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在溶液中

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During the investigation on the isolation of aureomycin from fermentation broth, it was observed that the stability of aureomycin depended upon the pH and temperature of the solution.

本文测定了金霉素在酸性溶液中(0.01,0.1及1N盐酸)及在碱性缓冲液中(pH7.4,8.0,8.6,9.2)的稳定性,找出在碱性缓冲液中的稳定性较在酸性溶液中为小。

The fluorescence anisotropy using steady-state fluorescence polarization method was measured for the solution of β-CD and cinchonine mixed and sonicated for 1h. The anisotropy values for the solution increased with the increase of the concentrations of β-CD, which implied the existence of some complexes of large size or nanotube structure. Many type of large size complexes formed between β-CD and Cin under high concentrations in gas phase were characterized by ESI-MS in moderate experiment conditions.

将辛可宁与环糊精的混合溶液超声1个小时后,用稳态荧光偏振方法测定溶液的各向异性值,发现随着环糊精浓度的增大,溶液的荧光各向异性不断增强,这意味着溶液中形成了大尺寸即纳米级结构的环糊精与辛可宁复合物;用温和的质谱测定条件表征发现高浓度的β-CD与辛可宁在气相中可形成各种类型的大尺寸复合物。

Through the experiments on hydration of AH in the following sulphate(Li_2SO_4、MgSO_4 、 Al_2(SO_4)_3 、MnSO_4 、CuSO_4 、CoSO4 、CdSO_4 、ZnSO_4 、NiSO_4 、FeSO_4), dissoluble sulfate hydrate origining from hydration process of AH affects it's hydrous rate, hydrous rate of AH does not connect with Z/R of cation in stimulation, theory that Z/R affect hydrous rate of AH does not exist. Third, hydration of AH in dissoluble sulfate complies with dissolve-nucleate -grow theory, concentration of Ca~2+ from dissolving of CaSO_4 is higher than one of CaSO_4·2H_2O, calcium sulphate dihydrite gets a motivity of crystallization. dissoluble sulfate takes the following function: double-salt or dissoluble sulfate hydrate from hydration of AH in it becomes heterogeneous particle and a kind of nucleation catalyzer, and reduces surface barrier when DH becomes crystal because the crystal of DH precedently appears in uneven place. Results indicate hydration of AH does not conform with double-salt theory, but it conform with this mechanism: dissolve-nucleate-grow, formation of DH is an uneven nucleation and crystalizaion process.

通过对CaSO_4在Na_2SO_4 、K_2SO_4 、Rb_2SO_4 、Cs_2SO_4 、(NH_4)_2SO_4溶液中水化过程,以及CaSO_4·2H_2O、CaSO_4与以上硫酸盐反应速度、产物的研究,说明复盐理论不正确;CaSO_4在(Li_2SO_4、MgSO_4 、 Al_2(SO_4)_3 、MnSO_4 、CuSO_4 、CoSO_4 、CdSO_4 、ZnSO_4 、NiSO_4 、FeSO_4)溶液中水化,水化过程中硫酸盐水合物的析晶影响着无水硫酸钙水化,与激发剂阳离子Z/R值大小无关,阳离子的Z/R参数影响水化率的规律并不存在; 3、无水硫酸钙在可溶性硫酸盐中的水化按照溶解-成核-生长理论进行,CaSO_4达到溶解平衡时Ca~2+的浓度大于CaSO_4·2H_2O溶解平衡的Ca~2+的浓度,CaSO_4·2H_2O获得结晶的驱动力,可溶性硫酸盐起到形成晶核的作用:水化过程与CaSO_4生成复盐或析出水合物所形成的细小物相,作为异质微粒使母相中存在不均匀性,这些不均匀性有效地降低成核时的表面能位垒,使CaSO_4·2H_2O晶核优先地在这些具不均匀性的地方形成,因此这些物质起成核催化剂作用。

The results show that, with the increase in ionic strength, the adsorbed amount of taurine on the resin D290, the distribution coefficient λ and the fraction of zwitterion Tau(superscript ±) all decrease, while the pH value of the solution at the equilibrium and the content of anionic taurine Tau(superscript -) increase. Moreover, it is found that, at a certain taurine concentration, the increase in ionic strength may improve the selectivity of the anion resin for taurine.

