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The catalytic activities of some coordination polymers in synthesis of DPC from oxidative carbonylation of phenol were investigated. Palladium complex Pd(C_2O_4)·0.5(C_4H_8N_2) has better catalytic activity in the typical reaction condition, it was synthesized with PdCl_2, oxalic acid and piperazine hexahydrate by solvothermal method under low temperature and characterized by IR, EA and TG.

以一些配位聚合物作为主催化剂考察它们在苯酚氧化羰基化生成碳酸二苯酯反应中的催化活性,经过比较,筛选出配位聚合物Pd(C_2O_4)·0.5(C_4H_8N_2)(在低温条件下以溶剂热法合成),采用IR、TG,EA和比表面分析技术对它进行了表征。

Ice in front of a friend wrote a law I wrote again on the "Austrian law is also operator of the" article, I just want to say, brother, I'll wait for you to reach this height, welcome to spray, but if you insist on ice law if, in the 80 before, S4 shoulder for you may just be a dream, of course, and perhaps this is just your Trumpet Master, you are already a resolution of other bright, but Master, you created a number of Master Honorary kill, no more than 100,000?

前面有一位冰法朋友写了一遍关于我写的"奥法也是人操作的"的文章,我只想说,兄弟,等你到达了我这高度,欢迎来喷,但如果你现在是坚持冰法的话,在80级前,S4肩对你来说可能只是个梦,当然,可能这法师只是你的小号,你其它的号早已风光无限,但就法师而言,你的法师制造了多少个荣誉击杀,超过十万没?

The close loop equation is used for the positional posture analysis of the output piece of space 3-RPS parallel mechanism and the forward displacement of the mechanism is educed to acquire the positional posture of output piece.

应用闭合回路方程法对空间3-RPS并联机构的输出件的位姿进行分析,推导出该机构的运动学正解,获得了输出件的位姿,给出该机构位姿分析的数值仿真实例。

By means of UV-vis spectrophotometer, the complex abilities of calix [4] arene ligands with metal ions were researched, and the effect of solvent systems was discussed.

使用紫外-可见分光光度法研究了杯[4]芳烃配体与金属离子的络合性质,并考虑了溶剂对配体与金属离子配位的影响,评价了杯[4]芳烃的不同取代基对过渡金属离子及稀土离子的配位作用。

WT5"HZMethod [WT5"BZ]The cephalogram of 18 untreated growing children were studied with the method of mandibular structural superimposition.

在 10岁和 13岁分别拍摄X线头颅侧位片,对每名儿童的前后两张头颅侧位片运用下颌结构重叠法进行研究。

One mixed-ligand complex ofnH2Otpa=terephthalate, tripy=4'-(4methyoxyphenyl-2,2':6',2-terpyridine was synthesized and characterized by IR, elemental analysis and thermo-gravimetric analysis. The crystal structure of the product was established by single-crystal X-ray diffraction.

采用水热法合成了新的维链状锌的配位聚合物nH2O(tpa=对苯二甲酸,tripy=4'-(4-甲氧基苯基)-2,2':6',2-三联吡啶),通过红外光谱和元素分析对该配位聚合物进行了结构表征,用X射线单晶衍射测定了晶体结构。

Based on the evaluation of rock mechanics properties of undrilling formation, a fuzzy optimization model for selecting the best similar layers with the same rock mechanics properties was established by applying theory of fuzzy optimization. Firstly the best similar layer located the undrilled area was chosen by the model. Secondly the performance of the bit used in the selected layer was evaluated by economic benefit index.

该方法在待钻地层岩石力学性质评价的基础上,首先应用模糊优选理论建立了地层岩石力学性质相似层位的模糊优选模型,用其进行相似层位的优选,然后应用经济效益指数法对相似层位的钻头性能进行评价,最后给出合理的钻头选型结果。

The experimental results showed that there were higher yield and bromine content when the bromine/peroxides method was used.

采用溴/过氧化物法和NBS法对五溴甲苯进行苄位溴化,合成了五溴苄基溴,比较了两种方法的优缺点。

To introduce the mould level measurement and automatic control for the thin slab continuous caster in Lanzhou Iron and Steel Plant, put emphasis on the working principle, technical features, installation and maintenance of the laser measurement system and simply describe the automatic control of the mould level.

介绍兰州钢厂薄板坯连铸结晶器液位测量与自动控制,重点介绍激光法测量的工作原理、技术特点、安装和维护,并对液位自动控制作了简要介绍。

This paper describes the technical features, process principle and process flow of that technique, putting emphasis on the implementation procedure of hole position arrangement, measuring control, boring and hole completion, grouting sequence, pressure treatment and hole seal. It discusses key points of construction quality control, analyzes problems occurred during the construction and puts forward treatment measures.

文章介绍了袖阀管法注浆技术特点、工艺原理及工艺流程,重点从孔位布置、测量控制、开孔与成孔、注浆顺序和压力、封孔处理等方面介绍了袖阀管法注浆实施过程,论述了质量控制要点,对施工过程中出现的问题进行了分析,并提出了处理措施。

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