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The structural and photocatalytic properties of TiO〓 as well as surface acidity were greatly improved by sulfation. SO〓〓/TiO〓 solid superacid with Hammett constant Ho less than -12.14 was prepared by treating the TiO〓 with 1.0mol. L〓 sulfuric acid solution and then calcining at 450℃ for 3h. When compared to unmodified TiO〓, the SO〓〓/TiO〓 superacid catalyst exhibited higher anatase content, smaller crystal size, higher specific surface area, centralized pore size distribution, and the blue-shifted band edge of uv-vis adsorption spectra. Furthermore, the SO〓〓/TiO〓 superacid also showed excellent reaction activity and stability for CH〓Br photocatalytic decomposition even under the moist reaction conditions. The apparent quantum efficiency of SO〓〓/TiO〓 was 10 times of that of TiO〓 catalyst for the photocatalytic degradation of bromomethane. Therefore, the SO〓〓/TiO〓 superacid catalyst is promising for practical application in environmental remediation.It was found that both L and B acid sites exist on SO〓〓/TiO〓 photocatalyst while only L acid sites on TiO〓 photocatalyst. On the basis of experimental results, the synergistic model of superacidic centers was proposed for SO〓〓/TiO〓 photocatalyst to explain the photocatalytic behavior and the mechanism of superacidifing effects, assuming that the adjacent L and B acid sites induced by SO〓〓 comprise cooperatively the superacidic center on superacid photocatalyst. The group cooperation of the superacidic center could strengthen the surface acidity, increase surface acid sites and the adsorbtion of O〓, promote separation of photogenerated electron-hole pair, enhance the interfacial transfer of charges and reversibility of water adsorption. Consequently the excellent photocatalytic activity, reaction stability and resistibility to humidity of SO〓〓/TiO〓 superacid photocatalyst may attributed to the group cooperated effect of the superacidic center on the photocatalyst.

研究结果表明:SO〓〓与TiO〓表面的结合为螯合式双配位结构;TiO〓光催化剂表面经H〓SO〓浸渍处理后,提高了表面酸性,改善了催化剂结构和光催化性能,当H〓SO〓浸渍浓度为1.0mol.L〓、烧结温度为450℃时,可制得SO〓〓/TiO〓超强酸催化剂(H〓<-12.14),其结构和光催化活性得到明显改善,与TiO〓相比,SO〓〓/TiO〓光催化剂的锐钛矿含量高、晶粒小、BET比表面积大、孔径分布集中、光谱吸收边蓝移,具有优异的光催化氧化活性、稳定性及抗湿性能,光催化降解溴代甲烷的表观量子效率比TiO〓催化剂提高了一个数量级,是一种有实际应用前景的高效光催化剂;由此提出了SO〓〓/TiO〓超强酸催化剂表面集团协同作用的超强酸中心模型,认为在SO〓〓/TiO〓超强酸催化剂表面,由SO〓〓诱导的相邻L酸中心和B酸中心组成了集团协同作用的超强酸中心,其集团协同作用显著地增强了催化剂表面酸性、增大了表面酸量及O〓吸附量、促进了光生电子和空穴的分离及界面电荷转移,具有可逆吸附水的性能,是SO〓〓/TiO〓超强酸催化剂具有优异的光催化氧化活性、很好的活性稳定性及抗湿性能的重要原因。

The apparent quantum efficiency of SO〓〓/TiO〓 was 10 times of that of TiO〓 catalyst for the photocatalytic degradation of bromomethane. Therefore, the SO〓〓/TiO〓 superacid catalyst is promising for practical application in environmental remediation.It was found that both L and B acid sites exist on SO〓〓/TiO〓 photocatalyst while only L acid sites on TiO〓 photocatalyst. On the basis of experimental results, the synergistic model of superacidic centers was proposed for SO〓〓/TiO〓 photocatalyst to explain the photocatalytic behavior and the mechanism of superacidifing effects, assuming that the adjacent L and B acid sites induced by SO〓〓 comprise cooperatively the superacidic center on superacid photocatalyst. The group cooperation of the superacidic center could strengthen the surface acidity, increase surface acid sites and the adsorbtion of O〓, promote separation of photogenerated electron-hole pair, enhance the interfacial transfer of charges and reversibility of water adsorption. Consequently the excellent photocatalytic activity, reaction stability and resistibility to humidity of SO〓〓/TiO〓 superacid photocatalyst may attributed to the group cooperated effect of the superacidic center on the photocatalyst.

