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The effect of acetic acid and its consumption, chloranil and its consumption on the preparation of TAMD by means of dioxygen liquid-phase oxidation of TMAL was probed into, and the results showed that both of them had great influence on the yield of TAMD.

探讨了冰乙酸及其用量、四氯苯醌及其用量对氧气液相催化氧化孔雀绿隐色体制取孔雀绿醇色体的影响,发现二者对醇色体的收率和纯度均有很大影响。

A new method using gel permeation chromatographic cleanup followed by high performance liquid chromatography-tandem mass spectrometry has been established for quantitative determination of Maleic hydrazide,Prowl and butralin residues in tobacco.

建立了用凝胶渗透色谱净化-液相色谱-串联质谱分析烟草中3种抑芽剂残留的方法。卷烟中的待测抑芽剂组分用V∶V=1∶1超声提取后通过凝胶渗透色谱净化;凝胶色谱柱为Biobeads S-X3玻璃柱(50 g,400 mm×25 mm),流动相为V∶V=1∶1溶液,流速5 mL/min;收集第10~25 min流出的液体用液相色谱色谱-三重四极杆串联质谱仪测定。

The sporophore of Cordyceps militaris and the cordycepin content of intermediate products were monitored in the whole course according to the relation between fixed and mobile phases of solvents in a combination system of binary and quaternary solvents, in which the applied methods were successively supercritical fluid extraction, alcohol sedimentation, low-pressure normal-phase silica-gel chromatography, reversed-phase high-performance liquid chromatography and fractional crystallization.

根据溶剂的固定相与流动相之间的相对关系,采用了二元和四元组合的溶剂系统,顺次采用超临界流体萃取法、醇沉法、低压正相硅胶色谱法、反相高效制备液相色谱法、分步结晶法和反相高效液相色谱法,子实体及其中间产物中的虫草素含量变化情况。

To study the bioactive components from water soluble extract of the Chinese eaglewood, various column chromatography of Chinese eaglewood led to the isolation of ten compounds. Their structures were elucidated as 2,3-bis(3-hydroxyphenyl)- propan-1-ol (1), [(2R,3R)-3-(4-amino-3,5-dimethoxyphenyl)oxiran-2-yl]methanol (2), 8-chloro-4'- methoxy-5,6,7,3'-tetrahydroxy-2-(2-phenethyl)-5,6,7,8-tetrahydrochromone (3), 4'-methoxy-5,6,7,3'-tetrahydroxy-2--5,6,7,8-tetrahydrochromone (4), the isomer of 4 (5), 4'-methoxy-5,6,7,8-tetrahydroxy-2-(3'-hydroxyphenethyl)-5,6,7,8- tetrahydrochromenone (6), 4'-methoxyisoagarotetrol (7), 6-hydroxy-2-(2-hydroxy-2- phenethyl)-chromone (8), 6-hydroxy-2-(2-phenethyl)-chromone (9), 6-hydroxy-2-(4'- hydroxy-2-phenethyl)-chromone (10), and Guaiacylacetone (11) by means of spectral analysis and comparison with references.

为了进一步发现沉香中具有生理活性的化学成分,本文对国产沉香的水溶性成分进行了研究,从中分离得到11个化合物,通过红外、紫外、质谱、核磁共振(1H-NMR, 13C-NMR, COSY, HSQC, HMBC, ROESY)波谱解析,分别鉴定为:2,3-二(3-羟基苯基)-丙-1-醇(1),[(2R,3R)-3-(4-氨基-3,5-二甲氧苯基)-2-氧化烯基]甲醇(2),8-氯-4'-甲氧基-5,6,7,3'-四羟基-2-(2-苯乙基)-5,6,7,8-四氢色原酮(3),4'-甲氧基-5,6,7,3'-四羟基-2-(2-苯乙基)-5,6,7,8-四氢色原酮(4),化合物3的差向异构体(5),4'-甲氧基-5,6,7,8-四羟基-2-(3'-羟基-2-苯乙基)-5,6,7,8-四氢色原酮(6),4'-甲氧基异沉香四醇(7),6-羟基-2-(2-羟基-2-苯乙基)色原酮(8),6-羟基-2-(2-苯乙基)色原酮(9),6-羟基-2-(4'-羟基-2-苯乙基)色原酮(10)和Guaiacylacetone (11)。

Through the SPCE061A programming, this design requests us use the single chip microcomputer, PLC or other components to control the LED digital tube and the double color LED lamp on the traffic light control panel, enable the system to have the following functions: The four intersections of the crossroad all have double color LED (gives out red light and green light, superimposes for yellow light) to demonstrate the condition of every channel on the intersections; Each intersection has two digital tubes to demonstrate current traffic light countdown; use the button or other way to simulate the counting of the traffic flow volume.

设计要求通过SPCE061A的编程,使用单片机、PLC或其他器件来控制交通灯控制板上的LED数码管以及双色LED灯,使系统具有以下功能:十字路口的四个路口都有双色 LED (发红、绿光,叠加为黄色光)显示各路口的各条通道状态;每个路口有两位数码管显示当前红绿灯的倒计时;可利用按键或其它的方式模拟对车流量的计数;有四种工作状态:正常工作状态、紧急工作状态、设置状态和查询状态;红绿灯变换时有语音提示;查询时,可语音播报当前路况。

The efficacy of photocatalytic oxidation was relative to the number of dip-coated plate, which 2 and above plates was superior to one plate, and also vertical plane to the light source was more efficient than parallel plane. The reaction rate constant showed the color removal decreased as initial MB concentration was raised. As for efficiency of catalyst durability, it was found that TiO2 dip-coated stainless steel plate performed 95% color removal at 5ppm MB even after 4 times repeated usage, which showed favorable durability. However, when the concentration up to 10 ppm, the color removal decreased as the used counts was raised.

