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安替比林

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The complexation ability of antipyrine 4-position acyl derivatives have been discussed briefly.

初步探讨了影响安替比林4位酰代衍生物β-二酮配体配位能力的因素

Methods: The original method diacetyl monoxime solution concentration of 2 g/L to switch to 10 g/L solids volume direct add to antipyrine dissolved of solution;DMA plus 10 ml water 2 ml 1 h after boiling liquid cooling, Pure water volume to 25 ml determination.

将原法二乙酰一肟溶液浓度2 g/L改为10 g/L的固体量直接加到安替比林溶液中溶解;水样10 ml加DMA2 ml沸浴1 h后冷却,纯水定容至25 ml测定。

Keywords Caffeine;Antipyrine;Sodium Salicylate;Satongfeng Injection;HPLC;Determination of content

咖啡因;安替比林;水杨酸钠;撒痛风注射液;高效液相色谱法;含量测定

Antipyrine ;; Cerebral Hemorrhage ;; Endothelin-1;; Plasma ;; Trauma ;; Calcitonin Gene-Related Peptide ;; Patients

安替比林;;脑出血;;内皮缩血管肽1;;血浆;;外伤;;降钙素基因相关肽;;病人

The linear ranges were 14.0 ̄140 μg/ml( r = 0.9998 ) for caffeine; 27.0 ̄270.0 μg/ml ( r = 0.9998 )for antipyrine; 0.1 ̄1.0 mg/ml ( r =0.9999) for sodium salicylate.

色谱条件为:KromasilC18色谱柱,流动相为20mmol/L磷酸二氢钾-甲醇-冰醋酸(55250.4),流速1ml/min,检测波长为242nm,线性范围:咖啡因14.0~140.0μg/ml,r=0.9998;安替比林27.0~270.0μg/ml,r=0.9998;水杨酸钠0.1~1.0mg/ml,r=0.9999。

The color development reaction between titanium in extra-low ferrochrome,nitrided ferrochrome and diantipyryl methane is studied.

研究了微碳铬铁、氮化铬铁中钛与二安替比林甲烷的显色反应。

Absorption spectrum of this complex is measured in 420nm wavelength,so titanium content in ferrotitanium will be determined.

将经典的铝还原—硫酸高铁滴定法,改为在硫酸—盐酸介质中,二安替比林甲烷与钛生成黄色可溶性络合物,在波长420nm处测量吸光度,借此进行测定钛铁中钛量。

The results show that the photolysis of phenazone is a pseudo first order reaction, and no dependence on pH is observed for the process.

结果表明,安替比林的光降解遵循拟一级反应动力学规律,pH值变化对光解速率基本没有影响。

The influence of initial pH value and environmental substances in water was discussed, the photolysis mechanism, proposed products and possible photolysis pathways of phenazone were analyzed.

以波长为254 nm的紫外杀菌灯为光源,研究了水溶液中消炎镇痛药物安替比林的光降解行为;考察了初始pH值及水中其他物质对PZ光降解的影响,探讨了PZ光解机制,并分析其降解产物及光解途径。

Seven Schiff bases of N-(4-hydroxyphenylmethylene)-1-naphthylamine, N-(4-hydroxyphenylmethylene)-p-methoxyaniline, N-(4-hydroxyphenylmethylene)-benzylamine, N-(4-hydroxy-3-methoxyphenylmethylene) furfurylamine, N-(4-hydroxy-3-methoxyphenyl methylene)-p-methylaniline, N-(4-hydroxy-3-methoxyphenylmethylene)-p-methoxyaniline and N-salicylidene-4-aminoantipyrine were first synthesized by the one step solid phase reactions between aromatic aldehydes with phenolic hydroxyl and amines at room temperature without solvent.

分别以带酚羟基的芳醛与胺类反应,首次通过室温固相反应一步合成了N-(4-羟基苯基亚甲基)-1-萘胺、N-(4-羟基苯基亚甲基)-对甲氧基苯胺、N-(4-羟基苯基亚甲基)-苄胺、N-(4-羟基-3-甲氧基苯基亚甲基)糠胺、N-(4-羟基-3-甲氧基苯基亚甲基)-对甲苯胺、N-(4-羟基-3-甲氧基苯基亚甲基)-对甲氧基苯胺和N-亚水杨基-4-氨基安替比林7种Schiff碱,反应15min完成,产率均超过90%。

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