四氧化物

ABSTRACT In the present paper experimental studies on thermodynamic behaviour of titanium and silicon oxides in a number of quaternary and pentanary molten slags have been made by means of H〓O/H〓 chemical equilibrium between copper melts and molten slags in alundum crucibles with the molybdenum plate as the liners.

本文采用H〓O/H〓定组成混合气体与钼衬坩埚中熔渣之间的化学平衡方法，实验研究了多个四元和五元熔渣中钛和硅氧化物的热力学行为。

The results revealed that ethane and oxygen can react on catalysts with good reactivity and selectivity.

评价结果表明，临氧条件下，在四种铁基复合氧化物催化剂上的反应性能差别较大，这种反应性能上的不同是与催化剂本身结构和晶格氧的活泼性密切相关的。

They have close relationship as the former may provide new ideas and approaches for the later, while the later may be the simulation for the former and gives it helps in degradation products identification and mechanism explanation. It is necessary to choose a suitable system, which has high potential of treating EDs and close relationship to the natural environment, to combine the researches in the two aspects. Our group has been engaged in researches on the photochemical properties and application to water pollution control of different ferric species including Fe -OH complexes, Fe -polycarboxylate complexes, Ferric oxides and Fe -humic acid complexes. Fe -oxalate complexes system has higher efficiency than the other ferric species systems in photooxidation and degradation of organic compounds. This thesis is focused on the photodegradation of nine EDs estradiol (E2), estrone (E1), 17α-ethynyl estradiol (EE2), diethylstilbestrol , bisphenol-A , 4-Nonylphenol , 4-Octylphenol , di-n-butyl phthalate , and di (2-ethylhexyl) phthalate .

因此从处理效率和环境化学意义两方面考虑，结合本课题组在不同铁形态（包括Fe-OH配合物、Fe-多羧酸配合物、Fe氧化物、Fe-腐殖酸配合物等）的光化学特性及其在水污染控制中的应用方面较系统的研究工作基础，本论文选择了四类共9种典型的内分泌干扰物（雌二醇（E2）、雌酮（E1）、17α-乙炔基雌二醇（EE2）己雌酚、双酚A、壬基酚、辛基酚、酞酸二丁酯和酞酸二乙基己基酯），研究了它们在Fe-草酸盐配合物体系中的光降解效果，推测其降解机理，探索环境内分泌干扰物光氧化处理的新体系，同时为预测其在环境中的光降解行为提供了依据。

To enable the fabrication of thermally stable ultralow dielectric constant film, specific precursor materials are used, such as, cyclic siloxanes and organic molecules containing ring structures, for instance, tetramethylcycloterasiloxane and cyclopentene oxide.

为了能够制造热稳定超低介电常数材料，使用特定的前驱物材料，例如环硅氧烷和例如四甲基环四硅氧烷和环戊烯氧化物这样包含环状结构的有机分子。

It can be divided into four methods to prepare manganic manganous oxide from the raw stuff: electrolytic product of manganese、manganous salt、manganese oxide compound and manganese carbonate.

四氧化三锰的生产方法主要有四种：金属锰悬浮液法、锰盐法、高价锰氧化物法以及碳酸锰法。

Starting from tetrafuran, 2_(4_Aminosulfonylphenyl)_4H_1,2_thiazine_1_dioxide, an antiepileptic drug with special structure, was obtained via esterification, sulphonation, chloridization, condensation and cyclization.

以四氢呋喃为原料，经酯化、磺化、酰氯化、缩合、环化等步骤，合成了化学名为 4_(四氢_2H_1，2_噻嗪基_2 )苯磺酰胺_S_S_二氧化物的抗癫痫药舒噻嗪，通过IR、1HNMR和元素分析对其结构进行了表

Synthesis of the antiepileptic tiagabine hydrochloride;2. Starting from tetrafuran, 2_(4_Aminosulfonylphenyl)_4H_1,2_thiazine_1_dioxide, an antiepileptic drug with special structure, was obtained via esterification, sulphonation, chloridization, condensation and cyclization.

