定量测定

Methods The 100 patients with CI and 107 control subjects without any blood disease or tumors were evaluated by applying the Chart of Typical Behaviors of TABP, meanwhile the endothelin and thrombomodulin contents in plasma of the patients were measured for the mark of the damage of blood vessel endothelium. The CI group, control groups and part of CI group with the same level of blood pressure were subgroup by the result of questionnaire, correlation analysis was made between the amounts of blood markers and ill performance characteristics of TABP.

对100例CI患者和107例无血液病和肿瘤的对照者进行A型行为评定量表测定，并同时对两组人员的血管内皮细胞损伤的血浆标志物内皮素和血栓调节蛋白含量进行测定；再根据A型行为问卷调查结果，分别对CI组和对照组患者，以及在同一血压水平的CI患者按照个体的行为特征进行分组，然后对其血浆标志物浓度进行相关分析。

Methods The 100 patients with CI and 107 control subjects without any blood disease or tumors were evaluated by applying the Chart of Typical Behaviors of TABP, meanwhile the endothelin and thrombomodulin contents in plasma of the patients were measured for the mark of the damage of blood vessel endothelium. The CI group, control groups and part of CI group with the same level of blood pressure were subgroup by the result of questionnaire, correlation analysis was made between the amounts of blood markers and ill performance characteristics of TABP. Results 40% CI patients were TABP.

对100例CI患者和107例无血液病和肿瘤的对照者进行A型行为评定量表测定，并同时对两组人员的血管内皮细胞损伤的血浆标志物内皮素和血栓调节蛋白含量进行测定；再根据A型行为问卷调查结果，分别对CI组和对照组患者，以及在同一血压水平的CI患者按照个体的行为特征进行分组，然后对其血浆标志物浓度进行相关分析。

Macerate 1.0g of the powdered sample with 20.0 ml of chloroform plus 0.3ml of 25％ NH_4 OH in a glassstoppered flask overnight.

本文报道用不含粘合剂的氧化铝薄层，以二甲苯-丙酮-无水乙醇-二乙胺(50：40：10：0.6)为展开剂分离茄科植物中的莨菪碱、东莨菪碱、山莨菪碱、樟柳碱及红古豆碱等五种莨菪烷生物碱，用改良Dragendorff试剂-Wagner试剂(1：1)显色，定量收集莨菪碱、东莨菪碱及山莨菪碱的斑点，莨菪碱和东莨菪碱用氨甲醇洗脱，蒸干洗脱液后分别用pH 5.6及pH 4.5的溴甲酚绿溶液作比色测定；山莨菪碱用4％醋酐氯仿洗脱，蒸干洗脱液后用pH 5.6的溴甲酚绿溶液作比色测定。

The invention discloses a method for measuring seawater chemical oxygen demand by photometry, wherein the seawater exemplar is first pre-processed, then using the basic potassium hypermanganate as reaction system, the potassium permanganate is deacidized quantitatively by organics to produce manganate, using pure water or margin solution as reference ratio, measuring the absorbance an of the manganate at its maximum absorbing wave length 430 nm, drafting the A-COD value operating curve, obtaining the concentration of the organics in the water, i.e.

本发明公开了一种对海水化学需氧量进行测定的光度测定法，该方法首先将海水样品进行预处理，再以碱性高锰酸钾为反应体系，这样海水中的有机物在强碱性介质中与过量的高锰酸钾迅速反应，高锰酸钾被有机物定量还原后生成锰酸盐，以纯水或空白溶液作参比，在锰酸盐的最大吸收波长430nm处测其吸光度A，该吸光度A与海水样品中的有机物的含量具有正相关关系。

All the methods used now have a common technical difficulty: The presence of large amount of uranium makes unacceptable interferences to the determination of neptunium. A separation procedure is absolutely necessary to separate neptunium from uranium completely.

国内一直没有一个比较理想的准确、灵敏的方法，解决铀产品中微量镎的测定问题，主要原因是现有的方法存在一个共同的技术难点：常量的铀对微量镎的测定干扰很大，必须要将常量铀与微量镎定量分离。

The metalloproteins which are widely distributed in vivo are very important target molecules of NO. A new Y/〓 reaction system which can form Y-NO bond has been established and has been used to measure the NO affinity of metalloporphyrins as metalloprotein models. Three kind of bond energies of the Co-NO bonds in series of cobalt nitrosyl tetraphenylporphyrins have been determined by thermodynamic cycles combined with calorimetric measurements and relevant electrochemical data.

本文以金属卟啉模拟体内重要的NO靶分子金属蛋白，通过确立新的适于量热和电化学测定的Y／〓成Y-NO键反应体系，利用合适的热力学循环，建立了新的适于金属卟啉体系的NO亲合势的测定方法，得到了苯腈中系列亚硝基四苯基钴卟啉Co-NO键的键能，即钴卟啉NO亲合势的定量标度，以表征钴卟啉的NO结合能力。

Three kind of bond energies of the Co-NO bonds in series of cobalt nitrosyl tetraphenylporphyrins have been determined by thermodynamic cycles combined with calorimetric measurements and relevant electrochemical data.

本文以金属卟啉模拟体内重要的NO靶分子金属蛋白，通过确立新的适于量热和电化学测定的Y／〓成Y-NO键反应体系，利用合适的热力学循环，建立了新的适于金属卟啉体系的NO亲合势的测定方法，得到了苯腈中系列亚硝基四苯基钴卟啉Co-NO键的键能，即钴卟啉NO亲合势的定量标度，以表征钴卟啉的NO结合能力。

The determination of cytokinin levels is a primary and basic approach in the cytokinin studies. The Amaranthus betacyanin bioassay was modified for the rapid and convenient determination of cytokinin activity. Meanwhile, the procedures for quantitative analyses of cytokinins by HPLC and ELISA were estabolished, and these gurantee the analyses of cytokinin levels with high precision.

在细胞分裂素的活性测定中，通过改进尾穗苋苋红素合成法建立了一种简便、准确的生物试法，同时还建立了根据物理化学和免疫学原理而测定细胞分裂素的HPLC和ELISA方法，使得细胞分裂素的定量更加准确。

Methods To determine the serum PCT of 35 patients with bacteriosis and 15 patients with nonbacterial disease by gold immunochromatographic assay,and determine C-reactive protein and alkaline phosphatase of neutrophilic granulocyte in corresponding period.

方法采用半定量的胶体金免疫结合法，测定35例细菌感染性疾病住院患者及15例非细菌感染性疾病住院患者的PCT，并同期测定患者C-反应蛋白与中性粒细胞碱性磷酸酶。

There are two methods to detect and quantitative analysis Neu5Ac, one is high performance liquid chromatography with the use of Aminex87H column, the other one is barbituric acid method.

对Neu5Ac的检测和定量也有两种方法，一种是利用Aminex87H酸性糖基柱，通过高效液相色谱测定；另一种是硫代巴比妥酸法测定。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。