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We have developed a simple and easy-handling procedure for copper-catalyzed cyanation of aryl halides using K4[Fe_6] as the cyanide source. The present procedure has ligand- and base-free advantages, and was accomplished under the conditions of exposure to the air without degassing of the solvent.4. We carried out the selective control of preparation for phenyl ether and phenol from iodobenzene with 10 mol% of Cu_2·H_2O as the catalyst under the condition of exposure to air.

这个程序有无配体无碱的好处,并能够在暴露于空气的条件下进行,溶剂也不用脱气。4、空气气氛下,用10 mol%的Cu_2·H_2O催化碘苯偶联,实现了制备二苯醚和苯酚的选择性控制:即在有(来源:Aa955BC55论文网www.abclunwen.com)机溶剂NMP中实现了碘苯直接制备二苯醚的Ullmann反应,在H2O中实现了碘苯直接制备苯酚。

If the geoid or quasi-geoid model is given, GPS can be used directly to determine orthometric height or normal height, which can take the place of the traditional geometric leveling and make the seperation mode of plane control network and elevation control network in traditional geodesy become a history.

在高精度、高分辨率大地水准面模型的支持下,利用GPS技术可以直接测定正高或正常高,从而取代传统繁琐的水准测量方法,使得平面控制网和高程控制网分离的传统大地测量模式成为历史。

This method can make sure the structure radiant sound status in total noise and the detail phonate part quickly and correctly.(3) Study on the control mechanism of structure noise radiated from rotary machines, we build a common model of rotary machine structure noise analysis relied on the general characters of rotary machines. Based on this model, we analyzed various influence factors to structure radiant noise using the union of revolution and numerical calculation method. We found that the joint stiffness between the rotor and the frame is the most sensitive parameter of structure radiant noise by calculating and analyzing.

根据本文对于旋转机械结构噪声控制技术的研究结果和惯性振动筛工作的特殊要求,对有关参数的选择进行了讨论,并通过试验为降低惯性振动筛噪声找到了两个新的方法:即,在轴间相对运动要求不高的情况下,可以在激振器与筛体之间安装一组减振器,通过适当选取减振器参数,既可以使机体在工作频率附近获得稳定振幅,保证振动筛正常工作,又可以使机体的高频响应减小,降噪效果显著;反之,如果轴间相对运动精度要求(来源:1aABC论文网www.abclunwen.com)较高,可以采用空心滚动体轴承,在保证滚动体强度的条件下也可以获得较好的降噪效果。

Stability, robustness and oscillation of differenct uncertain time-delay systems are analyzed. Synthetical time-delay control schemes are proposed, including robust stabilizing control, variable structure control, robust dissipative control and so on. Industrial time-delay system model are established based on the theorematic results and industrial requirements. Pratical control algorithms and APC-software are developed and applied to practical process successfully.

在国家自然科学基金资助下,本项目对各类不确定时滞系统的稳定性分析、振动性质分析、鲁棒镇定控制器设计等问题进行了全面的理论分析,并结合流程工业生产过程的特点和企业需求,建立工业过程时滞系统模型,开发实用型的控制算法和先进控制软件,在一些典型的工业生产过程进行了成功的应用,取得了显著的经济效益和社会效益。

Permanent Magnet Synchronous Motor driven by triphase sinusoidal current is studied object in this paper. The movement equtions in several coordinates are set up based on the analysis of electromagnetism restricted relation.

本文以三相正弦波驱动的永磁同步电机为研究对象,在深入分析其内在电磁约束关系的基础上,给出了不同坐标系下的运动方程,根据其数学模型,确定了电动车用电机在旋转坐标系下的矢量控制方案。

Supporting by the software developed by author, the system can carryout peg-in-hole assembly operation along arbitrary direction with high speed and reliability even under the condition of unchamfered parts.