研究结果表明:SO〓〓与TiO〓表面的结合为螯合式双配位结构;TiO〓光催化剂表面经H〓SO〓浸渍处理后,提高了表面酸性,改善了催化剂结构和光催化性能,当H〓SO〓浸渍浓度为1.0mol.L〓、烧结温度为450℃时,可制得SO〓〓/TiO〓超强酸催化剂(H〓<-12.14),其结构和光催化活性得到明显改善,与TiO〓相比,SO〓〓/TiO〓光催化剂的锐钛矿含量高、晶粒小、BET比表面积大、孔径分布集中、光谱吸收边蓝移,具有优异的光催化氧化活性、稳定性及抗湿性能,光催化降解溴代甲烷的表观量子效率比TiO〓催化剂提高了一个数量级,是一种有实际应用前景的高效光催化剂;由此提出了SO〓〓/TiO〓超强酸催化剂表面集团协同作用的超强酸中心模型,认为在SO〓〓/TiO〓超强酸催化剂表面,由SO〓〓诱导的相邻L酸中心和B酸中心组成了集团协同作用的超强酸中心,其集团协同作用显著地增强了催化剂表面酸性、增大了表面酸量及O〓吸附量、促进了光生电子和空穴的分离及界面电荷转移,具有可逆吸附水的性能,是SO〓〓/TiO〓超强酸催化剂具有优异的光催化氧化活性、很好的活性稳定性及抗湿性能的重要原因。

Rise and development with the trade of security investment fund,how to use and draws lessons from the fund achievements of the western countries and appraise the system and cany on objective and overall appraisal to the security investment fund of our country rationally,become an important problem put in front of the theory worker and real worker in our country.

随着证券投资基金行业的兴起和发展,如何合理地运用和借鉴西方国家的基金业绩评价体系对我国证券投资基金进行客观全面的评价,成为摆在我国理论工作者和实际工作者面前的一个重要问题。

In practice, however, this advantage is somewhat illusory: Management changes, like marital changes, are painful, time-consuming and chancy.

事实上这种优势有点不太实际,因为更换管理阶层,就像是结束婚姻关系一样,过程是相当地费时痛苦且要看运气。

By practical application,the bidirectional circumrotation/speed adjustment of motor are realized safely and reliably.The products has a small physical volume,fast heat transmission,high efficiency and can operate properly in severe environment.It can enhance the reliability of the drive circuit and the system,and adapt to both military and commercial usage.

经实际应用,该电路不仅安全可靠地实现了电机的双向转动和调速功能,且产品体积小,导热性能好,效率高;还能在恶劣的使用环境下安全工作,提高了驱动电路和系统的可靠性,适合军、民两用。

for carrying out a small physical volume and high reliability of the motor driving and control,by using hip4081 chip and aln hybrid integrated technology,a hybrid integrated technology h bridge circuit based on hip4081 is designed to control bidirectional circumrotation and speed regulation of the motor.by practical application,the bidirectional circumrotation/speed adjustment of motor are realized safely and reliably.the products has a small physical volume,fast heat transmission,high efficiency and can operate properly in severe environment.it can enhance the reliability of the drive circuit and the system,and adapt to both military and commercial usage.

摘 要:为了实现小体积、高可靠的电机驱动与控制,利用hip4081专用芯片和aln厚膜混合集成技术,设计一种基于hip4081的厚膜h桥电机驱动电路,完成了h桥式驱动电路对电机双向转动和调速的控制。经实际应用,该电路不仅安全可靠地实现了电机的双向转动和调速功能,且产品体积小,导热性能好,效率高;还能在恶劣的使用环境下安全工作,提高了驱动电路和系统的可靠性,适合军、民两用。

On the other hand, in few-cloudy and cloudy days, the error was 15.50% and 41.28% respectively which showed that error increases with cloudage.

误差随着云量的增多逐步增大,故模型在少云和多云的天气状况下不能很好地模拟实际情况。

How to collocate , let vegetation protect slope off limits , is the new problem in the actual project .

如何布置,使植被更大限度地发挥&固滩护堤&的作用,是生产实际中提出的新问题。

Rock slopes and colluvial slopes are common natural slopes in mountain areas. For simplicity, the slope stability analysis is often performed by two-dimensional limit equilibrium methods in terms of circular slide surfaces, which are not usually found in rock and colluvial slopes.

岩石边坡及崩积层边坡为山坡地常的自然边坡,许多上述边坡的稳定分析,常简地假设破坏面为圆弧形,采二维的极限平衡法分析软体进动面的安全系计算,此常与实际的况一致。

Furthermore, the article concludes that the combinatory method achieves the best results and possesses the applicable value.

基于此类方法的自动词性标注技术可以较好地满足实际应用的要求。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

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