复合分析

After filtration process, the results showed that the filtration effect of sewage was satisfactory. DTA and XRD patterns showed that the membrane calcined at 1000℃was composed ofγ- Al_2O_3, t -ZrO_2 and amorphism SiO_2, the phase transformation wasn't occurred until 1200℃.

DTA和XRD分析表明，经过1000℃煅烧后的复合膜中，主晶相为γ-Al_2O_3和t -ZrO_2，SiO_2以无定形态存在，复合膜经1200℃的热处理后仍然没有发生γ-Al_2O_3向α- Al_2O_3的相变。

This paper introduced the cable anchor support technology under the situation of compound roof for Yongxia mining area, analyzed the principle of anchor rod with cable anchor , and made a declaration for the support parameters.

介绍了永夏矿区复合顶板条件下煤巷锚网索支护技术的情况，分析了复合顶板条件下锚杆加锚索支护的原理，并对支护参数进行了说明，对类似条件下的巷道支护具有较强的指导意义。

The characteristics of pentacene/perylene derivatives based organic solar cells are investigated in this thesis Donor and acceptor layers are pentacene and N N'-dioctyl-3 4 9 10-perylenetetracarboxylic diimide (PTCDI-2~13C) respectively Twelve organic solar cells with pentacene/PTCDI-2~13C heterojunctions were fabricated to study the influence of various alkylic perylene derivatives on the power conversion efficiency Under the sunlight simulator with AM1 5G filter and 100 mW/cm2 the solar cell of pentacene/PTCDI-7C heterojunction with cathode of Ag/Al bilayer has the best performance among the devices with pentacene/PTCDI-2~13C heterojunctions In PL spectrum analyses the pentacene/PTCDI-7C film had lower recombination rate than the other pentacene/PTCDI-2~13C films; therefore more excitons could reach the P/N junction and enhance short-circuit current Furthermore the PTCDI-7C film grown on the surface of penatcene was more matched than other PTCDI films analyzed by the PL peak shifts of 10 nm and 45 nm thick PTCDI-2~13C and images of atomic force microscope More lattice match between the films of pentacene and PTCDI resulted in fewer defects in P/N junction and more carries can reach electrodes Accordingly the power conversion efficiency approach 2% was obtained from the solar cell with the active layer of pentacene/PTCDI-7C

本研究探讨以五环素/骈苯衍生物异质接面太阳能电池之特性，利用pentacene作为电子施体有机材料，PTCDI -2C~13C作为电子受体有机材料，制作出异质接面为pentacene/ PTCDI-2C ~13C等12种有机太阳能电池，比较不同碳数的骈苯衍生物对於有机太阳能电池之光电转换效率之影响。在AM1 5G、100 mW/cm2的模拟太阳光下，以pentacene/PTCDI-7C异质接面太阳能电池具有短路电流9 882 mA/cm2、开路电压0 376 V、填充因数0 523及光电转换效率达1 945%，皆比其他pentacene/PTCDI-2C ~13C异质接面太阳能电池来的大。由薄膜分析可知PTCDI-7C在这12种太阳能电池中具有较低的电子电洞复合发光效率，可以让较多激子到达异质接面进行电荷分离，减少电子电洞对复合发光的机率；此外，由光激发萤光光谱之峰值位移配合原子力显微镜表面结构图，可以得知当PTCDI-7C成长在pentacene上时会顺著pentacene的结构成长薄膜，故较无缺陷产生在P/N接面处；而在其他结构下则无此现象产生，致使在pentacene/PTCDI-7C薄膜中的载子有较大的机会可以移动至电极，使光电流提高，进而使光电转换效率提高。

In order to study the depolarization of compound binary wave plates,Mueller matrixes of different combined wave-plates were studied by means of theoretical analysis and experimental verification.

为了研究二元复合波片的退偏性能，采用了理论和实验相结合方法，对不同的波片复合后的米勒矩阵形式进行了理论分析和实验验证。

The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究，实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先，利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维，比较不同的热处理温度与反应时间的改变对产物生成产生影响，进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示，结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现，若热处理温度在100~4750C下可得到Cu23Cl奈米粒，475~4900C 可得Cu奈米粒，450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时，可产生直径比较细的纤维，纤维直径为107 88±21 01nm；且由於奈米金属颗粒镶嵌在二氧化矽纤维中，直径比较细的纤维，可以得到比较小的奈米金属颗粒，这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时，由於表面电浆子共震关系，而使纤维颜色由淡白黄绿色变成黄绿色，再变红褐色。由实验结果得知，利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度，可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

The effect of the form(including individual,complex and complex proportion),the dose of graphite,carbon black,carborundum and the alkalinity of base slag on the melting speed were studied.

以石墨、炭黑、碳化硅等三种含碳材料和碱度分别为0.8、1.0和1.2的基渣为原料，研究了炭黑、石墨和SiC加入形式(单独或复合，包括复合时的比例)和加入量以及基渣的碱度等因素对保护渣熔化速度的影响，并对试验数据进行了多元线性回归分析。

The methods of disturbance, spiral cylindrical cavity and stripline resonator were used respectively for measuring the permittivities for microwave dielectric substrates. The substrates are made from PTFE based fine ceramics, and errors of measurement have been analyzed.

采用微扰法、螺旋圆柱谐振法和带状线谐振法分别对聚四氟树脂复合精细电子陶瓷微波复合介质的复介电常数进行了测量与误差分析。

This paper expounds the oxyacetylene flare overlaying welding technology of tungsten carbide rod made to be metal matrix carbide ceramal compound overlaying welding layers.

介绍碳化钨条氧乙炔火焰堆焊制备金属基碳化物陶瓷复合耐磨堆焊层的工艺方法，结合碳化钨条氧乙炔火焰堆焊工艺过程、堆焊层性能特点、泥沙磨损实验结果及显微组织形貌，分析讨论了热源性质对堆焊层性能的影响以及复合耐磨堆焊层的抗泥沙磨损特性。

The paper presents the analysis of PDC bit structure commonly applied in colliery and coal field exploration and a brief introduction on processing technology and attentions which should be paid in application.

主要对煤矿和煤田勘探中常用的金刚石复合片钻头的结构进行了分析，并简要介绍了复合片钻头的加工工艺和使用中应注意的问题。

The complex of gold conjugate and analyte then moves onto the membrane strip and migrates towards the capture binding protein, where it becomes immobilized and produces a distinct signal in the form of a sharp red line.

金标和分析物的复合物扩散到膜上，并向检测蛋白移动，在那里复合物被固定住，产生清楚的信号——一条红线。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。