法的测量结果进行χ^2检验;将足印图三线法、比值法划分的轻、中、重度结果分别与负重侧位X线片所测得数据作线性相关分析。

This article studied differences in postpartum fatigue and birth outcomes between women who pushed immediately and those who delayed pushing during the second stage of labor. Data were collected from primiparous women in their 38th to 42nd gestational week who did not receive epidural analgesia during labor and were free of complications during pregnancy. Using a quasi-experimental design, 72 participants selected by convenient sampling were assigned based on individual participant's preference to either an experimental or control group. For the experimental group, pushing was delayed until the point after full cervical dilation at which the mother felt a strong physical pushing reflex, the fetal head had both descended to at least the +1 level in the pelvis and turned to the occiput anterior position, and uterine contractions were at least 30 mmHg. For the control group, the physician instructed mothers to begin pushing after full cervical dilation at the point when the fetal head was in the occiput anterior position and uterine contractions were at least 30 mmHg.

本研究目的在探讨初产妇女第二产程立即用力与延迟用力对产后疲惫及生产结果的影响,收案对象为怀孕38-42周初产妇女、待产期间未施打硬脊膜外麻醉,且怀孕期间无任何合并症,於待产期间向其解释研究目的及收案方法后予以收案,采类实验设计法,以方便取样并依个案之意愿分派於实验组及控制组,实验组於子宫颈完全扩张后等到强烈想用力的感觉、胎头位到达坐骨棘连线下1公分以下、胎头位置转到枕前位、子宫收缩规律强度至少30mmHg才教导向下用力;控制组於子宫颈完全扩张后即教导向下用力,共收案72位。

Error analysis In order to analysis the pose error of the hexapod machine tool, considering the characteristics of the parallel mechanism,"analysis on the error prominency factors for the hexapod machine tool pose error"is proposed. Numerically, the error prominency factor can express the influence on the pose error of the tool resulted from the mechanism parameter error within the whole workspace.

四、位姿误差分析为了定量地对并联机器人机床位姿误差进行分析,结合并联机构的特点,首次提出了&并联机器人机床位姿误差放大因子分析法&,因位姿误差放大因子是反映机床机构参数误差对刀具末端误差影响大小的机床工作空间内的统计值,因此既可作为机床结构参数精度设计的依据又可对机构参数进行优化。

It is well known that the large lattice mismatch (16%) and thermal expansion coefficient mismatch between GaN and sapphire substrate are the main origins of TDs. By new growing technique of LEO, we acquired high quality GaN films almost free of TDs. The stress characteristics in GaN films with MLTB growing technique is dependent on growing systems and conditions, and the changes of stress and dislocation density are rightabout; Combining buffer layers of high temperature and low temperature is first developed to growing GaN films with low dislocation density, and the mechanism of lowering TDs density is that the first buffer layer of high temperature can make nuclear in second buffer layer of low temperature bigger. This technique also can restrain yellow luminescence effectively.

众所周知,晶格失配和热应力失配是GaN异质外延中位错产生的主要原因;为此,我们对几种降低缺陷的MOCVD外延生长方法进行了新的尝试,其中尝试了侧向外延生长技术,得到了低位错密度(小于10〓/cm〓)、高质量的GaN外延层;尝试多低温缓冲层法,发现材料中的应力特性与生长系统和生长条件有关,材料中的应力与位错密度按相反方向变化;首次尝试高低温联合缓冲层法,材料中高温缓冲层可以使随后的低温缓冲层中成核颗粒增大,从而导致随后高温GaN外延膜中位错密度降低,并且能够有效地抑制黄光峰。

Three primer pairs located in psbA~trnK, psbB~psbH and trnR-ACG~trnN-GUU regions were applied in phylogenetic analysis according to Maximum parsimony and Neighbor-joining methods. The consistent results between the phylogenetic analysis and taxonomy indicated the application potential of the three primer pairs in phylogenetic analysis and species identification. However, due to no sequence variation observed in amplified regions between two vegetable soybean varieties (KS5 and KS8), two cowpea subspecies (Vigna unguiculata ssp. cylindrica and Vigna unguiculata ssp. sesquipedalis), and among three rice varieties (TNG67, TK9, and TCS10), the three primer pairs are not effective in identifying variation within species.

选择其中三组引子对(基因体位置为psbA~trnK、psbB~psbH及trnR-ACG~trnN-GUU)增幅片段之序列进行亲缘分析,以最大简约法及邻接法之分群结果皆与目前植物分类相符,故三组引子对在物种间亲缘关系分析及物种鉴定上都有不错的效果,位於psbA~trnK及psbB~psbH之引子对效果尤佳,但是三组引子对在物种内变异的辨识效果不甚理想,在两个毛豆品种间(高雄5号与高雄8号)、两个豇豆亚种间及三个水稻品种间(台农67号、台稉9号与台中秈10号)的增幅片段没有明显差异存在。

And at the basis of analysis of basic theories, the paper construes some problems in practice, including onus probandi in the sue, effectiveness of subrogation to the creditors, the limit of subrogation and so on. Finally, this paper puts forward proposals about legislation administration and judicature with a view to consummating relevant legal system in China.

同时,在分析代位权诉讼中的基本理论问题的基础上,就我国债权代位权制度审判实务中存在的举证责任、代位权行使对债权人的效力、债务人的处分权限制和代位权制度与民诉法上的代位强制执行制度适用冲突等问题进行分析,并在对立法、执法、司法等方面提出对策建议,以求发挥该制度在司法实践中的现实作用。

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