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According to the observation of the microstructure of small diameter lumber with scan electron microscope, there are many bordered pits of the radial trancheidal wall in the small-diameter Larch, and most of them have pit film. The resin is not only in resin canal, but also in some trancheid and ray parenchyma cells. The drying defects of small-diameter Larch lumbers were the most severe in consecution heating, fluctuating-heats 2h in between, and drying defects were nearly not observed in fluctuating-heats 6h. There is tylosis in the vessel of the heartwood of small-diameter Cathay poplar. The bordered pits of the radial trancheidal wall are dense, and the pits between vessels are alternate, most of them have pit film. Different collapse happened in all the small-diameter Cathay poplar lumbers. The collapse of small-diameter Larch lumbers was the most severe with consecution heating, fluctuating-heats 2h in between, the least with fluctuating-heating 6h.

通过扫描电镜观察发现,小径木落叶松的径壁具缘纹孔数目较多,且多具纹孔膜,小径木落叶松除在树脂道中含有树脂外,在一部分管胞胞腔内以及一些木射线细胞中也含有树脂,在产生缺陷的小径木落叶松锯材中,连续加热方式下锯材的开裂缺陷最为严重,波动2时次之,波动6时几乎没有开裂现象;小径木大青杨心材导管中的层状浸填体含量较多,且径壁具缘纹孔较为密集,管间纹孔呈互列方式,绝大多数纹孔具有纹孔膜,干燥后的小径木大青杨锯材均有不同程度的皱缩现象产生,其中连续加热干燥试验锯材的皱缩现象最严重,波动2时次之,波动6时干燥试验锯材的皱缩缺陷最小。

The invention discloses a dielectric hole-microhole composite material and synthesizing method in the inorganic porous material, adsorbing material and catalytic material technical domain, which comprises the following steps: adopting zeolite molecular sieve as raw material; reacting with sodium bisilicate solution under 30-60 deg.c for 10-300 min; disintegrating particle part of zeolite molecular sieve into piece with microhole structure; adding cetyl trimethyl ammonium bromide as molder; adjusting pH value of mother liquid to 10-12; aging 1-8h; adding in the high-pressure autoclave to do water heat synthesizing reaction at 80-130 deg.c for 24-72h; separating solid; washing; drying; sintering under 500-600 deg.c for 5-10h; obtaining the Si-Al porous material with dielectric hole and microhole composite structure.

本发明属于无机多孔材料、吸附材料和催化材料技术领域,涉及具有介孔-微孔复合材料及其合成方法。其特征是以沸石分子筛为原料,用偏硅酸钠的水溶液在30~60℃反应10~300分钟,使沸石分子筛的颗粒部分解离形成具有微孔结构的碎片,加入模板剂十六烷基三甲基溴化铵,然后调节母液pH值为10~12,老化1~8小时,然后加入高压釜于80~130℃进行水热合成反应。反应24~72小时后,分离出固体,水洗、干燥,然后于500~600℃焙烧5~10小时,得到具有介孔和微孔复合结构的硅铝多孔材料。本发明的效果和益处是所发明的合成方法可用于合成多种沸石结构和介孔结构的复合材料,所合成的材料经过质子交换可以具有较强的酸性,在吸附和催化领域具有广泛应用前景。

For bulk lamella-forming diblock copolymers, perpendicular lamellae and concentric lamellae spontaneously form under the neutral and strongly preferential surface, respectively. When the surface preference is relatively weak, novel structures such as parallel lamellae, helices and catenarian structures are observed.

对体相形成层状相的双嵌段共聚物,我们发现在中性孔壁下共聚物自组装形成垂直于孔壁的垂直层结构,在强选择性孔壁下形成一系列的同心层结构,而在弱选择性孔壁下形成平行于孔轴的平行层、螺旋和链节等新奇结构。

Emblica have many different forms and most of them have tails and their perforation plates divide into two types:(1)there is one simple perforation plate at each end of the vessel elements and (2) there is one simple perforation plate at one end of the vessel elements and two simple perforation plate at the other end;(3)a few vessel elements have special inclusions;(4)the intervascular pits are alternate pits;(5)the pits between the vessels and rays are mixed pits ,pits with transverse gashes and scalariform pits.

