回流

The fluid field in the atomizing-combustion chamber can be carved up as three areas: inside circumfluence area, circumvolve shooting fluid area and outside circumfluence area.

燃烧室流场可分为内回流区、旋转射流区和外回流区3大场区。

The method comprises following steps: taking diphenol and 3- trifluoromethyl- 4- chloronitrobenzene as raw material, salt precipitating for diphenol and potash, refluxing with water- containing toluene, reacting with 3- trifluoromethyl- 4- chloronitrobenzene and getting dinitro monomer; taking dinitro monomer, ferro powder and HCl as raw material, ethanol and water as disslovant for refluxing and ethanol recrystallization, getting fluorine- containing aromatic diamido monomer.

合成方法是以二酚与3-三氟甲基-4-氯硝基苯作原料，先将二酚与碳酸钾成盐，甲苯带水回流反应，然后与3-三氟甲基-4-氯硝基苯反应制得二硝基单体；再以二硝基单体，铁粉，HCl为原料，乙醇和水做溶剂，回流反应、乙醇重结晶，得到含氟芳香二胺基单体。

The results showed the feasibility of the continuous fermentation system with full distillage recycle.

结果表明：进行一定时间的酒糟滤液全回流的连续回流发酵是可行的，但最大稀释率不宜大于0.35 h-1，此时连续发酵的生产强度为22.1 g/，酒精产量为

The optimum extraction conditions for gingerol were identified as the follows: 70% ethanolas solvent, ratio of material to liquid as 1:12.5, synergistic extraction time 60s with ultrasound wave and microwave for one time.

最佳工艺条件：70%乙醇为溶剂；料液比1：12.5；超声波250 W微波协同处理60 s，姜辣素的提取率达到1.843%，处理后物料经70℃热回流提取2 h，姜辣素的提取率可达到3.262%，是直接热回流提取2 h的1.5倍。

The method comprises following steps: reacting hydroxylation carbon nano-tube successively with reagent containing halogen and hydrosulphide to prepare sulfhydryl carbon nano-tube; reflowing the sulfhydryl carbon nano-tube and platinum salts in polyatomic alcohol, processing in hydrogen atmpsphere to obtain sulfhydryl anchoring platinum / carbon nano-tube catalyst; reflowing the sulfhydryl carbon nano-tube successively with the hydrochloroauric acid and the platinum salts in polyatomic alcohol, processing in hydrogen atmpsphere to obtain sulfhydryl anchoring platinum-gold / carbon nano-tube catalyst.

本发明将市售羟基化碳纳米管先后与含卤试剂和氢硫化物反应得到巯基化碳纳米管。再将巯基化碳纳米管与铂盐在多元醇中回流，氢气氛中处理得到巯基锚固铂/碳纳米管催化剂。将巯基化碳纳米管依次与氯金酸和铂盐在多元醇中回流，氢气氛中处理得到巯基锚固铂-金/碳纳米管催化剂。

The change of the length of circulation area is gentle because of the change of the angle of the blunt-body, from 30°-70°, the lenth is increased by the increment of the angle.

2回流区长度随钝体角度变化较为平缓，在30°～70°范围内，回流区的长度随角度的增大而增大。

The method is characterized in that:(1) the reflux of the 2-[N, N- 2amino]-3-cyano-group-4-thiopheneacetic-5-carboxylic acid tetra ester is carried out in the proper sodium hydroxide aqueous solution of alcohol for 5h to 6h and the pH value is kept over 10 during hydrolysis;(2) the ethanol of 20 per cent to 60 per cent is added and then the strontium chloride aqueous solution with 2times to 2.5times molal weight is directly added, precipitates the crystal, is filtered and dried;(3) water is added to carry out the reflux and the little salt packed in the crude product is removed, and the product is collected through heat filtration.

其特征在于：①将2--3-氰基-4-羧甲基噻吩-5-羧酸四酯在适量氢氧化钠水醇溶液中回流5～6小时，水解过程保持pH值10以上；②然后再加入20-60％乙醇，随后直接加入2-2.5倍摩尔量氯化锶水溶液，析出结晶，过滤，晾干；③加水回流，除去粗品中包裹少量盐，热过滤，收集产品。

Uterine obstruction of venous return can produce prearrest hypotension or shock and in the critically ill patient may precipitate arrest.1,2In cardiac arrest the compromise in venous return and cardiac output by the gravid uterus limits the effectiveness of chest compressions.

在怀孕20周以后，妊娠子宫挤压下腔静脉和主动脉，使静脉回流和心输出量受阻。子宫静脉回流受阻会导致停跳前高血压或休克，对病情危重的患者促进心跳停止[1，2]，同时，妊娠子宫还限制肺的舒张。

The invention relates to a dynamic matrix control system of high-purity distillation, which comprises distillation tower, intelligent checker, DCS system, superior host, and on-site bus, while they are connected. The control system uses tower product group as the object variable, and the reflux ratio and reboil ratio as control variable; the superior receives history temperature and pressure data from the DCS real-time database, via the predict control and dynamic matrix controller, to obtain the output values of present controller as reflux ratio and reboil ratio, then feedback said two values to DCS system, to function the distillation object. The invention can confirm the high-purity stable operation, with better dynamical control.

本发明公开了一种高纯精馏的动态矩阵控制系统和方法；系统包括：精馏塔、智能检测仪表、DCS系统、上位机和现场总线；所述精馏塔、智能检测仪表、DCS系统和上位机通过现场总线依次相连，实现信息流的上传和下达；本发明所涉及的控制系统采用塔双端产品组分为被控变量，回流比和再沸比为对应的控制变量；上位机从DCS实时数据库中获得历史的温度、压力等数据，通过推断控制环节和动态矩阵控制器环节，得到当前控制器的输出值-回流比和再沸比，再把控制器输出值返回给DCS系统，实现了对高纯精馏过程的双端产品高纯控制，对双端组分的高纯度平稳操作，具有很好的动态品质和控制效果。

The best reaction conditions of the second step was confirmed by the orthogonal experiment. Its yield was 90.5% when the reagents were refluxed for 3.0 h at 120℃.

第一步反应很快，回流30 min即可；通过正交试验得出第二步反应的最佳条件为：反应体系在120℃回流3.0h，产物的产率为90.5%。

Plunder melds and run with this jewel!

掠夺melds和运行与此宝石！

My dream is to be a crazy growing tree and extend at the edge between the city and the forest.

此刻，也许正是在通往天国的路上，我体验着这白色的晕旋。