固缩的

The synthesis of diphenylamine from aniline-phenol by liquid phase condensation in the presence of Pd/C catalyst was studied.

研究了在Pd／C催化剂存在下，通过液／固催化缩合反应由苯胺和苯酚合成二苯胺的方法。

The Catalyst used for preparation of carbodiimide from condensation of isocyanate were reviewed in this paper, including phosphorus-containing heterocycle compounds, phosphonate,organic metal compounds and polymer-grafting solid catalysts.

综述了异氰酸酯缩合生成碳化二亚胺催化剂的开发现状，包括磷杂环化合物、磷酸酯类化合物、金属有机化合物、聚合物接枝固相催化剂4大类。

ABSTRACT Immobilized penicillin acylase (from E.coli) was used to catalyze 7 phenylacetamido 3 E propenyl cephalosporanic acid hydrolyzation into 7 amino 3 E propenyl cephalosporanic acid. Then, trans APRA was acylated with hydroxyethyl ester of 4 hydroxy D phenylglycine to obtain trans cefprozil.

以7 苯乙酰氨基 3 E 丙烯基 3 头孢菌素 4 羧酸为原料，在青霉素酰化酶作用下，首先酶法水解得到3 E 丙烯基 3 头孢菌素 4 羧酸，过滤固相酶，滤液调pH分离得到反式APRA固体；在青霉素酰化酶作用下，反式APRA再与对羟基苯甘氨酸乙二醇酯缩合，得到反式头孢丙烯；酶法合成所得的产品与进口反式头孢丙烯对照品一致。

The white loquat (Eriobotrya japonica Lind1. cv. Guanyu) fruit was treated with hot air of 38℃ for 24 h and 48 h, and then stored at a low temperature. The changes of fruit quality were studied by analyzing the total soluble solids, titratable acidity, loss weight, and wrinkled skin during storage.

方法］在枇杷贮藏前，进行了24和48 h 38℃热空气处理，并检测在低温贮藏下的可溶性固形物含量、可滴定酸含量、失重以及皱缩等的变化。

To synthesize the octreotide, Phe-Leu-Glu-Glu-Leu and C_(15)H_(31)-CO-Lys-Thr -Thr-Lys-Ser peptides, the strategies are as followings: Fmoc- group as protective group for α-NH_2; TBTU, DIEA and HOBt as coupling reagent; and ethanedithiol -phenol - thioanisole - H_2O - TFA ( 2.5:5:5:5:82.5 , V/V ) as cleaving solution.

采用Fmoc固相合成法，以苯并三哗四甲基脲四氟硼酸盐、二异丙基乙胺和1-羟基苯骈三氮唑为缩合剂；苯酚—乙二硫醇—苯甲硫醚—水—三氟乙酸(5：5：2.5：5：82.5，V/V)为切割试剂，合成了奥曲肽、Phe-Leu-Glu-Glu-Leu及C_(15)H_(31)-CO-Lys-Thr-Thr-Lys-Ser三种小分子多肽，并对奥曲肽的合成规模进行了放大。

The experimental method and reaction conditions for synthesis of acetals and ketals on more than 40 catalysts such as solid superacids、 heteropoly acids、 con-exchange、 resins、 molecular sieves、 niobic acid、 vitamin C、 iodine、 sulfate、 chloride、 montmorillonite and etc.

综述了固体超强酸、杂多酸、固载杂多酸、脱铝超稳沸石、树脂、分子筛、铌酸、漆酚衍生物、维生素C、碘、硫酸盐、氯化物、蒙脱土等40多种催化剂催化合成缩醛的方法和反应条件。

Using silicotungstic acid as catalyst with the catalyst supported on active carbon,2-methyl-2-ethyl-acetic-1,3-oxathiolane(targeted compound I,an aroma compound with apple flavor )was synthesized by the reaction of ethyl aceto-acetate and 2-mercapto-ethanol.

以活性炭固载硅钨酸作为催化剂，用乙酰乙酸乙酯与巯基乙醇缩和合成了具有浓郁苹果香气的香料化合物2-甲基-2-乙酸乙酯基-1，3-氧硫杂环戊烷。

In this thesis, the tripeptide GHK has been synthesized by liquid-phase method and octpeptide Eptifibatide by solid-phase method. Coupling agents and purification problem have been studied in the process of peptide synthesis.

本论文分别采用液相法和固相法合成了具有药用价值的三肽GHK及八肽Eptifibatide，研究了多肽合成过程中缩合剂及纯化等问题。

The characteristics of the salt formation in Tarim Basin is deep, high temperature and high pressure, easy to result in the undergauge, collapse, drill bit or pipe sticking.

针对塔里木盆地石炭系盐层埋藏深，温度高，地层压力大，极易发生&缩径、坍塌&，造成卡钻，同时由于盐岩层的塑性蠕动，形成不规则井眼，甚至造成套管挤毁变形事故，井身质量难以控制，固井质量难以保证等问题，通过对同类型已钻井进行总结分析，提出了一系列钻井技术措施，并在T726井严格实施。

Chapter 2: Four kinds of condensations of aromatic amine with benzaldehyde derivatives were obtained by solid phase synthesis. Their structures were identified by element analysis and 1H NMR spectroscopy. Their SHG properties, fluorescent and thermochromic properties were also tested.

第二章：通过室温固相反应合成了四类苯甲醛缩芳胺希夫碱衍生物，用元素分析和核磁共振对其结构进行了确定，并测试了它们的非线性性质、荧光性质以及热致变色性质。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。