结果发现,余甘子次生木质部导管分子中存在着许多不同的样式,导管分子大多数具尾;其穿孔板存在着两种类型:(1)两端均为1个单穿孔板;(2)一端为1个单穿孔板;另一端为2个单穿孔板;(3)极少数的导管分子具有特殊的内含物;(4)管间纹孔式为互列纹孔式;(5)导管射线间纹孔式为混合型纹孔与横列刻痕状纹孔以及梯状穿孔。

On the basis of investigating the developments of inorganic mesoporous material's syntheses and applications, mesostructured tin oxide, bismuth oxychloride, lead sulfide, bismuth sulfide, titanium phosphate and zinc phosphate were synthesized by Sol-Gel and hydrothermal techniques, employing the neutral surfactant organic amine and anion surfactant alkyl sulfonate as templates.

中文题名非硅基介孔材料的合成与表征副题名外文题名论文作者周书喜导师李健民学科专业物理化学研究领域\研究方向学位级别博士学位授予单位中国科学技术大学学位授予日期2003 论文页码总数92页关键词介孔材料介孔分子筛馆藏号BSLW /2003 /O643.3 /50 在对无机介孔材料的合成、应用等方面的发展现状进行了充分调研的基础上,本文运用溶胶一凝胶法、水热法等合成手段,选用中性表面活性剂有机伯胺和阴离子表面活性剂烷基磺酸盐为模板,制备了二氧化锡、氯氧化铋、硫化铅、硫化铋、磷酸钛、磷酸锌等无机介孔材料。

Special localized cutting communication with the customer; 2.5 If not available notched hole diameter less than 60 mm hole, can be used to be relatively enlarger for the opening; After opening 2.6 backplane approach, starting with the opening negative, positive exposed bit sharp, nated from the positive control (both sides maintain collapse teeth); 3 connected corner of the corner of the 3.1 connection method, identify three Kok code on the middle and lower (50 mm poured from top to bottom. Another try a) 3:00 even in the corner of the counter and cross wooden cabinet on the sideboard; 3.2 corner of the Outer Limits with a shutter-ping; 3.3 In accordance with the drawings corner of the size, will have a fixed angle of the black reinforce the lower corner with 3:00 counters even

特殊局部地方的切割必须与客户沟通; 2.5如割口不大可用圆孔、直径小于60mm孔,可用相对应的扩孔器进行开孔; 2.6后背板开孔方法,先从反面开孔,正面露出钻头尖时,再从正面往里操作; 3 转角条的连接 3.1转角条的连接方法是,找出三个角码,上中下(上下50毫米往里,另居中一个)三点连在与转角柜交叉柜体的侧板上; 3.2转角条的外沿与门板一平; 3.3按照图纸转角条尺寸,将已固定的转角条用黑钉上中下三点与转角柜连

Elaborated the punching components formation principle, the basic dies structure and the rate process and the principle of design; and designed some conventional punching die:the die for big diameter three direction pipe which solved the problom of traditional machining,the drawing and punching compound die with float punch-matrix,the drawing and cutting compound dies with unaltered press,the compound die for the back bowl of the noise keeper,the design of the compound die which could produce two workpieces in one punching,the bending die for the ring shape part ,the bending die which used the gemel ,automate loading die for cutting, the drawing,punching and burring compound dies with sliding automated loading,the punching die for the long pipe with two row of hole,the drawing die for the square box shape workpiece and the burring die for the box shape workpiece.