以四氢呋喃为原料，经酯化、磺化、酰氯化、缩合、环化等步骤，合成了化学名为 4_(四氢_2H_1，2_噻嗪基_2 )苯磺酰胺_S_S_二氧化物的抗癫痫药舒噻嗪，通过IR、1HNMR和元素分析对其结构进行了表

The second part was to test the appearance, ingredient analysis, surface potential, thermal conduction properties, and magnetism of the nano composite fluid prepared from the parameters. The experiment found that unoxidized particles, Ag, Cu, Fe, and Ni appeared round. If combined with oxygen in water as oxides, the nano particles would grow toward certain directions. In copper/iron nano composite fluid, FeO appeared cubic, Cu2O appeared coniferous. In silver/iron nano composite fluid, FeO was polygonal. In dielectric potential detection, the nano composite fluid was likely to aggregate and deposit, except for silver/iron set. In other sets, the pH of silver/cobalt nano composite fluid was 7, surface potential was 21.21mV; the pH for silver/nickel nano composite fluid was 6.5, surface potential was 21.04mV; the pH for copper/iron nano composite fluid was 7, surface potential was -30mV. The fluid particles of the three sets could all maintain suspension of 2 weeks or more. For thermal conduction, the silver/nickel, nano composite fluid showed the best thermal conduction. Under temperature of 30℃ fluid weight conduction of 0.4%, the thermal conduction increase was 26%. For magnetic detection, except for silver/iron nano composite fluid, the nano particles of other three sets were paramagnetic, and all four sets were soft magnetic nano composite materials.

第二部分。将由较佳制备参数所产出的奈米复合流体，进行形貌外观、成分分析、表面电位及热传导性质实验与磁性检测；在奈米颗粒的形貌部分，经实验发现Ag、Cu、Fe、Ni等未氧化的颗粒皆呈现近似圆形，而若与水中的氧结合形成氧化物，奈米颗粒则会朝特定方向成长，在铜/铁奈米复合流体中FeO为四方体结构、Cu2O的颗粒是针叶状，在银/铁奈米复合流体中FeO则为多边形结构；而介面电位检测方面，结果显示经本制程所产出的奈米复合流体除银/铁奈米复合流体这一组较容易聚集沉淀外，其他三组中银/钴奈米复合流体的pH值为7，表面电位为21.21mV，银/镍奈米复合流体的pH值6.5表面电位为21.04mV而铜/铁奈米复合流体的pH值为7时表面电位约在-30mV，且此三组流体颗粒皆能维持悬浮性2周以上，悬浮性较佳；热传导实验部分，四组奈米复合流体中以银/镍奈米复合流体在增进热传上效果最佳，在温度30℃及流体重量浓度0.4﹪条件下热传导系数增进达26﹪；磁检测方面，除了银/铁奈米复合流体外，其他三组奈米颗粒皆属顺磁性，且这四组奈米复合材料都是属软磁性。

The chlorin e6 7 and chiorin 11 were oxidized further with osmium oxide in the same oxidization condition to yield bateriochlorin 8 and 12, respectively.

卟吩醛2在碱性条件下转化为卟吩e6三甲酯7，2与烷基溴化镁的格氏反应给出脱镁叶绿酸醇9，选择高钌酸四丙基铵和N-甲基吗啉N-氧化物将3-位羟基氧化成羰基，所生成的卟吩二酮10在酸性条件下脱去甲酸甲酯生成焦脱镁叶绿酸衍生物11，用四氧化锇对7和11实施氧化，则分别转化为细菌卟吩衍生物8和12。

Experimental Center of National Level One, Hubei Traditional Chinese Medica l College, Wuhan 430061）Abstract To investigate the protective effects of Jiaweisinisa n on acute liver injury induced by intraperitoneal injection of D-ga lac-tosamise, serum superoxide dismutase, malondialdehyde , glutathioe contents were measured. The pathological changes of liver wer e observed simultaneously. The results showed that JWSNS could decrease serum MD A content, but increase serum SOD and GSH activities in acute liver injury induc ed by D-GalN. It was also found that JWSNS could alleviate the degeneration and necrosis of the hypatocytes.

为研讨加味四逆散防治肝损伤的作用机理，通过动物试验，先用加味四逆散预防给药，再采用D-氨基半乳糖造成大鼠急性肝损伤模型，然后检测大鼠血清超氧化物岐化酶、丙二醛、还原型谷胱甘肽水平，同步观察该方对急性肝损伤大鼠体内脂质过氧化反应及肝脏病理改变的影响，结果表明该方可明显升高大鼠血清SOD、GSH水平，降低MDA水平，肝脏病理学检查亦表明该方使肝细胞变性坏死程度减轻。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。