地方法

In spite of this, the preparation of thiol-end functionalized PMMA was achieved by introducing a short block of polystyrene after the RAFT polymerization of MMA.Third, RAFT technique was applied to design and synthesize some well-defined poymers. Five monomers, lauryl methacrylate,(N,N-dimethylamino)ethyl methacrylate, poly methyl ether methacrylate, 4-(4\'-cyanobiphenyl-4-yloxy) butyl methacrylate and 2-ethyl methacrylate were chosen to RAFT homopolymerization or copolymerizations mediated by cumyl dithiobenzoate.

RAFT方法在具有特定结构聚合物的设计与合成上的应用，在机理研究的基础上，本论文选择五种不同结构的甲基丙烯酸酯类单体：lauryl methacrylate，(N，N-dimethylamino)ethyl methacrylate，polymethyl ether methacrylate，4-(4'-cyanobiphenyl-4-yloxy)butyl methacrylate和2-ethyl methacrylate，用CDB调控RAFT聚合的方法设计合成了一些特定结构的聚合物，详细而深入地研究了它们的均聚、共聚动力学，发现了双硫酯并非在聚合反应初期就全部转化，而是随着反应进行逐步消耗，这与理想的活性聚合体系有很大差别。

In this paper, base on model ship and ship-test, orderliness of the deflective force of single-screw ship for stopping maneuver and hydrodynamic explanation are concluded by the method of qualitative a...

本文在总结船模和实船试验的基础上，通过定性分析的方法，给出单桨船倒车偏向力的一般规律和水动力学解释，并给出几类单桨船制动机动偏向力的估算方法，有助于舰船驾驶员充分、快速地掌握本船的制动机动性能。

We prepared the ordered porous alumina membrane by a two-step anodization method in oxalic or sulfuric acids, which is a self-ordered hexagonal array of cells with an adjustable pore diameter of 20-150nm and a different pore structures (i.e. Y-branched, dendriform, toothed and torous ones). Furthermore, the template-electrodeposition, vapor-catalytic growth, and controlled chemical etching were developed for well-aligned carbon nanotubes and oxide nanopillars with adjustable diameter, Al2O3-AlN one-dimensional heterojunction, Y-junction and dendriform metal nanowires, as well as Y-junction, and torous carbon nanotubes. The resultant one-dimensional junctions were characterized by XRD, SEM, TEM,HRTEM, and STM, and the field emission of the well-aligned carbon nanotubes and the luminescence of ZnO nanopillar array have also been mearsured.

完善和发展了阳极腐蚀法制备多孔氧化铝膜的方法，制备出了孔径在20-150nm之间可调和具有不同孔结构（如Y形、树枝状、锯齿状）的系列多孔氧化铝模板，在此基础上，利用电化学沉积、气相催化生长和化学控制腐蚀等方法，成功地生长出具有可调直径的碳纳米管和氧化物纳米柱有序阵列、Al2O3-AlN异质结纳米线、Y形和树枝状的金属纳米线以及Y形、藕节形和锯齿形的碳纳米管等多种一维结纳米材料及其阵列体系，探索了基于模板孔壁内沿生长一维结纳米材料的机制，较系统的研究了碳纳米管阵列的场发射性能和氧化锌纳米柱的发光性能，为低维纳米材料器件化提供了实验基础。

The teaching and learning action based on network becomes popular in current high school, by the didactical feedback information of all kinds can be obtained after the processing of education information.It can provide the scientific and effective instruction for the teaching and the learning. This paper focused on the education information processing method and the realization technology with middleware based on network.

基于网络环境的教学活动在高校日益普及，通过对网络教学环境中教育信息的处理得到的各类教学反馈信息能为教师施教和学生学习提供科学有效地指导作用，本文在研究网络教学环境中的教育信息处理方法的基础上，结合中间件技术重点探讨了数学处理方法在网络平台的实现技术。

In chapter four, the preperation of ytterbium diiodide was examined. The reductive cleavage of Se-Se bond and S-S bond induced by ytterbium diiodide was investigated. The reaction of diselenides and disulfides with allylic bromide promoted by ytterbium diiodide was also examined. The intermolecular Barbier-type reaction induced by ytterbium diiodide was studied. In the last section of this chapter, the intermolecular reductive coupling of nitriles with azides induced by samarium diiodide was investigated.

第四章，研究了二碘化镱的制备方法，以及二碘化镱作为一种优良的单电子转移试剂在有机合成中的应用：二硒醚的Se--Se键和二硫醚S-S键的还原断裂，及其在合成烯丙基硒醚，硒代酯和烯丙基硫醚，硫代酯中的应用，实验结果表明二碘化镱也能促进分子间的Barbier反应，而文献认为二碘化镱不能促进分子间的Barbier反应；最后研究了二碘化钐促进的叠氮化合物与腈的交叉还原偶联反应，一步高收率地制备脒的方法。

A new method for determination of Pd using precipitation separation by butanedione dioxime as a selective reagent and complexometic titration EDTA released from EDTA-Pd complex was established.

建立了丁二肟选择性沉淀分离和析出EDTA-Pd络合物中的EDTA，Pb(NO3)2返滴定测定Pd的新方法，系统地研究了在硝酸或盐酸介质中测定Pd的条件，并对比了本法与《国家标准》分析方法的结果。

The development of network and communication technology provide convenient and shortcut approach to exchange information and share resource. On the other hand, there has been the problem how to manage the network since the network appeared. SNMP emerging as the times require with the development of Internet provides the universal methods to get and configure the information of network management from the objects managed. It is a discussable problem how to understand SNMP deeply and apply SNMP to practice effectively.

网络和通信技术的发展，一方面为信息的交流，资源的共享带来了方便、快捷的途径；另一方面，从网络出现起，就存在着网络管理的问题，在Internet发展中应运而生的简单网络管理协议定义了从被管理对象获取和配置网络管理信息的简单而功能强大的通用方法，然而要透彻地理解它和有效地应用于网络管理的实践中是值得研究的问题。

The simulation results and engineer practice show t hat the application scope of is distinguishingly exˉ tended, and the outlier's influence on filter precision is weaken.

仿真计算和实际工程应用表明，该方法有效地拓展了3σ方法的应用范围，很大程度上消除了野值对滤波精度的影响。

The Nazarov cyclization, a powerful tool for the construction of five-membered carbocycles from divinyl ketones and related compounds, has attracted increasing attention in recent years due to its wide applications in the synthesis of complex natural and unnatural products.

Nazarov环合反应是通过二烯酮类物质和类似化合物构建五元碳环的有效方法。由于该方法广泛地应用于复杂天然和非天然产物的合成，近年来引起人们的广泛关注。

The principle and process of detecting weak signal by using Duffing oscillator are discussed in detail.

传统的检测方法总是千方百计地通过抑制噪声来检测有用信号，可是在抑制信号的过程中不免使有用信号受到损失，因此这是一种两败俱伤的方法。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