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In this paper a method was developed for simultaneous determination of four β-agonists by gas chromatography/mass spectrometry in pork tissues.

本文建立了猪肉组织中β-激动剂多残留的固相萃取-气相色谱-质谱检测方法。

Based on Darcys law and material balance principle, mathematical model of three-dimensional three-phase was derived in porous medium with artificial fractures, and the gravity was considered in the model.

根据物质平衡原理和达西定律,考虑基质和人工裂缝作用下三维三相渗流模型,并考虑了重力作用影响,结合应变孔隙度模型、应变渗透率模型,建立了流固耦合整体压裂数学模型。

The herbicides in the sample was extracted with ethyl acetate. The extract was decanted into a flask through a filter paper, then the filtered solution was concentrated to dry. The dry sample was dissolved and added to 5 mL with acetone-n-hexane (30:70, V/V). It was cleaned up by Florisil, concentrated again. The sample was dissolved and adjusted to 1mL with acetone.

匀浆后的草莓试样用乙酸乙酯进行提取,提取液经滤纸过滤后收集,再浓缩蒸干,用丙酮:正己烷(30:70, V/V)溶液溶解至5ml,经Florisil固相萃取柱净化,吹干后用丙酮定容,供气相色谱-质谱联用仪进行测定。

The circular centrifugal flotation cell has many originalities on the pulp aeration, air bubble mineralization, air pulp flow format in the ring shaped tank of the cell, feed method ect, due to the results of fluidics and turbulence and the action of centrifugal and gravitational force ect.

新型高效圆形离心浮选机充分发挥了湍流射流及离心—重力力场的作用,使其在矿浆充气、气泡矿化、浮选槽内矿浆流动形式、给料方式等方面独具特色。在普通喷动床环形区底部引入&充气&可消除环形区底部颗粒&死区&的影响,并能改善环形区气固间的热、质传递。

It was found that pathological changes could be demonstrated in villi of small intestine, lamina propria of stomach and myocardial cells in case of mice orally administrated with RV, while in case of mice intra-abdominally injected with RV, pathological changes could be demonstrated also in liver and kidneys in addition to the changes mentioned above.

结果 光镜下:RV口服组小肠绒毛、胃固有层、心肌细胞有改变;RV腹腔注射组除上述改变外,肝,肾也有改变;电镜下:肝细胞线粒体肿胀、凝集病变尤为明显,细胞核固缩-崩解,粗面内质网扩张,肝细胞中存在大量脂滴和空泡;毛细胆管明显扩张,微绒毛脱落。

In the contaminated lard sample, 6 organic compounds have been thus identified to be the raw materials or byproducts in the production of organic tin compounds. Based on the identified contaminants, it can be postulated that the chemical structure of the organic tin compound is dibutyltin-bis-(2-isooctyl thioacetate). The method is simple and precise, and has not been reported in the local literature.Keywords Organic tin compound, Lard, SPME-GC-MS

经过摸索研究,采用固相微萃取方法富集挥发性杂质,直接注入色谱中,经色谱分离,质谱测定,确定了杂质的结构,由杂质成分推断生产有机锡所用的原料,然后判断合成路线,最后确定有机锡的结构,从有毒猪油中鉴定出2-巯基醋酸异辛酯、双(2-醋酸异辛酯)二硫、双醋酸异辛酯硫醚等6种与有机锡有关的杂质,并与相应的有机锡工业品对照,发现工业品中也含有这些杂质,与其合成过程的原料及副产物相符,从而确定有机锡化合物为二硫代醋酸异辛酯二丁基锡。

All of the above characteristics as well as poorcrystallized, abundant peridotite inclusions, few xenocrysts, and elements covariation trend indicate that the Tianheyong basalts were solidified from primitive basaltic magma.

上述所有特征以及岩石结晶程度低、富含橄榄岩包体和少量捕虏晶、元素变异关系等均表明,天和永玄武岩是原生玄武岩质岩浆固结的产物。

The volatile compounds of silkies on feeding medlar and feeding stuff were extracted and identified with solidphase micro extraction and gas chromatography-mass spectrum 79 from silkies on feeding medlar and 61 from silkies on feeding stuff.

采用固相微萃取法,结合气相色谱-质谱技术对甘肃景泰条山农场的枸杞园散养和饲料笼养乌骨鸡肉的挥发性物质进行检测分析。

This produces particles called pions , the 'glue' that holds a nucleus together, and some of these tiny particles degrade into gamma rays.

这一过程产生的粒子叫做介子,介子象胶质封固在原子核的周围,其中有些发生衰变,成为伽马射线。

Wistar rats were administered with nimetazepam and nitrazepam,respectively,and urine samples winthin 24 h were collected.

给大鼠急性喂食硝基安定和尼美西泮,收集24 h内尿液,尿样用β葡萄糖醛酸酶水解,Oasis HLB柱固相提取,以DB-35 MS柱为分离柱,气相色谱-质谱联用检测。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。