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objective to determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of edaravone, by gas chromatography.methods sample solution was injected on a gdx column (0.18 mm~0.25 mm) with nitrogen as the carrier gas.the residue was calculated by the external standard method.results the linearity was good over the range of 25 μg/ml~400 μg/ml,with the correlation coefficient of acetone being 0.996 and the average recovery 96.8%.conclusions the method was proved to be simple,rapid,practical and highly sensitive.it is an efficient method for the quality control of acetoacetic ester.

摘要] 目的:用气相色谱法测定依达拉奉合成起始原料乙酰乙酸乙酯中丙酮的残留量。方法:采用固定相为二乙烯苯乙基乙烯苯型高分子多孔小球(直径为0.18 mm~0.25 mm),氮气为载气,用外标法测定乙酰乙酸乙酯中残留丙酮的含量。结果:该方法在丙酮浓度范围在25 μg/ml~400 μg/ml内呈良好的线性关系,响应曲线相关系数为0.996,平均回收率为96.8%。结论:本法简便,快速、实用,灵敏度高,可有效地用于乙酰乙酸乙酯的质量控制。

An experiment facility is set up, which consisted of a ceramic foam combustor, a gas flow system controlled by two pairs of solenoid valves for switching alternatingly the flow directions, and a measurement system.

预混合气体在多孔介质内往复流动下的超绝热燃烧是一项先进的燃烧技术,它以其高效、低污染的优越性正在引起人们的关注。

The basic idea of Frequent-Wavelet is to pass time series through the atrous smooth filters set, and then cluster the derived subsequences, so the problem of FTS mining is converted to the problem of FIS mining.

Frequent-Wavelet算法的基本原理是使时间序列通过多孔平滑滤波器组,然后对来自多个尺度序列的子序列进行聚类,从而将时间序列的频繁模式挖掘问题转化为项目序列的频繁模式挖掘问题。

The SEI film on the surface of three kinds of carbonous materials: Mesocarbon Microbead; Porous Carbon and Synthetic Graphite, which can electrochemically insert and extract lithium reversibly, was investigated in the appointed electrolyte.

在指定组成的有机电解液中,选择三类可电化学嵌脱锂的碳材料:中间相碳微球、多孔碳和人造石墨,研究其表面形成的固体电解质中间相膜的电化学性能。

To investigate the effect of surfactant self-assembling properties on the template synthesis of porous inorganic materials, the critical micelle concentration of surfactant cetyl trimethylammonium bromide was measured in both water and aqueous ethanol solvent using steady-state fluorescence techniques.

为了研究乙醇-水混合溶液中表面活性剂的自组装特性对多孔无机材料模板法合成的作用,采用稳态荧光法测定了乙醇-水混合溶剂的组成变化对十六烷基三甲基溴化铵临界胶束浓度的影响。

Another remarkable characteristic of printing and dye the waste water is that the colour is high, is it adopt biological carbon pool is it is it deal with to decolour to go on to it , for activated carbon absorbent spent to design originally, active charcoal adsorption method to utilize porous active charcoal material make one or many kinds of material of waste water it absorbs to be that surface get rid of in active charcoal.

印染废水的另一显著特点就是色度高,本设计采用生物碳池对其进行脱色处理,所用的吸附剂为活性碳,活性炭吸附法就是利用多孔活性炭物质使废水中的一种或者多种物质被吸附在活性炭表面而去除的。

Results showed that the monomer conversion increased slightly in the presence of the crosslinking agents The size of particles decreased slowh as the amount of cmsslinking agent increased.and the size distribution of the particles broadened at a higher amount of cmsslinking agent Divinyl benzene was more effective than ethyl glycol dimethyl methacrylate to make polymer crosslinked.During alkali treatment process,void latex particles can be obtained when no DVB or less than 0.5 wt% of EGDMA was used,while muhihollow structure was generated when DVB or more than 1.0 wt% of EGDMA was introduced.The volume expansion of the particles decreased with increasing the amount of emsslinkirlg agents.

结果表明,体系中加入交联剂后,单体转化率都有不同程度的提高;随交联剂用量的增加,乳胶粒粒径略有减小,交联剂用量较高时,乳胶粒粒径分布加宽;二乙烯基苯的交联效率稍高于双甲基丙烯酸乙二醇酯;不加入交联剂及EGDMA用量低于0.5%时,处理后乳胶粒呈空腔结构,加入DVB及EGDMA用量高于1.0%时,处理后乳胶粒呈多孔结构,并且乳胶粒体积增量随交联剂用量的增加而减小。

The evolution of orogenic zone,gold ore-formation and its dynamic mechanism are studied and the new viewpoint is put forward that thermal stress is a main controlling factor in metamorphism,formation ,evolution of structure and ore-forming geodynamic environment. The critical condition of fluid convection in porous equal medium and the new conclusion is reached first that the thickness of structural layer and temperature gradient are main factors influencing fluid convection andtransport of ore-forming matters in additional to physical properties of rocks. According to the conclusion some mechanisms such as the transform from compressive type to tensile one of erogenic zone,transport and accumulation of ore-forming matters such as gold and so on and many ore-forming temperature values are interpreted qualitatively.

探讨了区内造山带演化、金成矿及其动力学机理,提出了热应力是影响变质作用、构造形成演化及成矿地球动力学环境的主控因素的新认识;对多孔均匀介质中流体对流的临界条件进行探讨,首次提出了除岩石物理性质外,构造层厚度和温度梯度是影响流体对流乃至矿质输运的主要因素。

Considering a spherical porous carbon particle immersed in a static ambient atmosphere, the combustion characteristics under three basic conditions: frozen flow, equilibrium flow, partial flow are solved in a half-analytical and half-numerical way. By using the LAEA (Large Activation Energy Asymptotic Method), the departure value of some parameters such as combustion rate, temperature, and concentration are obtained. On this basis, the rules of a carbon particle combustion under various conditions when the gas phase Damk〓hler number is in the range of 0,+∞ are summarized.

建立氧化性环境中相对静止的多孔炭粒燃烧的控制方程,采用半解析、半数值方法求解出炭粒在冻结流、部分流、平衡流三种基本情况下的燃烧规律,并采用大活化能渐近匹配方法,计算出偏离冻结流、偏离平衡流情况下燃烧速率、温度及组分浓度等参数的偏离解,进而总结出炭粒在气相Damk〓hler数为0,∞整个范围内燃烧特性变化规律。

All countries scholar have been looking for new cavitation to replace the ultrasonic cavitation technique, the hydrodynamical technique have lower cost and equipment simpler characteristics than the light or particle cavitation , so it was valuable of

本文所做的主要工作及所取得结论: 1 设计并组装了一套水动力空化反应循环系统; 2 设计了3种不同型号(孔径分别为1毫米、2毫米、4毫米)的多孔板; 3 比较了不同板在不同条件下的空化效应强弱; 4 利用该装置对大肠杆菌菌液进行消毒杀菌的实验研究;结论:(1)在孔径较小时,空化效应更强

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