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The effects of some important factors on structure, pore size, porosity, flux, weight of vapor transfer, etc. have been investigated by changing temperature of PVDF resolution, types of solvent, molecular weight of PVDF, weight of additive, time of solvent pre-evaporation and so on. The optimal process of making membrane and recipe of solution were made out.

然后通过改变PVDF溶解温度,铸膜液的溶剂,PVDF的分子量,PVDF用量,添加剂氯化锂用量,涂膜时预挥发时间,凝固浴温度以及凝固浴中无机盐氯化钠、溶剂丙酮等影响因素,考察这些因素对膜形态结构及孔径,孔隙率,水通量,透湿量等性能的影响规律,初步确定了铸膜液配方及涂膜工艺条件。

The preparation procedures were optimized by orthogonal test L9(34) with the mean particle size and the amounts of total-phenol as indexes. Factors of the extraction pressure and temperature,diameter of nozzle, pre-expansion temperature were evaluated for their effects on preparation process.

以平均粒径、厚朴酚、和厚朴酚的总酚含量为考察指标,采用L9(34)正交实验,对影响RESS制备厚朴纳米液的因素(萃取温度、萃取压力、喷嘴孔径、预膨胀温度)进行优选。

Injection parameters such as injection pressure and nozzle diameters were investigated by using the quantitative calibration results.

在改变喷射控制参数和环境参数的喷雾特性研究中,应用定量标定的试验结果深入开展了喷油压力、喷孔孔径、环境密度和环境温度对喷雾各个特性参数影响的研究。

Injection parameters such as injection pressure and nozzle diameters were investigated by using the quantitative calibration results.

在改变喷射控制参数和环境参数的喷雾特性研究中,应用定量标定的实验结果深入开展了喷油压力、喷孔孔径、环境密度和环境温度对喷雾各个特性参数影响的实验研究。

Therefore, by comparing particle distribution of the spraying under different water pressure, and the nozzle's outlet velocity simulation get by Ansys, which is a software for mechanical simulation, a proposal of the application of 1.5mm nozzle, 8Mpa water pressure on the spot was put forward.

在比较多种光学测粒仪的基础上,选择Winner313系统测量不同孔径喷嘴在不同供水压力下喷雾雾场的粒径分布。通过分析比较喷嘴在不同压力下喷雾雾场的粒径分布和Ansys模拟得到的喷嘴内部及出水口速度场,建议现场应用1.5mm喷嘴、供水压力为8MPa进行喷雾。

Pneumophila serogroup 5 antibody to develop two immuo-colloidal gold tests respectively. Main works listed below as:1、Preparation and identification of polysaccharide antigen of L. pneumophila Bacteria of LP1 ~ 7,9 and 10 were cultured on yeast agar buffer activated carbon for three to five days at 37℃, 5%CO2. Protein-free polysaccharide antigens were obtained after harvest in cells, extraction, deproteinization, dialysis and other steps. Their immunogenicities were verified by ultraviolet spectrophotometer full-wavelength scanning and Western blotting.2、Preparation and identification of rabbit anti-LP1 antibodies and rabbit anti-LP5 antibody Rabbit anti-LP1 and anti-LP5 antibodies were purified after rabbits were immuned with antigens isolated as described above. The purities of both antibodies were above 80% and the titer of blood serum 1:32 tested by double antibody sandwich assay.3、Development of colloidal gold immunochromatographic assay kit The size of colloidal gold particles in the kit was 25nm. The optimal concentrations for antibodies were 30μg/ml and the sensitized concentrations of NC membrane were 5 mg/ml.

主要研究工作从以下几个方面进行:1、LP1~7、9和10型多糖抗原的制备与鉴定将LP1~7、9和10型菌株分别接种在缓冲活性炭酵母琼脂培养基上,37℃、5%CO2的条件下培养,3~5天后洗下菌苔,经抽提、除蛋白、透析等步骤后得到基本无蛋白的LP多糖抗原,经紫外分光光度仪全波长扫描及Western blotting验证其抗原良好。2、兔抗LP1抗体和兔抗LP5抗体的制备与鉴定分别用LP1、LP5型多糖抗原免疫家兔,采用琼脂糖双向扩散试验检测,两种抗体血清效价均为1:32;饱和硫酸铵法提取抗体,SDS-PAGE检定其抗体纯度均达到80%以上。3、胶体金免疫层析检测试剂的初步研制采用柠檬酸三钠还原法制备约25nm大小的胶体金颗粒;分别制备兔抗LP1抗体、兔抗LP5抗体的金标探针,两种抗体的最适标记量均为30μg/ml;选择适当孔径的微孔滤膜为载体包被两种抗体,NC膜包被浓度均为5mg/ml。

A quasi-double layer perforated structure, with veneer as walls, its space between being 0.08 cm, is built when the outer wall is perforated, with each aperture 1 mm, space length 1.5 cm, and the hard sound absorption material is added to the supported.

该隔声室利用胶合板作为双层墙壁材料,两墙壁间距离为0.08cm,外墙壁均匀穿孔,孔径为1mm,间距为1.5cm,并在支撑物上加垫较硬吸声材料组成准双重穿孔隔声结构。

The latter played a key role to the formation of the final Si-NPA.2. Si-NPA is composed of large quantities of well-separated, quasi-identical siliconpillars with a cross section size of ~1.5 m. These silicon pillars are uniformlyarrayed and perpendicular to the surface.

新鲜制备的Si-NPA具备下述结构特点:(1)Si-NPA是具有明显的尺度结构层次的微米/纳米结构复合体系;(2)在微米层次上,Si-NPA由大范围均匀排列的、彼此很好分离的硅柱组成,柱的横截面尺寸约为1.5nm;(3)在纳米层次上,Si-NPA中的硅柱均呈多孔状,孔径在~20-40nm,孔壁由粒径约为5nm的硅纳米晶粒组成。

Porous alumina templates with different apertures were fabricated by changing the oxidation voltage in two-step anodic oxidation, and then Cu nanowires were synthesized in porous alumina by the alternating current electrochemical deposition method. The Cu/PAA was analyzed by SEM and XRD, the results have shown that Cu nanowires were indeed synthesized in porous alumina which had the same diameter and good structure of wire grating.

通过改变二次氧化过程中的氧化电压,制备了不同孔径的多孔Al模板;采用交流电沉积的方法,制备了含Cu阳极PAA膜。X射线衍射分析表明,阳极PAA膜上确有Cu生成;扫描电镜显示,Cu纳米线粗细均匀,具有很好的线栅结构。

The algorithm only needs to solve an ill-posed linear system and a well-posed minimization problem and requires only the knowledge of the near field measurements of the scattered fields due to point source fields at a finite number of incidence and observation points distributed over a limited aperture.

该算法只需求解一个不适定的线性系和一个适定的非线性最小化问题,而且只需要点源入射场的散射场在某个有限孔径中若干有限个入射和测量点上的近场测量信息。

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