固质

Methods Using acetamide as the internal standard,extraction column and extraction conditions of fluoroacetamide from blood and urine samples were optimized by comparing the extraction efficiency of different solid-phase extraction columns and the effects of experimental conditions on recovery.

选择乙酰胺为内标，通过比较不同固相柱的萃取效率和不同条件对回收率的影响，优化用于血和尿样中氟乙酰胺萃取的固相柱和提取条件，利用氟乙酰胺与乙酰胺质谱图的分子离子峰面积之比与氟乙酰胺浓度的定量关系，建立血和尿样中氟乙酰胺鼠药的GC/MS定量分析新方法。

Based on the first heat treatment, the second ball milling and calcining favor the osculation and mass transfer of the reactants in the second solid state reaction, and compared with one-step method, the density of resultant LiFePO4/C is ameliorated.

在一次热处理的基础上，二次球磨和烧结有利于第二次固相反应过程中反应物质的接触和传质，较一步固相法提高了生成的LiFePO4的振实密度。

Based on the assumptions of semi logarithmic relationship between coefficient of permeability and void ratio as well as the relationship between effective stress and void ratio of soil, the method of Lie Group Transformation is applied to solve the non linear partial differential equation of large strain consolidation of homogeneous saturated clay in semi infinite domain.

基于有效应力与孔隙比以及渗透参数与孔隙比之间的关系的一些假定，采用李群变换求解考虑材料非线性和几何非线性的半无限均质土体大变形固结非线性偏微分方程，得到了一个不考虑自重固结的完全解析解。

Most endothelial cells fell off, elastic fibre autolyze; the number of SMC decreased, some SMC nucleus contracted completely or depressed, typical apoptosis body were seen in later stage, muscle silk autolyzed and disappeared mostly; in outer layer saw much collagenic fiber, arranged unorderly; inflammation cells were seen in the aneurysm wall(hypertrophy cell et al.).

多数瘤壁的内皮细胞溶解脱落，不连续，弹力纤维自溶；动脉瘤血管壁均可见SMC明显减少，较多SMC染色质边聚、固缩，部分SMC核全部固缩或出现不规则凹陷，SMC核胞浆或胞核部分出现脱落或裂解成碎片，晚期可见典型的凋亡小体出现，肌丝大都自溶消失：外膜可见大量的胶原纤维，排列较紊乱；瘤壁还可见炎性细胞浸润。

Metarhizium anisopliae was an important entomopathougenic fungus for insect pest control. Authors studied the factors affecting conidial production of the fungus in the solid-phase of liquid-solid diphase process Results showed that vermiculite and rice hull were fine carriers for the fungal culture.

研究了昆虫病原真菌绿僵菌R8-4菌株液固两相法培养过程中固相培养阶段的条件，包括培养基载体、接种量、接种后基质含水量、培养过程中的温度、光照、通气量等因素对产孢量的影响。

In group 35mg/kg, the karyopyknosis of the tubular epithelial cells of cortical increased. The structure of epithelium disappeared, that of glomcrulus disorganized and medulla were involved. In group 25 mg/kg and 30 mg/kg, severity of pathological changes were between that of group 20 mg/kg and group 35 mg/kg.

35mg/kg染毒组皮质部小管上皮细胞细胞核固缩增多，上皮细胞结构消失，少数肾小球结构紊乱，髓质部小管细胞核固缩，管腔消失。25mg/kg和30mg/kg染毒组病理损伤程度介于上述两组之间。

We found out one kind of new orange-red long afterglow material La2O2S: Eu3+, Mg, Zr.2 In the phosphor Gd2O2S, Mg, Ti which was prepared by high-temperature solid-state method, the orange afterglow phenomenon can be seen after illuminated with UV light.3 Using the high-temperature solid-state method, Gadolinium oxysulfide phosphors doped with rare earth ions were synthesized. We can observe the red or orange phosphorescence in Gd2O2S doped with Eu3+, Sm3+, Tm3+, Yb3+, Dy3+, Er3+, Nd3+or Ho3+. This is a new result of the long afterglow phosphors research.4 Using the microwave radiation method, the new Sm3+ doped gadolinium oxysulfide phosphor, which has the orange-red long afterglow emission after illuminated with UV light or visible light, was synthesized for the first time.5 In fluorescent materials YOX doped with europium ions, the long afterglow phenomenon wasnt observed but the blue luminescence of Eu2+ and red luminescence of Eu3+ are simultaneously examined. This is a new result of the valence stability and change of Eu2+ in yttrium oxyhalide .We systematically studied the effects of the host, addition agents and reaction atmosphere on the valence change and fluorescence property of europium ions.