研究结果表明:(1)随着溶液离子强度的升高,阴离子树脂对牛磺酸的平衡交换吸附容量逐渐降低,牛磺酸在树脂上的分配系数λ逐渐下降;(2)随着溶液离子强度增大,达到平衡时液相的pH值升高,溶液中牛磺酸阴离子Tau含量迅速增加,而牛磺酸两性离子Tau含量迅速降低;(3)在一定的牛磺酸浓度范围内,溶液离子强度增大,有利于提高离子交换树脂对牛磺酸的选择性。

The results show that the samples exposed to the air previously for 24 h can be passivated automatically in acetic acid solution with Cl- with the corrosion potential remaining 100mV.No such phenomenon was observed for samples which were cathodically polarized with the corrosion potential stabilizing at a value of -242±3mv. The passive film formed by anodically polarizing is more proof than formed in the air.

研究还发现:在空气中放置24小时后的试样在Cl-醋酸溶液中能自钝化,自腐蚀电位为100mv;经阴极极化后的试样在Cl-醋酸溶液中不能自钝化,其自腐蚀电位为-242±3mv;经阳极极化形成的钝化膜比在空气中自然形成的钝化膜更致密。

In the aqueous solution of sodium hydroxide,benzoylformic acid can coordinate with 2,4-dinitrophenylhydrazine to form a complex which has maximum absorption at 458 nm.Thus the content of benzoylformic acid can be quantitatively determined.

在氢氧化钠溶液中,苯乙酮酸和2,4-二硝基苯肼形成一种红棕色的溶液,该溶液在458 nm处有最大吸收,据此可以快速分析混合物中苯乙酮酸的含量。

The chemistry behavior research of wollastonite indicated that the silicon-potassium fertilizer has a chemical active in organic acid.The factors affecting manurial effect of silicon-potassium fertilizer are not only soil pH and desilicification,but also content and type of organ in the soil.Wollastonite chemistry behavior indicates that silicic acid can be dissolved out from silicon-potassium fertilizer in chlorhydric acid solution if pH of solution is not smaller than 2. The drop of apparent density,increase of DBP sorptive rate and specific surface for leavings indicate that hydrated silicon oxide is polyporous,and those mineralogic feature presignify that silicon-potassium fertilizer has a role of conservation of both Moisture and Fertility and improving soil structure.After active ingredient releasing,silicon-potassium fertilizer leaves half the substance (non-active ingredient)in soil.

熟料单矿物在酸溶液中的化学行为研究表明,硅钾肥矿物在有机弱酸中的化学活性较好,影响硅钾肥肥效发挥的因素是土壤pH值和土壤的去硅化程度,还有土壤有机质的含量与种类;硅灰石在盐酸溶液中化学行为表明,在反应体系pH不小于2的情况下,硅钾肥矿物大量溶出硅酸根组分;溶解残余物表观密度降低、DBP吸着率和比表面积增加表明水合二氧化硅是以多孔形式存在,为硅钾肥具有保水保肥、改良土壤结构的提供了矿物学依据。

In borate or phosphate buffered NaCl solutions with a constant total concentration of borate or phosphate, E_ increases with an increase in pH. With the increase of the concentration of chloride ions, E_ decreases markedly in the test solutions. Moreover, the buffer capacity and concentration of nonaggressive anions in the test solutions also exerts some effects on the crevice corrosion of Type 304 stainless steel. Furthermore, the cooperative inhibition effect of the environmental factors on crevice corrosion was investigated. The potential of crevice corrosion E_(cc shows a strong dependence on a parameter J, which was called as general environmental factor and defined as the product of concentration of nonaggressive anions, pH, buffer capacity and concentration of chloride ions.

