实验法

The experimental procedure were predigested under the condition that did not effect the experimental results by using alkal potassium persulphate oxidation -ultraviolet spectrophotometry to determine the total nitrogen in water sample with first water instead of redistillation non-ammonia water.

经实验证明，用碱性过硫酸钾氧化-紫外分光光度法测定水样中的总N，以一次蒸馏水代替重蒸馏无氨水，既减少了实验操作程序，又不影响测定结果，同时本文确定了最佳实验条件，并对标准样品进行分析，结果理想。

Methods Compared with the ultrasonic extraction and the refluent extraction experiment,colorimetric analysis was used to measure the content of active ingredients.

方法比较超声提取和回流提取实验，用比色法测定有效成分；采用回流提取正交实验，并对实验数据经不同的计算和分析比较优选螃蟹脚的提取工艺条件。

On the basis of the previous results and according to the central composite experimental design principles,the method of response surface method with 3 factors and 3 levels was adopted.then the factors influencing the technological parameters were determined by means of regression analysis.response surface and contour were finally graphed with the extraction rate as the response value.resultsthe optimum conditions of lycium barbarum polysaccharides extraction were as follows:the ratio of material to solvent of 1∶32,extraction temperature of 84℃ and extraction time of 2.3 h,one time extraction.conclusionthe yield of lycium barbarum polysaccharides is 11.10% under the optimum conditions.

方法在单因素实验基础上选取实验因素与水平，根据中心组合（box-benhnken）实验设计原理采用3因素水平的响应面分析法，依据回归分析确定各工艺条件的影响因子，以多糖提取率为响应值作响应面和等高线。结果在分析各个因素的显著性和交互作用后，得出枸杞多糖水浸提的最佳工艺条件为：料液比1∶32；浸提温度84℃；浸提时间2.3h；浸提1次。结论在最佳工艺条件下，枸杞多糖的实际提取率可达11.10%。

In this paper, aiming at the extraction of Sargassum fusiorme polysaccharide, experiment factors and levels were firstly selected by one-factor tests. Next, on the basis of this and according to the Box-Benhnken center-united experimental design principles, the method of response surface analysis with 3 factors and 3 levels was adopted.

针对羊栖菜多糖的提取，通过单因素实验选取实验因素与水平，根据Box Benhnken的中心组合实验设计原理，在单因素试验的基础上采用三因素三水平的响应面分析法，依据回归分析确定各工艺条件的影响因子，以多糖提取率为响应值作响应面和等值线图。

Experiment and flow visualization are conducted in a water-filled cavity which cover the range of Ra=1×10〓----6×10〓 and Pr=3. 3---6. 5. Similarity theorem is applied in analytical investigations. And core region stratification effects to heat transfer are studied. By using scale analysis, temperature and velocity profiles in turbulent natural convection boundary layer are obtained. The results reveals that for turbulent natural convection in enclosures, the bulk of the cavity fluid is essentially statement with thermally stratified temperature and the only substantial motion is that in the boundary layer along four side walls.

在实验方面，作者在高Ra范围内（Ra〓=1×10'~Ra〓=6×10〓，Pr=3.3~6.3）对封闭空间实验台以蒸馏水为介质进行了换热实验与流动显示；在理论分析方面，作者采用相似原理导出了分析解；研究了核心区温度分层规律及其对换热的影响；另外还运用尺度分析法探讨了紊流自然对流边界层温度与速度分布。

S extract had an inhibition effect against Sphaerotheca fuligenea,The inhibition rate was 100% when extract concentration was 20mg/mL and the inhibition rate got to 67.66% even at the concentration of 2.5mg/mL. The extract of E. humifusa had different preventive effects against four strains of S. fuliginea from four districts in Shanghai. The preventive effects on the Qibao and Baoshan were better than those of Nanhui and Qingpu. The microorganism inhibition experiment by filter papers indicated that the extract of E. humifusa had higher inhibition effect against bacteria than on pathogenic fungus. Diameters of the zone of inhibition of salmonellas, Echerichia coli and Staphylococcus aureus were 15.77mm, 12.27mm and 10.53mm respectively. The extract of E. humifusa had a certain effect against Colletotrichum lagenarium, Botrytis cinerea, Rhizoctomia solan and Pyricularia oryza but no effect against Helminthosporium maydis and Gibberella zea. The 4 cation exchange resins and ethanol deposition were used to isolate the active fractions from supernate after alkali deposition.

