失重

By means of FTIR,SEM,DSC,TGA and XRD,we studied the microstructure,particle shape,meltage temperature,decomposition temperature and crystal degree,and gained better understanding about influences of different degrees of substitution on microstructure and thermal property of starch acetates.

用傅立叶红外、扫描电镜、差示扫描量热、热失重和X射线衍射测试技术对淀粉醋酸酯的结构、形貌、熔融温度、分解温度和结晶度进行表征，分析了不同取代度对醋酸酯淀粉的热性能及其结晶结构的影响。

H2SO4. By means of FTIR, SEM, DSC, TGA and XRD, we studied the microstructure, particle shape, meltage temperature, decomposition temperature and crystal degree, and gained better understanding about influences of different degrees of substitution on microstructure and thermal property of starch acetates.

用傅立叶红外、扫描电镜、差示扫描量热、热失重和X射线衍射测试技术对淀粉醋酸酯的结构、形貌、熔融温度、分解温度和结晶度进行表征，分析了不同取代度对醋酸酯淀粉的热性能及其结晶结构的影响。

Structure and corrosion behavior of the high silicon cast iron in several different environments have been tested by means of weight-loss analysis and metallograph.

采用失重分析、金相分析等实验方法研究了高硅铸铁的组织及在不同环境下的耐腐蚀性能。

Structure and corrosion behavior of the high silicon cast iron in several different environments have been tested by means of weight-loss analysis and metallograph,and compare the corrosion resistant of high silicon cast iron with common gray iron and white iron.

采用失重分析、金相分析等试验方法研究了高硅铸铁在不同环境下的耐腐蚀性能，并对高硅铸铁、普通灰铸铁及白口铸铁的耐腐蚀性进行比较。

Oxidation weight loss experiments and metallographic observations were used to evaluate the protection effectiveness of the coating.

通过氧化失重对比试验和金相检验的方法，考察了该涂料的防氧化脱碳性能。

Sulfidation kenetics of studied materials have been examined and compared. The structure and morphological features of sulfide scales have been investigated using metallographical, X-ray diffraction and EMPA techniques.

测定并比较了这些合金的硫化腐蚀失重，通过金相、X光衍射相分析和电子探针技术分析研究了硫化物锈层的形貌和结构特征。

The results show that the composite coating is metallurgically bonded to the substrate and the microstructure is fine and uniform. The hardness of the composite coating is up to 400 HV, which is 2.5 times that of the substrate. Under room temperature and oil lubrication condition, the sliding wear tests indicate the friction coefficient and weight loss of the composite coating are smaller than those of substrate. The worn surface of the composite coatings is much smoother than that of the substrate, without grooves and crater.

结果表明，复合材料涂层与基体形成良好的冶金结合，微观组织细小、均匀；复合材料涂层硬度达400HV，约为基体的2.5倍；在室温油润滑条件下，滑动磨损试验表明复合材料涂层摩擦系数和失重均小于基体，磨损表面划痕较浅且平滑，无明显的犁沟、粘着、剥落现象；激光表面合金化显著提高了材料的耐磨性。

By dehydrochlorination reaction the poly[(2-methoxyl-5-octyloxy)phenylene vinylene] is synthesized and the material"s structure is characterized by nuclear magnetic resonance spectroscopy, infrared absorption spectrum, ultraviolet and visible spectrophotometry. At the meantime, the fluorescence spectrum is measured and the mechanism of fluorescence occurring is analyzed. Thermal Gravimetric Analyzer"s results show that the MO-PPV"s thermal stability is fine. Also the experiment of resolvable property indicates that the MO-PPV can well dissolve in chloroform. Through analyzing the film"s surface by Metaloscope and Atomic Force Microscope, the good filming is found.

通过脱氯缩合法合成了聚(2-甲氧基-5-辛氧基)对苯乙炔，并分别用核磁共振波谱法、红外吸收光谱法、紫外-可见分光光度法等对其进行了结构表征；测量了样品的荧光光谱，分析了荧光产生的机理；热失重仪分析了材料的热稳定性，研究表明MO-PPV材料具有良好的热稳定性；溶解性实验发现材料在氯仿中溶解性较好；金相显微镜和原子力显微镜研究了薄膜的表面形貌，发现该材料的成膜性良好；材料的导电性研究表明，固体材料在掺杂下才可以表现出导电特性，而配成溶液的材料导电性因溶剂的不同而不同，并随溶解时间的长短发生变化。

The weight loss method, electrochemical impedance spectroscopy and surface analysis methods were employed to investigate the corrosion behavior of steel A3 under the combined effect of Streptomyces and Nocardia sp.

采用腐蚀失重法、电化学交流阻抗法和表面分析技术研究了A3钢在链霉菌和诺卡氏菌共同作用下的腐蚀行为。

The aim of this study was to develop a novel amphiphilic functional block poly(ε-caprolactone) bearing ketone groups MPEG-b-P(OPD-co-CL. 2-oxepane-1, 5-dione was copolymerized with ε-caprolatone in which methoxy poly (MPEG, Mn=5 000) and stannous octoate were used as initiator and catalyst, respectively. The syntheses were conducted by bulk and solution polymerization. 1H NMR results showed that peak position and splitting of the polymers synthesized through solution polymerization were consistent with theoretical data, demonstrating the products were designed block copolymers. While in the bulk polymerization, polymer peak position was changed due to their high reaction temperature, suggesting their structural variation.

将带有羰基官能团的4-羰基己内酯和ε-己内酯分别在甲氧基聚乙二醇(MPEG，Mn=5 000)为引发剂，异辛酸亚锡为催化剂溶液和本体体系中开环聚合，合成了两亲性侧基带有羰基官能团的聚己内酯嵌段共聚物MPEG-b-P(OPD-co-CL.1H NMR结果表明采用溶液聚合法合成的聚合物各峰的峰位置和分裂情况与理论一致，证明了产物是实验所设计的嵌段共聚物，而采用本体聚合法合成的聚合物由于温度的影响，聚合物各峰的峰位置发生了变化，说明其结构发生了变化；差示扫描量热法分析结果表明随着OPD单体含量的增加，聚合物的熔点，玻璃化转变温度和熔融焓增加；热失重测试结果表明OPD单体的引入增加了聚合物的热敏感性。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。