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Monochloroethylene carbonate is prepared by chlorination of ethylene carbonate with sulfuryl chioride ,a solution of monochloroethylene carbonate in ethylene carbonate is reacted with triethylamine to give vinylene carbonate.A parameter design method was applied to select the optimum synthesis conditions.63.3% and 78% yields superior to the conventional for monochloroethylene carbonate and vinylene carbonate were obtained respectively,and the process was also simplified .

以碳酸乙烯酯为原料,用磺酰氯作为氯化剂生成一氯代碳酸乙烯酯,三乙胺为脱卤化剂在碳酸乙烯酯溶剂中合成碳酸亚乙烯酯,对一氯代碳酸乙烯酯和碳酸亚乙烯酯制备的工艺参数进行优化,收率分别达到63.3%和78%,均超过了传统方法,且简化了工艺,缩短了反应时间,易于工业化生产。

Objective:The aims of the present study were to determine the expression of transformation growth factor β 1 (TGF β 1) mRNA and TGF β 1 protein in the peripheral blood and its relation to serum levels of procollagen type Ⅲ N terminal peptide in the patients with cirrhosis.

转化生长因子-β1(TGF-β1)在一些体外和体内的研究中均显示能刺激胶原和细胞外基质的合成,同时又可通过抑制ECM降解以加强纤维的发生,在肝纤维化中起重要作用。

It was shown from the results that emulsifier TP-Ⅴ which was prepared by PEG 4000 reacted with TME, in the molar ratio of TME to PEG 2:1, at about 110℃ for 1 h, catalyzed by boron trifluoride diethyl etherate, has a very good emulsifying impact for TME. Particle size distribution of the emulsion was homo-geneous and viscosity of the emulsion was small.

实验结果表明,以M相对适中的PEG4000与TME按物质的量比2: 1、在催化剂三氟化硼乙醚作用下、110℃左右反应1h合成的乳化剂TP-Ⅴ,对萜烯基环氧树脂具有很好的乳化效果,制备的乳液粒子粒径均一度较高,乳液表观黏度较小。

Using semi-quantitative RT-PCR, the differential expression profiles of eleven selected genes were confirmed in the ovaries of triploid and diploid. These genes fell in gene categories with a wide range of functions. The results indicated that triploidy affects the dynamic gene regulatory network in triploid ovary. This study established a firm basis for future investigation on characterization of crucial molecular events for normal ovarian development in shrimp.To further dissect exact gene functions for gonad development of shrimp, three differentially expressed genes between diploid and triploid ovary, PCNA (proliferating cell nuclear antigen), CAS/CSE1 (cellular apoptosis susceptibility protein/chromosome segregation 1) and SSRF (spermatogonial stem-cell renewal factor) were characterized on certain aspects.

利用抑制性消减杂交技术,建立了对虾二倍体和三倍体卵巢间的2个消减文库;在正向消减文库(以三倍体卵巢作为实验组,二倍体卵巢作为驱动组)中,鉴定到54个基因;在反向消减文库(以二倍体卵巢为实验组,三倍体卵巢为驱动组)中,鉴定到16个基因;选取11个差异表达的基因,利用半定量RT-PCR的方法对其在二倍体和三倍体卵巢间的表达进行了检测,均能很好地与消减结果相吻合;这些差异基因编码多种功能的蛋白,分析表明染色体的三倍化使三倍体卵巢中的基因调控网络受到了影响;为深入揭示维持卵巢正常发育的关键分子调控事件奠定了基础。

The fluctuating deviation of bed voidage and theenhancement index of bed uniformity derived in this study can describerespectively the bed uniformity and its extent. A new criterion of demarcationof uniformity, composed of materialparameter, operating parameters (H0, u/umf) and vibrationparameters, can be used to predicting a suitable range ofbed uniformity.

对空隙率波动偏差的分析表明,振动参数、颗粒物性和操作参数均对床层均匀流化行为有不同程度的影响,且振幅和振动频率越大越能明显提高以小米或玻璃珠为物料的床层的均匀稳定性,而颗粒物性和操作参数直接影响振动能量在床层中的传播。

The urase activity,trypsin inhibitor activity and content of routine nutrition constituent were analysised and determined,in terms of process test of soya by extrusion,far-infrared baking and digestion .

对大豆进行挤压膨化、远红外烘烤和蒸煮加工,测定其尿酶、胰蛋白酶抑制因子的活性及常规营养成分的含量,得出三种加工方法对尿酶、胰蛋白酶抑制因子的影响是同步的,均可使它们的活性降到标准值以下,符合饲喂要求。

C. Functionalization of [60]Fullerene with Vaporous Reagents via Its Calix[8] arene Complex Supramolacular complexes are applied widely in synthesis chemistry.

结果表明,它们均是有效的硅氢化催化剂,并具有某些独特的催化性能,如在催化苯乙烯的硅氢加成时,以高达85%-100%的区域选择性得到α-加成物。

As noted above,membrane-stabilizers unexpectedly improved the heart function andprevented ER stress both in vivo and in cultured cells.We know that the membranestability depends on the sodium homeostasis in fact.To investigate whether ER stress isassociated with sodium channel action,which determins the membrane stability,wepretreated H9c2(2-1) cells with veratridine,a sodium channel activator.

上面的研究发现膜稳定剂在体内体外均抑制了内质网应激,并改善了心脏功能,而膜稳定作用实际上是维持细胞钠离子稳态的结果,为了研究内质网应激反应与钠离子活动的关系,我们用一种钠通道激活剂藜芦定刺激H9c2(2-1)细胞,30分钟时GRP78表达增加;24小时时PERK磷酸化和CHOP蛋白表达显著增加,说明钠离子通道过度激活诱发了内质网应激反应。

It adopts Reynolds time-average N-S equation and k-s turbulence model to calculate the inner 3-D viscid turbulence flow of hydraulic turbine. In the unstructured grid, the governing equations are discredited with Finite Volume Method based on Finite Element Method. And the pressure correction method is proposed in numerical calculations.

然后采用基于雷诺时均N-S方程与标准k-ε湍流模型来计算水轮机三维粘性湍流场,在非结构化网格中,采用基于有限元的有限体积法对方程进行离散,用压力校正法进行数值求解。

These data demonstrated that it was convenient and simple of vitrification methods to cryopreserve embryos with high transfer efficiency.

玻璃化冷冻方法简便、迅速,无论是细管法还是OPS法均获得了比较理想的胚胎移植效果。

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Recall that, in the Kolmogorov axiomatization, measurable sets are the sets which have a probability or, in other words, the sets corresponding to yes/no questions that have a probabilistic answer.

延期开工的Kolmogorov宣布要衡量所有套职能有限许多坐标限制在于衡量子寅。换句话说,如果是/否的问题回答f可看的价值观念在许多最有限坐标,然后它有一个概率的答案。

The experimental results showed that the algorithm can filter singular points and remain fixity of the target edge.

实验表明:基于模糊理论的图像智能滤波方法比常规图像滤波方法运算量小,它既能去除奇异点,又能保持图像中目标的边缘不变性,具有很好的滤波效果。

It explains in detail how the methods of elicitation, discussion, and induction are to be used in the physics teaching.

本文根据心理学原理论述了改革初中物理教学的必要性,并对"启发、讨论、归纳法"在物理教学中的应用作了详细的阐述。