在含NaCl 的硼酸或磷酸盐缓冲溶液中,在相同的缓冲溶液总浓度下,E_c随pH 值增加而增加;但随着氯离子浓度的增加,E_c显著降低;另外缓冲容量及其阴离子对304 不锈钢缝隙腐蚀也有影响;最后实验研究了这些环境影响因素的协同影响规律,得出环境综合影响因素参数J,J 由pH 值、缓冲容量、氯离子浓度及其缓冲溶液中其它阴离子浓度定义,缝隙腐蚀电位与参数J 有好的线性关系。

The alkali solution concentration and steam explosion process condition were optimized by testing the solubility of soft cellulose after steam explosion before and after treatment towards aq.NaOH with various concentration. It was concluded that the soft cellulose can dissolve in the 9% aq.NaOH solution completely under the condition of explosion pressure 3.0Mpa and explosion time 60s. At the same time, the influence of sweller-thiourea on the new aq. alkali soluble cellulose/NaOH solution was studied in this paper. The dissolving phenomena and the steam explosion mechanism of soft cellulose were discussed.

本文通过对闪爆前后软木纤维素在不同浓度的稀碱溶液中溶解度的测试分析,优化了碱溶液浓度和最佳闪爆工艺条件,得出在闪爆压力超过3.0MPa,保压时间为60s的条件下,软木纤维素可完全溶解于9%的NaOH稀碱溶液中,并且对助溶剂-硫脲对碱可溶纤维素/NaOH水溶液的增溶效果进行了研究和探索,同时也对溶解机理和闪爆机理进行了分析讨论。

The results of its fluorescence probe showed that when the guanidine hydrochloride concentration in denaturation solution was about 1.0 mol/L,there existed some stable hydrophobic regions,which could interact with a hydrophobic reagent 8-anilino-1-naphthalene sulfonic acid,in the partially folded intermediate of Bacillus amyloliquefaciensα-amylase;with the denaturation concentration increasing,the stable hydrophobic regions disappered.the results of fluorescence quenching using acrylamide and potassium iodide as quenchers showed that using acrylamide as quenchers,with the protein denaturation extent increasing,the number of Trp that can be quenched increased untill all the Trp residues were quenched;Using potassium iodide as quenchers,with the maximum number(8) of tryptophan residues in a partially folded intermediate Bacillus amyloliquefaciensα-amylase molecule could be quenched by potassium iodide;with the denaturation concentration increasing,the number of Trp that can be quenched decreased to 5.the results of their protein electrophoreses and SEC showed that no aggregate or aggregate precipitation of Bacillus amyloliquefaciensα-amylase formed during the whole unfolding/refolding procedure of Bacillus amyloliquefaciensα-amylase induced by guanidine hydrochloride or urea.

ANS外源荧光探针结果表明:盐酸胍诱导的芽孢杆菌α-淀粉酶分子去折叠过程中存在着能够与探针分子1-苯胺基-8-萘磺酸结合的稳定的疏水区域;而随着芽孢杆菌α-淀粉酶分子在盐酸胍溶液中变性程度的加深,这一疏水区域逐步被瓦解。丙烯酰胺和碘化钾猝灭结果表明:在盐酸胍溶液中,随着芽孢杆菌α-淀粉酶分子变性程度的进一步加深,其分子内能够被丙烯酰胺接近的色氨酸残基逐渐增多,直至全部被猝灭。但位于芽孢杆菌α-淀粉酶分子表面的能够被碘化钾猝灭的色氨酸残基,在中间态芽孢杆菌α-淀粉酶分子中数目达到最大的8个,而随着其分子变性程度的进一步加深,反而减少至5个。

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I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

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不要 '夸大' 你的业绩或成果,条件或者技能。