固质

This project is going to investigate the crystallization of polymers in scCO2 and to study the polymorphism and solid-phase transition of crystallizable polymers with different molecular structure and different tacticity in scCO2 for accumulating the fact of crystallization of polymers in the titled surrounding, revealing the rule of solid-phase transition of polymers in scCO2 and exploring the mechanism responsible for these phenomena.

本项目研究聚合物在scCO2中的结晶行为，研究不同分子结构、不同等规程度聚合物的同质多晶现象与固相转变，积累现象、寻找规律、探求机理。

MethodsThe constituents of volatile oil from Dictamnus dasycarpus was investigated by SPME/GC/MS.

方法利用固相微萃取/气相色谱/质谱联用技术对白鲜皮的挥发油成分进行了研究。

ObjectiveTo analyze constituents of volatile oil from Dictamnus dasycavpus.

作者：吴琴，叶冲，宋培浪，韩伟白鲜皮；，，挥发油；，，固相微萃取；，，气相色谱/质谱联用摘要：目的分析白鲜皮挥发油成分。

In a climatically controlled chamber (28±1℃, L16:D8), E. splendens was planted in pots containing mixed vermiculite and perlite without Cu. At about 220 d after seeding, plants (around 65 cm in height) were used to collect their volatile using SPME. Eleven chemicals were identified using GC-MS, p-pinene, D-limonene, elsholtzia ketone, dehydro elsholtzia ketone,γ-elemene, humulene, caryophyllene, a-caryophyllene, and three sesquiterpenes. The most abundant volatiles were caryophyllene and y-elemene, followed by humulene and a-caryophyllene.

室内在不含Cu的蛭石和珍珠岩混合基质中种植海州香薷，用固相微萃取法收集健康植株(株龄220余天，株高65cm左右)的挥发物，采用GC-MS法识别出11种主要组分，从中鉴定出β-蒎烯，D-柠檬烯，香薷酮，脱氢香薷酮，γ-榄香烯，蛇麻烯，石竹烯，α-石竹烯(α-caryophyllene)，以及三种倍半萜类化合物，其中石竹烯和γ-榄香烯含量高，其次为蛇麻烯和α-石竹烯。

Qualitative and quantitative analyses was carried out by gas chromatograph-flame photometric detector. This article focus on optimizing the absorbent, elute and material for secondary cleaning up.

通过对基质固相分散吸附剂、洗脱剂、净化材料与方式的优化，建立了油菜籽中5种常用有机磷农药残留分析的前处理方法。

The main enzymolytic products from the reaction of VS on torpedo acetylcholinsterase were studied by means of GC-MS.

本文用气相色谱及气相色谱-质谱联用的方法，对VS与电鳐乙酰胆碱酯酶固相酶作用后其含硫、氮部份的主要酶解产物进行了分析鉴定。

In this research, we used Trifluoroacetic anhydride as a derivatizing agent to esterify the trace glycerol in biodiesel, followed by the determination of trace glycerol using microwave assisted headspace SPME extraction technique combined with GC-ECD.

本研究利用三氟醋酸酐与生质柴油中的微量甘油进行酯化反应，反应后的衍生物以本实验室开发的微波辅助顶空固相微萃取装置采样，并以气相层析仪搭配电子捕捉侦测器作分析。

In this study was carried out in the greenhouse of Shandong Agricultural University,'Fragaria×ananassa Duch.

中文摘要：本研究在山东农业大学日光温室进行，以盆栽'丰香'和'罗莎'草莓为试材。采用顶空固相微萃取-气谱-质谱联用技术测定果实中芳香物质，DTNB比色法测定果实醇酰基转移酶活性。

The solid-phase microextraction technique was evaluated for the determination of furoic acid and creatinine in urine. For furoic acid, the alkaline hydrolysis step was first performed to hydrolyze the furoic acid-glycine conjugate to free furoic acid.

本研究利用固相微萃取(solid-phase microextraction， SPME)动与气相层析质谱仪之结合，建立尿中呋喃甲酸与肌酸酊的分析技术，以提供评估呋喃甲醛暴露之生物侦测工具。

(1)PAL is better entrapped by PAG with a T∶C ratio of 8∶30.(2)PAL immobilized by glutaric dialdehyde on Bio-Gel P-300 is better than by CDC.(3)The best one is the dehydration and redehydration method.(4)Immobilized and permeated PAL active yeast cells are resistant to trypsin digestion and retain its PAL activity.

(1)固定化酶活性采用T∶C比为8∶30明显高于8∶19；(2)以戊二醛将PAL固定于Bio-GelP300优于用DCD固定化的酶；(3)质脂体包被中以脱水再加水法对酶活性影响较少，脂类组成以磷脂酰胆碱：胆固醇：磷脂酰丝氨酸比值7∶2∶1最好；(4)固定化PAL活性酵母细胞能较好地抵抗人工肠液中胰蛋白酶的水解作用，亦能明显降低苯丙氨酸的浓度。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。