脱色率和钢网片数有关,钢网片数超过2片以上时,其光催化效能优於单片者;光催化效能与钢网摆放方式或光源入射的角度有关,与光源垂直摆放的脱色率优於与光源平行摆放者;由反应速率常数得知,反应物之脱色率随著反应物初始浓度的提升而递减:在耐用性方面,亚甲基蓝5ppm在重覆使用四次后,其六个小时脱色率皆维持95%,显示自制光触媒钢网之耐用性颇佳,若将反应物浓度提升至100ppm,其脱色率随著使用次数之增加而递减。

In this paper, the distribution of four subclasses of four subclasses of Seyfert Galaxy ( Seyfert 1s,Seyfert 1.5s, Seyfert 2s and Seyfert 3s or lin -ers)in the two -color diagram are comoared, It is found that the four subclasses have significantly different distribution in two -color diagram and have significantly different average color index, and especially Seyfert 1s are bluer than Seyfert 2s.

文章比较了四种赛弗特星系子类(1型赛弗特星系,1.5型赛弗特星系,2型赛弗特星系和3型赛弗特星系或低电离核星系)大双色图中的分布情况。结果发现四种赛弗特星系子类在双色图中具有显著不同的分布,特别地1型赛弗特星系比2型赛弗特星系要蓝。

Among four yeast strains with the capability of decoloring indigo carmine isolated from sludge samples taken from the textile wastewater treatment facility by enrichment cultivate,a strain Y-1 was selected on the basis of excellent dye decolorization.

通过富集培养,从印染污水处理厂污泥中分离出四株靛蓝胭脂红脱色酵母,挑选其中脱色效果较好的酵母Y-1菌株进行摇瓶脱色研究。

This research utilized the method of organic synthesis, researching different amounts and positions of hydroxy-substituted benzoic acid and serotonin into amide reaction, so as to produce a series of polyhydroxy substituted N-benzoylserotonin derivatives (compound 1-10). Accordingly, this study conducts the following four tests. I. The activity of antioxidant and the experiment of ability to scavenge DPPH free radical, II. The ability of overall antioxidant—the activity of TEAC, III. The activity test of inhibit Tyrosinase, and IV. The study of absorbing UV / VIS Spectrophotometers. This study use trolox, arbutin, and octyl salicylate as the control groups, and to test the ability of anti-oxidation, the activity of inhibit Tyrosinase, and the ability of absorbing UV. This research ultimately intends to investigate the applied value of those compounds into cosmetics.

本研究主要利用有机合成的方法,将不同数量及不同位置的羟基取代苯甲酸化合物与色洛冬宁进行醯胺化反应后,得到一系列的多羟基取代之N-色洛冬宁苯甲醯胺衍生物(化合物1 ~ 10),进行四种不同活性测试方法:一、清除DPPH自由基能力抗氧化活性测试;二、总抗氧化能力活性测试;三、抑制酪胺酸酶活性美白测试;四、紫外线/可见光光谱仪吸收测试,并以水溶性维生素E、熊果素、水杨酸辛酯当作对照组,探讨其抗氧化能力、抑制酪胺酸酶的活性能力与吸收紫外线能力,再进一步探讨其应用於化妆品上的价值。

A method for simultaneous determination of oxytetracycline, tetracycline, chlortetracycline and choramphenicol in seafood was successfully developed using high performance liquid chromatography with ammonium acetate/water and acetonitrile as the mobile phase. The results showed that the four antibiotics were well separated under the optimum conditions, with the limits of detection being 32 μg/kg for oxytetracycline, 15 μg/kg for tetracycline, 23 μg/kg for chlortetracycline, and 19 μg/kg for choramphenicol. The recovery of standard additions was 76~92% and the relative standard deviation was 0.8-4.5%. The method is rapid, sensitive, accurate and reliable and can be applied in the analysis of antibiotic residues in seafood.

建立了同时检测海产品中土霉素、四环素、金霉素、氯霉素残留的高效液相色谱分析方法,以醋酸铵-醋酸/水缓冲液和乙腈作为流动相,通过二元梯度洗脱,使四种抗生素获得了较好的分离,以基线噪音的3倍计算,土霉素、四环素、金霉素、氯霉素最低检出浓度分别为32μg/kg、15μg/kg、23μg/kg、19μg/kg,在添加浓度范围内,四种抗生素的加标回收率为76~92%,相对标准偏差为0.8~4.5%,该方法快速、灵敏、准确,可靠性高,可用于海产品中抗生素残留的色谱分析。

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推荐网络例句

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了,排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意,我建议我们在价格上大家各让一半。

After an hour and no pup, look for continued contractions and arching of the back with no pup as a sign of trouble.

一个小时后,并没有任何的PUP ,寻找继续收缩和拱的背面没有任何的PUP作为一个注册的麻烦。