大孔

Then the utilization solvent parting method, low pressure silica gel separation method and so on column chromatograph, opposition silica gel, glucosan gelatin chromatograph, pocket resin, carries on the chemical composition to the effective spot the system separation; The chemical composition obtains which to the separation carries on the structure appraisal with four big spectra.

然后运用溶剂分离法、低压硅胶柱色谱、反相硅胶、葡聚糖凝胶色谱、大孔树脂等分离手段，对有效部位进行化学成分的系统分离；对分离得到的化学成分用四大光谱进行结构鉴定。

This paper was studied on used resin to improve the content of Gymnemic acid after determination the best extraction process.

在匙羹藤酸提取实验基础上，采用大孔吸附树脂法进行匙羹藤酸的精制。

The result of saturated static adsorption of different types of resins showed that YWD-04 was suited to use on Gymnemic acid.

使用静态吸附法确定了大孔吸附树脂YWD-04最适于匙羹藤酸的精制。

Gymnemic acid was greatly refined by resin.

通过大孔吸附树脂，匙羹藤酸得到了较好的富集和纯化。

Seven macroporous adsorption resins were compared on their adsorption properties for total saponins from Helleborus thibetanus,and the LSA-30 type resin possessed the better adsorption ability.

对7种大孔吸附树脂的铁筷子总皂苷吸附性能进行了比较筛选试验，并对选定的树脂进行了吸附与解吸优化条件研究。

Methods: PNS was got by extracting panax notognseng with general method of alcohol circumfluence, purified with organic solvents, and separated with D101 macroreticular resin. The hematolysis rate and the immunocompetence of biology of PNS were determined by hemolysis test and experiment of splenocyte proliferation respectively.

乙醇回流法提取PNS粗提物，经有机溶剂除杂后，通过大孔树脂柱层析分离纯化；溶血性试验测定PNS作用后红细胞的溶血率；脾淋巴细胞增殖反应测定PNS的生物免疫活性。

The pigment of Berberis heteropoda Schrenk is a type of anchocyanin and it is strong in resistance against light and to some extent, good in enduring heat and low consistence oxide. But it is poor in resistance against reductant and preservative. It can be applied to the condition of PH. It is also found that sucrose and most of metal ions do not exert negative effects on the stability of the pigment, except Fe3+, Fe2+and low consistence Pb2+, which have some extent effects. Adding stability matter can improve its stability. The harm trace elements contains are within requirement of the National Standard on food safety, As the lexicological study indicates that the pigment does not have any toxicity and mutagenesis, it can be used as edible pigment.

结果表明：大孔树脂吸附-解吸附法纯化黑果小檗色素实验室工艺简单易行，色素回收率高；黑果小檗色素属于花色苷类色素；耐光性好；对热有一定耐受性；对低浓度氧化剂有一定耐受性；耐还原性差；对防腐剂耐性差；适用PH＜6条件下使用；蔗糖和大多数金属离子对色素无不良影响，但Fe~(3+)、Fe~(2+)、Sn~(2+)和低浓度pb~(2+)对色素有影响，加入稳定剂后，可提高色素的耐热性、耐氧化性、耐防腐剂能力；经对有害微量元素进行检测和毒理试验表明，该色素安全无毒，可以作为天然食用色素使用。

The sample had a hexagonally well-ordered array as shown by SEM observation. The diameter of macroporores was 360 nm corresponding to a shrinkage of 25%.

通过SEM检测，大孔以六方有序的方式排列，其孔径及孔径收缩率分别为360nm和25%。

Quercetin, quercetin rhamnoside, hyperin, syringoside and eleutheroside E wereisolated from the flower of Acanthopanax senticosus. Searching bioactive natural compound and establishing quality evaluation standard arefocused on this experiment. Using cold immersing of 70% methanol to extract from flower ofAcanthopanax senticosus and integrating macroporous resin, silica gel column chromatography,sephadex gel to abstract. We obtained five monomer compounds (compoundⅠ-compoundⅤ),quercetin, quercetin rhamnoside, hyperin, syringoside and eleutheroside E. That five compoundswere determined by HPLC in eight parts of Acanthopanax senticosus (flower, root, leaf fruit,shoot, new shoot, phloem of shoot, skin of shoot), which provide science bases for establishingquality evaluation system and settle infarctate foundation.

本文以从刺五加花蕾中寻找具有重要生物活性的天然化合物和建立质量评价标准为主要目的，对其化学成分进行研究，采用70％甲醇冷浸的方法对刺五加花蕾中的成分进行提取，运用大孔树脂吸附色谱法、硅胶柱层析法以及葡聚糖凝胶柱层析相结合的方法进行分离，得到5种单体化合物，分别为槲皮素、槲皮素鼠李糖苷、金丝桃苷、紫丁香苷和刺五加苷E；利用高效液相色谱法对这5种化合物在刺五加花蕾中的含量进行了测定；考察了8个部位(花蕾、根、叶、果、茎干、新枝、茎韧皮部、茎皮)中这5种化合物的含量分布情况，并作一比较，为今后建立刺五加质量评价体系提供了科学依据，奠定了坚实的基础。

The parasacral region using a curved probe (2–5MHz) was scanned in 17 patients in search of the medial borderof the ischial bone and the lateral border of the sacrum, whichrepresent the limit of the greater sciatic foramen.

我们在17位病人身上用2–5MHz 的弯探针在骶骨旁区域进行超声探测，寻找坐骨内侧缘和骶骨外侧缘，从而划出坐骨大孔的区域。

What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢？

I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我，一个心中布满虚荣的女孩子真实的想法。