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Chapter two 4-Hydroxybenzoic acid is connected with PEG6000 through defoliant DCC at rooom temperature, then the product is refluxed with chloroacetic acid in acetone to afford PEG-bound phenyloxyacetic acid, which is reacted with thionyl chloride, ammonium thiocyanate and arylamines in turn to give PEG-bound disubstituded thioureas. After the cleavage with sodium methoxide in methanol, the eleven disubstituted thioureas are obtained.

第二章 利用PEG6000作载体,通过脱水剂DCC在室温下将对羟基苯甲酸以酯键连接在PEG6000上,再与氯乙酸在较温和的条件下生成PEG6000支载的芳氧乙酸,然后,依次与亚硫酰氯、硫氰酸铵、芳胺反应,生成PEG6000支载的硫脲,最后用甲醇钠的甲醇溶液切割PEG,得到了十一种1,3-二取代硫脲。

The effect of aging temperature and room temperature plastic deformation ratio of thermo-mechanical treatment alloy on material performance process for 2A12 aluminum alloy was investigated.

采用工艺实验研究2A12铝合金形变热处理工艺中时效温度和室温塑性变形量对材料性能的影响。

Tests where in closed case at room temperature 26 degree Celsius.

测试,如在封闭的情况,在室温26摄氏度。

Demineralization in the Trikoflex washing compartment at 60°C to 80°C for approx. 30 to 60

先浸渍脱矿质助剂,然后在小反应箱内室温下保持5分钟

Effects of some major factors on deoxidize rate of silver, such as Mix ratio connection of tartaric acid and glucose, over all concentration of mixed liquid, the pH level, the reaction temperature, the reaction time etc.

考察了酒石酸与葡萄糖的配比关系、还原混合液的总浓度、pH值、反应温度、反应时间对银还原率的影响,得出了酒石酸与葡萄糖、无水乙醇的质量比为1:2.6:1,pH值为12,在室温下放置时间为3-5d,银的还原率大于92.7%的最佳条件,总回收的金属银纯度为98.2%。

The deoxidizer of the invention can be reduced and regenerated below 150 DEG C, and can purify the trace oxygen in the olefin with a carbon atom more than 3 at room temperature to less than 0.05ppm.

本发明的脱氧剂可以在150℃以下还原再生,室温下将C3以上烯烃中的微量氧净化至0.05ppm以下。

A strong and stable room temperature phosphorescence emission was observed from the ternary inclusion complex of α-bromonaphthalene/β-cyclodextrin/hexahydropyridine without deoxygenation from solution in the presence of micro amount of HHP.

微量六氢吡啶存在下,由于三元包络物α-溴代萘/β-环糊精/HHP的形成,不经除氧就可观察到强而稳定的室温磷光发射。

Mechanical twinning is strongly grain size and texture dependance.

研究结果表明,镁合金在室温变形条件下,孪晶在变形的过程中发挥了重要的作用。

The high income and high mucosity of SD depositer (26.5%) could affect the clarification and the stability of the oral liquid.

由于预实验证明生化汤室温粘稠,醇沉物占总浸膏高达26.5%,影响口服液的澄明度及稳定性,采取醇沉工艺进行精制。

The second specific capacity of the charge-discharge with the rate of 0.1C at room temperature of the samples synthesized under the optimized conditions reached 145.7mAh/g, 85.7% of the theoretical capacity, with almost no descension after circulating for 10 times.

优化条件合成出的样品,在室温以0.1C倍率充放电,第二循环放电比容量高达145.7mAh/g,为其理论容量85.7%,且循环十次比容量基本没有衰减,但高倍率充放电时,材料极化较大,容量衰减较快。

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With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐,因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。

Closes the eye, the deep breathing, all no longer are the dreams as if......

关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。