在作者所开发的控制软件支持下,该系统能够在零件不具备倒角的情况下高速、可靠地完成沿任意方向的精密销孔装配作业。

PID control has been successfully used in many fields such as aviation, spaceflight, missile and other industry control system. The study object in the thesis is missile that flies hedgehopping over sea at minimum altitude. Many interference problem must be solved when missile flies at minimum altitude, otherwise the missile would be dangerous of bumping into the sea under the circumstances of bad weather and wave. The different kinds of interference factors are contradictions with requirements of control system, which can not be solved by PID control.

尽管在航空、航天、导弹以及其它工业控制领域PID控制曾经应用的十分普遍和成功,但对本文所研究的某型超低空掠海飞行的导弹,要实现超低空飞行必须处理好各种干扰问题,否则,在恶劣的气象和海情的条件下便有使导弹与海浪相撞的危险。

Face this kind of situation, the author thinks not to answer to the control that funds overspends from production very busy season just begins, and should be when plan of funds of year of make known to lower levels of management department of superior of the beginning of the year, build a rigorous plan management and budgetary management system, combine the characteristic of highway conserve branch, act on the principle of keep expenditures within the limits of income, making overall plans and take all factors into consideration, year funds the plan presses different content, with the work out estimated method, below the analysis, premise that forecast, undertake index is decomposed, layer upon layer fulfil, fore-and-aft decompose team and group, each accessary production unit, transverse fulfil each room, departmental door, implement pyramid form manage by different levels, make every every branch, worker has index, responsible, form fore-and-aft after all, transverse control a network to stagger of edge, freely.

面对这种局面,笔者认为对经费超支的控制不应从生产大忙季节才开始,而应在年初上级治理部门下达年度经费计划时,就建立起一套严格的计划治理和预算治理制度,结合公路养护部门的特点,本着量入为出、统筹兼顾的原则,将年度经费计划按不同内容,用编制预算的方法,在分析、猜测的前提下,进行指标分解、层层落实,纵向分解到班组、各附属生产单位,横向落实到各股室、各部门,实行金字塔形的分级治理,使每个部门、每个职工都有指标、有责任,形成一个纵向到底、横向到边、纵横交错的控制网络。

According to the change of the kinds of elements content in slag, F in slag volatilizes in the form of KF and NaF, KF volatilizes much more easily than NaF, KF plays a leading role in the F volatilization, theoretical analysis shows that the saturation vapour pressure of KF in the test slag is 31. 4 times of NaF; when F content is far more than K, KF volatilization is first order grade reaction, it is dominated by K content, the apparent activate energy is 275. 30KJ/mol.

4依据对含氟熔渣中高温条件下(1450℃、1505℃)的各种元素含量的变化情况,发现氟在熔渣中是以碱金属氟化物挥发,并且,KF比NaF具有更好的挥发性,在氟的挥发中占主导地位,理论研究也证明,在1505℃试验组成的熔渣中,KF的饱和蒸气压是NaF的31.4倍;在含氟量远大于钾含量的情况下,KF挥发为一级反应,受钾浓度控制,其表观活化能为275.30KJ/mol。

When the hydraulic pressure power supply stops or controls the solenoid valve opens, in driving pliers' pressure oil pressure vanishing, the piston under the precompression brake block spring's function rapidly promotes, affects on the friction liner and presses to is applied the brake the body, simultaneously the driven pliers in the driving pliers and under connecting bolt's function, lead through the glide guide pillar's function rub the liner to press to are applied the brake the sleeve to become the brake.

当液压动力源停止或控制电磁阀打开时,主动钳内的压力油压力消失,活塞在预压的制动弹簧的作用下迅速推出,作用在摩擦衬垫上并压向被制动体,同时从动钳在主动钳和连接螺栓的作用下,通过滑动导柱的作用带动摩擦衬垫压向被制动体完成制动。

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The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了,排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意,我建议我们在价格上大家各让一半。

After an hour and no pup, look for continued contractions and arching of the back with no pup as a sign of trouble.

一个小时后,并没有任何的PUP ,寻找继续收缩和拱的背面没有任何的PUP作为一个注册的麻烦。