提取液对黄瓜白粉病菌体外分生孢子萌发抑制实验表明地锦提取液对黄瓜白粉病菌分生孢子的萌发有很好的抑制作用，抑制率随着地锦提取液浓度的增大而增高，当浓度为20mg/mL时，抑制率达到100%，即使在浓度为2.5mg/mL时，抑制率也达到了67.66%；室内盆栽苗期预防性实验表明了地锦提取液对上海4个不同地区的黄瓜白粉病菌均具有不同程度的抑制效果，对七宝和宝山地区的菌株抑制效果优于南汇和青浦地区的菌株；用滤纸片法测定了地锦提取液的抑菌谱，实验结果表明地锦提取液对供试的4种植物病原真菌：黄瓜炭疽病菌、黄瓜灰霉病菌、水稻纹枯病菌和水稻稻瘟病菌均具有一定的抑制效果，而对玉米小斑病菌和小麦赤霉病菌没有抑制效果，对供试的3种人类致病细菌沙门氏菌、大肠杆菌和金黄色葡萄球菌均具有很好抑菌效果，抑菌圈直径分别为：15.77mm， 12.27mm和10.53mm。

Firstly, the theory and knowledge of sparking and burning are briefly introduced. The holistic project of this experiment is designed aiming to the experiment motive. And then the micro-process technique on silicon is chosen. According to the technique, the structure and size of the micro chamber, the spark device, the gas-fired channels are designed. The mask of lithography is produced based on the design. At last, the whole burning room is produced by the techniques of photolithography, deposition, dry etching, wet etching, lift off, etc.

本文首先介绍了点火燃烧的有关原理和基本知识，然后根据提出的实验研究目标，确定了微小空间内点火特性实验总体方案，之后结合拟采用的硅微加工工艺设计确定了微燃烧室、放电点火装置、燃气通道等各部件的结构尺寸，并最终得到光刻用掩膜版图形，最后分别采用光刻、淀积、干法刻蚀、湿法刻蚀、剥离等硅微加工技术完成了实验用微燃烧室的制作。

Based on the experiment, a prediction method of surface tension was provided in this paper.

本文在这种情况下，在国内首次系统的开展了激光散射法测量液体表面张力的理论和实验研究工作，搭建了实验系统，并利用该系统对一些清洁汽车替代燃料的表面张力进行实验研究。

In this thesis, three major achievements were made in theoretical study: conditions and rules for preparing nano-powders by chemical precipitation are analyzed from the point of view of thermodynamics and kinetics, the principle, standards and experimental method for the aqueous dispersion of nano-scaled metal oxide powders were proposed and verified, mathematical model of nano-filming addition of dopants by chemical coprecipitation was established. In experimental research, nm-ZnO, nm-Bi〓O〓, nm-Co〓O〓 and nm-MnO powder with spherical shape, narrow particle size distribution and small particle size were prepared successfully, highly stable and dispersive aqueous suspensoid of nm-ZnO, nm-TiO〓, nm-Co〓O〓 and nm-MnO powder were prepared successfully and surface modification on these nano-powders was also achieved, 0-3 nanocomposite ZnO varistors with nm-ZnO, nm-TiO〓and nm-MnO respectively were prepared successfully by conventional mechanical attrition, and exhibited much better electrical properties than those of conventional varistors.

综上所述，本文在理论研究方面取得了三项成果：（1）从热力学和动力学角度推导并分析了液相化学沉淀法制备纳米粉体的反应条件和规律，（2）提出了纳米氧化物的水分散体系的设计原理、规范和通用实验步骤，（3）提出了共沉淀的数学模型和计算方法；在实验方面所取得的成果有：（1）成功制备了粒度小、分布窄、形貌对称的纳米氧化锌、纳米氧化铋、纳米氧化钴和纳米氧化亚锰，（2）成功地制备了纳米氧化锌、纳米二氧化钛、纳米氧化钴和纳米氧化锰的高稳定分散悬浮液并实现了干粉体的表面改性，（3）成功地进行了纳米氧化锌、纳米二氧化钛和纳米氧化锰对压敏电阻的0—3复合掺杂实验，试样性能远优于常规压敏电阻，为实现压敏电阻的高能高压化提供了新的方法和思路。

To adopt system menstruum deal with fermented products of mycelium from Tremella aurantialba, then mycelium from tremella aurantialba was studied with the clotting time of the thrombogen, the whole blood clotting time in mice and thrombosis experiment in mice.

采用系统溶剂法处理金耳菌丝发酵物，得乙酸乙酯部位、正丁醇部位及水溶部位，通过凝血酶原实验、小鼠凝血实验及小鼠体内血栓形成实验等来筛选具有抗凝血作用的有效部位。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。