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The chloroform layer and the aqueous layer were separated by multiple column chromatography including macroporous resin, silica gel and polyamide column and preparative HPLC. The compounds obtained were identified by mass spectra and NMR data.

大青叶乙醇提取物,用氯仿萃取后得到氯仿层和水层,各层再分别采用硅胶柱、大孔树脂柱、聚酰胺柱、制备液相、葡聚糖凝胶柱层析及重结晶等分离手段进行分离、纯化,并应用化学性质和质谱、波谱法(1H-NMR、13C-NMR、HMBC)鉴定其化学结构。

Results the safe angle range for needling yamen (gv 15) were: 16.27±7.68~29.46±7.23 degrees for males and 18.46±4.81—33.61±7.83 degrees for females; the danger angle of upward oblique insertion was negatively correlated with the extension of bowing and raising the head, that is, the larger the angle of backward raising the head, the smaller the range of danger angle of needling into the great occipited foramen.

结果:得出哑门穴安全针刺角度,男性为16.27±7.68~29.46±7.32度,女性18.46±4.81~33.61±7.83度。且向上斜刺的危险角度范围与头颅俯仰程度呈负相关,即头颅后仰角度越大,刺入枕骨大孔的危险角度范围越小。

Results The symptom group had the phenomenons which posterior cranial cavity was small and heteromorphosis,the volume of infratentorial brain tissue was large,cerebellum tonsil shifted down slightly and the debouch of inferior foramen occipital was crowded.

结果 症状组有后颅腔小、形态变异、幕下脑组织体积大、小脑扁桃体轻度下移和枕骨大孔出口拥挤现象。

For the arch dam which reservoir has no suitable breach to build lasher and has mass flood discharge, opening large orifice for flood discharge has great advantage.

对于库区无适宜垭口可兴建泄洪道,而泄洪量又较大的拱坝工程,在坝身中开设大孔口泄洪具有显著的优越性。

50% ethanol elution part and water elution part were the active fraction with insulin resistance in selaginella, and was worth further studying.

卷柏水提液及大孔树脂50%乙醇洗脱部分均对大鼠胰岛素抵抗有明显的缓解作用。

This paper focuses on the evenness problem which occurs after solving the blockage problem through using bubble plate to replace sieve plate.

重点研究了采用泡罩板取代筛板解决堵塞问题后出现的均匀性问题,多方案优化的结果是采用较大直径的泡罩,并且加装一块大孔均布板,可以满足稳定运行的要求。

The product is in the pore structure on the graft copolymer of styrene divinyl benzene [-N amines (CH 3) 2 The ion exchange resin], the less alkaline, in the acidic, neutral and effective exchange of inorganic acid medium. and the larger size can be adsorbed molecules in aqueous solution and the use of anion.

本产品是在大孔结构的苯乙烯二乙烯苯共聚体上接枝叔胺基[-N(CH3)2]的离子交换树脂,其碱性较弱,能在酸性、近中性介质中有效地交换无机酸,并能吸附分子尺寸较大的阴离子以及在非水溶液中使用。

Methods:(1) Silica column chromatography and LH-20 were used in phytochemistry study.(2) Based on the extraction ratio of arctiin, the best extraction procedure was acheived under the direction of L9(34) orthogonal experimental design. From 10 types of resins, the one with the maximal binding ability for Arctii was selected and silica-column choramatograpy was used in its seperation and purification procedure.(3) The animal diabetic experimental model in Wistar rats was established with streptozotocin and many biochemical factors were used to indicate the pharmacological effects of arctiin, including glycosylated hemoglobin, serum creatinine, seralbumin, monoxide nitrogen, glycerin trilaurate, cholesterol, HDL-ch, LDL-ch, Blood urea nitrogen, creatinine, SOD, ET, MDA, total Urine protein and albuminuria.

(1)采用硅胶柱层析、聚酰胺层析、LH-20等方法对牛蒡子的化学成分进行研究;(2)采用正交实验设计方法,以牛蒡子苷为指标,确定了牛蒡子乙醇回流提取的最佳工艺;对10种类型大孔吸附树脂进行筛选,筛选出对牛蒡子苷吸附效果最佳的树脂;采用硅胶柱层析法,对牛蒡子苷进一步分离纯化;(3)建立实验性糖尿病大鼠模型,以GLU、TC、TG、HDL-ch、LDL-ch、TB、ALB、BUN、CREA、GHbAlc、NO、SOD、ET、MDA和尿液中TB、ALB为指标,研究牛蒡子苷药理活性;(4)以差速消化法纯化Wistar大鼠的主动脉内皮细胞并进行传代培养,测定牛蒡子苷对高糖条件下RAECs活性、RAECs释放LDH、MDA和NO的变化以及RAECs表达内皮型一氧化氮合酶表达的影响。

In derivations of these equations, the discharges which flow through the check gate are calculated with the orifice equation for building the relationship between upstream pool and downstream pool of the gate.

在公式的推导过程中,过闸流量采用的是大孔口出流公式,没有采用工程中常用的闸孔出流公式,这是为了便于建立上、下游渠池间的联系。

Methods The clinical presentations,MRI images, operative technique and prognosis of 9 cases with tumors of the foramen magnum were analyzed retrospectively.

目的 研究枕孔区肿瘤的诊断与手术疗效方法回顾性分析9例枕大孔区肿瘤的临床表现和MRI影像,手术技巧和预后。

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The reasons of iron ions content overproof in grade Ⅱ desalting water system,such as variation water quality,contamination of regenerant , operation adjustment of pretreatment system and switching operation of bed were discussed.

对二级脱盐水系统中铁离子含量超标的原因,如来水水质发生波动、再生剂受到污染、预处理系统操作调整、床体运行切换等进行了论述。

You were hired to drum up new business, so go and do it.

公司雇你招徕新业务,你就做你的事好了。

Who is in possession of this?

这是谁的?