原文对于寒冲压技术的合种、特征及开展圆背做砬简单概述;阐述了冲压整机的构成本理、基础模具构造与活动进程及其设计本理;对典范的冲压件模具进佳的了设计:大曲径三通管冲压复合模设计掀世了大直径三通管的减工困难、带无沉动凸凸模的拉伸冲孔复合模设计、适力压边式落料拉伸切边复合模设计、长音器后挖碗落料、拉深、冲孔、翻边复合模设计、一模二件落料拉伸冲孔翻边复合模设计、环形弯曲件的模具设计、铰链舒方成形工艺及模具设计、半自动送料切角安装设计、涩板式送料拉深、冲孔、翻边模设计完成自动送料、长管少孔冲模设计、带凸缘台阶方盒形整件拉深模战盒形件正壁小孔翻孔模。

Elaborated the punching components formation principle, the basic dies structure and the rate process and the principle of design; and designed some conventional punching die:the die for big diameter three direction pipe which solved the problom of traditional machining,the drawing and punching compound die with float punch-matrix,代写医学论文,the drawing and cutting compound dies with unaltered press,the compound die for the back bowl of the noise keeper,the design of the compound die which could produce two workpieces in one punching,the bending die for the ring shape part ,the bending die which used the gemel ,automate loading die for cutting, the drawing,punching and burring compound dies with sliding automated loading,the punching die for the long pipe with two row of hole,the drawing die for the square box shape workpiece and the burring die for the box shape workpiece.

本文对于冷冲压技术的分类、特点及发展方向作了简略概述;论述了冲压零件的形成道理、基本生产模型结构与运动历程及其设计道理;对于典型的冲压件生产模型进行了设计:大直径三通管冲压复合模设计盖世了大直径三通管的加工难题、带有浮动凸凹模的拉伸冲孔复合模设计、适力压边式落料拉伸切边复合模设计、消音器后补碗落料、拉深、冲孔、翻边复合模设计、一模两件落料拉伸冲孔翻边复合模设计、环形屈曲件的生产模型设计、铰链卷圆成形工艺及生产模型设计、半自动送料切角装置设计、滑板式送料拉深、冲孔、翻边模设计实现自动送料、长管多孔冲模设计、带凸缘台阶方盒形零件拉深模以及盒形件侧壁孔眼翻孔模。

This paper describes the technical features, process principle and process flow of that technique, putting emphasis on the implementation procedure of hole position arrangement, measuring control, boring and hole completion, grouting sequence, pressure treatment and hole seal. It discusses key points of construction quality control, analyzes problems occurred during the construction and puts forward treatment measures.

文章介绍了袖阀管法注浆技术特点、工艺原理及工艺流程,重点从孔位布置、测量控制、开孔与成孔、注浆顺序和压力、封孔处理等方面介绍了袖阀管法注浆实施过程,论述了质量控制要点,对施工过程中出现的问题进行了分析,并提出了处理措施。

2 BJP direct toxicity on TEC NRK52E cell were subcultured on a 24-well plate (3×10〓/ml/well) and exposed to BJP κ or BJP λ in concentration 1, 5, 10, 20mg/ml for up to 24h, then the media was changed, and 〓H-thymidine was added for incubation for 18h at 37℃, the corporation was terminated, Acid-insoluble DNA was precipitated by adding 5% trichloroacetic acid radioactivity in the extracts was determined in scintillation counter.

细胞增殖的影响:将TEC株NRK52E以3×10〓/ml/孔分别加入24孔培养板,分别加入BJPκ与BJPλ(浓度1、5、10、20mg/ml)共同培养,均设3个复孔,24小时后加入〓H-TdR(1μCi/孔)在5%CO〓37℃孵育18小时,终止反应,加胰酶脱壁半小时后移到普通干燥试管,多头细胞收集器抽滤,用5%三氯醋酸,无水乙醇分别冲洗,烤干,冷却后加入闪烁液,放入液体闪烁计数仪测定放射性。

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And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

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