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At room temperature 1H NMR and 2H NMR spectra of each of the above mentioned compounds were singlets with different line widths which increased with decreasing temperature.

室温下被吸附的上述各种化合物的~1H NMR及~2H NMR谱均为一条线宽不同的单峰,且随温度下降而增宽。

12 Combination type appliances such as can opener/knife sharpeners are to be tested individually for each function; the

联合型器具,将按每一种功能独立进行测试;每个测试均从室温开始测试,除非一种功能测试立即接

The common ultrasonic clean machine was used to prepare nanocrystalline selenides at room temperature and nanocrystalline Ag〓Se, CuSe and PbSe were prepared by this method.

提出了采用普通的超声清洗机制备纳米硒化物的室温制备技术,分别制得了Ag〓Se、CuSe和PbSe等硒化物纳米晶。

The millimetersized tubular crystal selenium was first prepared. By studying the process of treating selenium in ethylenediamine, we proposed the mechanism of the preparation of selenides under solvothermal condition. The selenides came into being from the reaction of metal ions with Se〓, which was obtained by the amine attacking selenium. Moreover, a new precursor to prepare nanocrystalline selenides at room temperature was obtained. From this precursor, we have prepared nanocrystalline silver selenides, copper selenides, lead selenides and cadmium selenides nanorods.

首次报道了采用溶剂热处理的方法制备出厘米尺度的管状结构硒晶体;通过对硒粉在乙二胺中的溶剂热研究,初步探讨了以单质硒为硒源的溶剂热合成硒化物的反应机理应是硒受胺类的亲核进攻变成Se〓而进一步形成相应的硒化物;获得了合成硒化物纳米晶的前驱物,并在室温条件下合成了硒化银、硒化铜、硒化铅纳米晶和硒化镉纳米棒等。

Under atmospheric pressure, binary nanocrystalline sulfides and selenides such as CdS、CdSe、PbS、 PbSe、Cu〓Se、Ag〓S、Ag〓Se、SnSe are obtained at room temperature; nanocrystalline CdTe and PbTe are obtained by heating. Nanocrystalline NiSe〓、CoSe〓 and FeTe〓 are obtained by hydrothermal conditions.

根据硫、硒歧化的碱溶液与碲歧化的碱溶液稳定性的不同,发现在室温条件下可成功获得CdS、CdSe、PbS、PbSe、Cu〓Se、Ag〓S、Ag〓Se、SnSe等二元硫化物与硒化物纳米晶;加热条件下可成功获得CdTe与PbTe纳米晶;而NiSe〓、CoSe〓及FeTe〓的合成则要在水热条件下进行。

The results show that the ambient oxygen and ratio of the materials are critical to microwave sin...

结果表明:利用微波反应烧结β′-Sialon,原料配比和炉气中氧含量很关键;微波反应合成烧结Z值等于3的β′-Sia-lon的最佳工艺是1500℃、保温90 min,该工艺烧结的材料密度为3.050 g/cm3和室温抗弯强度为150 MPa。

The self-lubricanting coating of nickel-coated graphite was prepared by oxygen-acetylene flame spraying technology and its friction and wear properties at room temperature were studied in a ball on disk test rig.

选用镍包石墨粉末,采用氧-乙炔火焰喷涂技术制备镍包石墨自润滑涂层,在球-盘摩擦磨损试验机上探讨了室温条件下镍包石墨自润滑涂层的摩擦磨损性能。

Results The activity, recovery rate of activity and half-life of immobilized SOD were 333 U/g, 86.32% and 43.8 d respectively. After storage at room temperature for 5 d, the relative activity of SOD was still more than 80%. The optimal reaction temperature of immobilized SOD was 45℃, and the activity retentions after being used for the first and second times were 70.12% and 51.72% respectively. Both the optimal pH values for SOD before and after immobilization were 6, while the Km values were 0.16 and 0.18 mmol/L respectively.

结果 固定化超氧化物歧化酶活力为333U/g,酶活回收率为86.32%,半衰期为43.8d;固定化酶室温保存5d后,相对酶活力仍保持在80%以上,最适反应温度为45℃,使用一次后回收率为70.12%,重复使用两次后回收率为51.72%;固定化酶与溶液酶在pH6时活性最强,Km分别为0.18mmol/L和0.16mmol/L。

The company added that exceptional electrical properties including a volume resistivity of 109 ohm-cm and dielectric strength of 225 volts per mil at room temperature are provided.

该公司还补充说,这种涂层具有优异的电性能。在室温下体电阻率为109Ω/cm和介电强度为225v/mm。

The repulsions and the energy transferring will are increasing with the varying of the temperature for the -phase-difference solitons.

结果表明:在室温基础上,两个同相位孤子波的相互作用随温度变化伴有融合现象,当温度升高到350K时两孤子可融合成一束稳定的孤子波;两个反相孤子相互排斥现象随温度变化而增强;相位差为的两孤子,其相互作用随温度变化过程中有更多的能量转移,同时两孤子间的排斥现象随温度变化而增强。

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With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐,因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。

Closes the eye, the deep breathing, all no longer are the dreams as if......

关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。