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The results show that the oxidation process of arsenopyrite is speeded up with increasing concentration of FeCl3solution and rising temperature of reaction within the temperature range of 15~35℃, whereas the reaction rate of arsenopyrite is reduced at 45℃, and that the arsenic released from the reaction of arsenopyrite with FeCl3acidic solutions whose concentration is lower than 1×10-4mol·kg-1is in the form of As, which is likely to be soon oxidized into As in the FeCl3acidic solution.

结果显示:在温度为 15~35℃内,毒砂的氧化随FeCl3溶液浓度增加和反应温度升高而加速,而45℃时毒砂的反应速率反而降低;毒砂在与氧化剂FeCl3酸性溶液(浓度小于1×10-4mol·kg-1)反应时释放到溶液中的砷为As,As在FeCl3酸性溶液中很快被氧化成As。

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小,进行综合分析,确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量,测定条件:加入100ml浓度为8.0±0.1%的氢氧化钠,在恒温水浴中煮沸回流6h;采用溶剂萃取法测定JOB-1C中TATB的含量,选择TATB饱和的二甲基甲酰胺为萃取溶剂,用G4坩埚式过虑器进行萃取分离;采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量,通过实验确定了多波长组合:λ=267nm,275nm,283nm,291nm,299nm;朗波—比耳定律的适用范围为PNP浓度:0.005~0.025mg/ml,HMX浓度:0.06~0.30mg/ml;在测定波长下,对PNP、HMX标准溶液的吸光度—浓度进行线性回归,由回归曲线的斜率得出PNP、HMX的吸收系数;根据朗波—比耳定律和吸光度加和性原理,在测定波长下,对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归,回归曲线的斜率即为混合溶液中PNP的浓度。

The alloy catalyst was found to be unstable in the acidic solution because of the electrochemical and chemical dissolution of the catalyst.

发现在酸性溶液中,钯铁合金催化剂对氧还原反应的催化活性不稳定,原因是钯铁合金催化剂在酸性溶液中发生电化学/化学溶解;在碱性溶液中,覆盖在电极表面的钯铁合金催化剂的质量及电化学活性面积在电化学扫描过程中不发生明显变化,保持对氧还原反应的催化活性,证明钯铁合金催化剂在碱性介质中非常稳定。

The polymeric sol is obtained by process of preparing a calcium salt solution, containing calcium ethoxide dissolved in organic acid, and a phosphate solution, containing triethyl phosphite or triethyl phosphate dissolved in the organic acid, mixing the calcium salt solution with the phosphate solution to produce a mixed solution, and aging the mixed solution.

本发明的磷酸钙化合物的聚合物溶胶是通过如下步骤制备的:制备含有溶解在有机酸中的乙醇钙的钙盐溶液和含有溶解在该有机酸中的亚磷酸三乙酯或磷酸三乙酯的磷酸盐溶液;及将该钙盐溶液和该磷酸盐溶液混和制得混合溶液,并老化该混合溶液。

Typically,0.2 mmol of Cd solution, and 0.4 mmol of MPA solution were mixed in a 40 ml solution and the pH of the solution was adjusted to 10.0 by solution was palced in a three-necked flask and was deaerated.

通常情况下, 0.2浓度的镉溶液,和0.4浓度的MPA的混合溶液中40ml溶液和pH值的溶液是调整,以10.0的溶液放置在是在三口瓶中,并除去溶液中的气体。

Typically,0.2 mmol of cd solution, and 0.4 mmol of mpa solution were mixed in a 40 ml solution and the ph of the solution was 二氰基丙酸乙酯 to 10.0 by solution was palced in a three-necked flask and was deaerated.

通常情况下, 0.2浓度的镉环硫乙烷,和0.4浓度的mpa的混合溶液中40巯基丙酸甲酯溶液和ph值的溶液是调整,以10.0的溶液放置在是在三制作乙酸钙中,并除去溶液中的气体。

A preparation method of the visible-light photocatalyst Bi2WO6 nano-powder is characterized by comprising the steps as follows:(1) the selection of raw materials;(2) bismuth nitrate Bi(NO33 question mark 5H2O is added into a citric acid solution to obtain the citric acid solution containing white sediment;(3) EDTA is added into ammonia water which is then added dropwise with the citric acid solution containing the Bi(NO3)3 question mark 5H2O so to obtain a solution of bismuth;(4) the solution of bismuth is added with (NH4)6W7O24 question mark 6H2O solution to form a precursor solution which is then stirred, dried, coked, cooled and ground to obtain decarburized powder;(5) the decarburized powder is roasted for 2h to 4h under 450 DEG C to 550 DEG C to obtain the visible-light photocatalyst Bi2WO6 nano-powder.

可见光催化剂Bi 2 WO 6 纳米粉体的制备方法,其特征在于它包括如下步骤:1原料的选取;2将Bi(NO 3 ) 3 5H 2 O加到柠檬酸溶液中,得到含有白色沉淀的柠檬酸溶液;3将乙二胺四乙酸加到氨水中,并缓慢滴加入含有Bi(NO 3 ) 3 5H 2 O的柠檬酸溶液中,得铋的溶液;4将(NH 4 ) 6 W 7 O 24 6H 2 O溶液加入上述铋的溶液中,组成前驱液;搅拌,干燥,焦化,冷却后,研磨,得去碳的粉体;5将去碳的粉体在450~550℃下焙烧2~4h后,得到可见光催化剂Bi 2 WO 6 纳米粉体。

According to the theoretical analysis,the results show that the fresh air dehumidified before mixed with return air is more energy-saving among many kinds of realization shapes.Indoor exhaust used as regeneration air can also reduce the total energy consumption of the system.It may enhance the regeneration property when the recuperator is adopted to absorb energy to preheat the dilute liquid.

对此空调系统进行理论分析,得出如下结论:在溶液除湿蒸发冷却空调系统的多种实现形式中,新风经除湿后与回风混合比新回风混合后再除湿节能;将室内排风返回溶液再生器,进行热湿交换,既可加强对处理空气的预冷,回收排风冷量,又可提高再生器的效率,降低系统能耗;把回热器吸收除湿浓溶液中的部分热量用于溶液再生器的稀溶液预热,可以提高溶液的再生性能。

The results of experiment show the glass fiber dealed with by KH550 is notscattered in these solvents such as the water, the component solvent of phenol andtetrachloroethane, and ethyl alcohol solution of KH550, but it is evenly scattered inthe solution of PET, the concentration of which has great effect on the dispersion ofglass fiber. The glass fiber can' t be scattered when the value of consistency is below0.2664g/ml, and 0.75g glass fiber can be scattered in 100ml solution.

本实验通过对玻璃纤维分散的研究发现,玻璃纤维(长 3mm,经 KH550 处理)在水、苯酚/四氯乙烷、KH550 的乙醇溶液中都不能分散,而在 PET 的苯酚/四氯乙烷溶液中能均匀分散,且溶液的浓度对分散性影响很大,当浓度。2664g/ml 时,玻璃纤维不能分散,玻璃纤维在 100ml 浓度为 0.4444g/ml 的溶液(90℃下,PET 的饱和溶液)中的最大分散量为:0.75g。

As for watersoluble hydrophobically associating polymer, it has not been reported as a foam stabilizer.

由于聚合物在溶液中的不溶解性,使其研发成为一种泡沫储存剂。

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