经过系统的研究总结得到以下的结论与成果： 1采用高温固相反应法合成了一系列稀土离子掺杂的硫氧化镧发光粉，发现了该体系中Eu~(3+)的长余辉发光，从而得到一种迄今未见文献报道的红色长余辉发光材料：La_2O_2S：Eu~(3+)，Mg，Zr； 2在Gd_2O_2S，Mg，Ti磷光粉中观察到橙色的长余辉发光现象； 3采用高温固相反应法合成了一系列稀土离子掺杂的硫氧化钆磷光粉，在掺杂Eu~(3+)、Sm~(3+)、Tm~(3+)、Yb~(3+)、Dy~(3+)、Er~(3+)、Nd~(3+)、Ho~(3+)的Gd_2O_2S中观察到红色和橙色长余辉发光； 4首次采用微波法合成了Gd_2O_2S：Sm~(3+)，Mg，Ti磷光粉，该磷光粉经紫外或可见光激发后呈现明显的橙红色长余辉发光； 5在YOX中同时观察到Eu~(2+)和Eu~(3+)的发射，系统研究了基质、添加剂及反应气氛对Eu价态和发光的影响。

The experimental products include crystal phase quartz, feldspar (alkila-feldspar, albite, K-feldspar), zinnwaldite and topaz, a melt phase and a trace vapour. The solid products were been studied by optics method, electron microprobe and X-ray analysis. The results show that liquidus temperature raises slightly and solidus temperature falls down obviously and that the upper temperature limit raises for the stability field of quartz and topaz, and falls down for the stability field of alkila-feldspar as F contents in crease.

实验淬火产物包括结晶相石英，长石(碱性长石，钠长石、钾长石)，铁锂云母和黄玉及玻璃相和微量流体，对固相淬火产物进行了系统和详细的显微观察及电子探针和x射线分析，研究了F对钠长花岗岩液、固相线温度、相关系和相组合的影响和含F钠长花岗岩的结晶序列和熔体演化、F在流体和熔体之间的分配及F对花岗质熔体结构的影响，对含黄玉矿物组合进行了一系列热力学矿物平衡计算，获得如下重要结论

The first pan of this dissertation involves: the study of the interaction of DNA and a kind of neurotransmitter, aderenaline; development of a novel method for immobilization of DNA and methylene blue on micro-hollow paraffined graphite electrode and paraffin encapsulated micro-hollow-array carbon disk electrode M (h ApCE ; investigation of the three dimensional electrode.

本论文分两部分，第一部分包括：研究了DNA和神经递质肾上腺素的相互作用，并通过电化学氧化腐蚀充蜡石墨电极、碳纤束充蜡电极发展了一种固载DNA的新方法，提出了三维固载的机理，并在电极的填充介质和电极上修饰不同的物质两方面对该三维电极进行了研究。

Clover pump, butterfly pump, stainless steel volume pump, 10000 pump with the delivery, milk uniform machines, screw, titanium dioxide slurry pumps, single - thick screw pump, pneumatic slurry pumps (leather spray pump, beating pump, insert barrel pumps, pump thick), high-shear dispersion emulsion pump, solid-liquid mixing pump, titanium dioxide slurry pump, high pressure are quality pumps, beverage pump, plate heat exchangers, a variety of filtration equipment, wash tank ball, cleaning spinning ball, automatic spray the ball and sanitation level clamp, live joints, valves, pipe fittings, products, services, covering industry, agriculture, transportation, energy, construction, light industry, automobile, shipbuilding, mining, metallurgy, ceramics, Titanium, Key Laboratory of universities and scientific research institutes, aerospace and other areas of national economy, an important industry for more than 140 countries and regions in the world to provide specialized service.

专业致力于设计、开发、制造、销售食品机械设备、制药机械设备、化工机械设备、乳品饮料机配套设备及机电类产品：JM胶体磨［colloid mills立式胶体磨、分体式胶体磨、卧式胶体磨、管线式胶体磨、全封闭式胶体磨、双冷却式胶体磨、分散均质胶体磨］、多功能研磨机、钛白粉研磨机，多功能研磨机组、湿式超微粒粉碎机、胶磨机、磨浆机、水粉混合器，THJ-L/F系列混合机、MC18混合机、打浆机、均质机、高剪切乳化均机、ZB3A系列胶体泵（转子泵、凸轮泵、三叶泵、蝶型泵、不锈钢容积泵、万用输送泵）、乳匀机、螺杆泵、钛白浆料输送泵、单螺杆浓浆泵、气动浆料泵（皮革喷浆泵、打浆泵浦、插桶泵、浓浆泵）、高剪切分散乳化泵、固液混合泵、钛白粉浆料泵、超高压均质泵、饮料泵、板式换热器、各种过滤设备、洗罐球、清洗旋转球、自动喷球及卫生级卡箍、活接头、阀门管道配件，产品服务领域覆盖了工业、农业、交通、能源、建筑、轻工、汽车、船舶、矿山、冶金、陶瓷、钛业、高校科研院所重点实验室、航空航天等国民经济重要产业领域，为全球140多个国家和地区提供专业化服务。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。