四体

Due to the key challenge for complicated techniques and preparation, there were few reports about ternary systems. A series of polyimide/SiO_2-TiO_2 hybrid films with different contents of inorganic particle were fabricated using tetraethoxyl silicane and tetrabutyl titanate as precursor in situ with sol-gel method and both phases in situ. Chemical structure and micro-morphology of hybrid films were studied by means of IR, SEM and XRD.

本文以正硅酸乙酯和钛酸四丁酯为前驱体，采用原位溶胶-凝胶法和两相原位同步法制备了一系列不同含量的聚酰亚胺/SiO_2-TiO_2杂化薄膜，利用红外光谱、扫描电镜和XRD观察了薄膜的化学结构和微观结构，并测试了薄膜的热稳定性、电击穿场强和耐电晕性。

A series of polyimide/SiO2-TiO2 hybrid films with different contents and weight ratio of inorganic particle were fabricated using tetraethoxyl silicane and tetrabutyl titanate as precursor by situ method. Chemical structure, micro-morphology and thermal stability of hybrid films was studied by means of SEM, IR and XRD, TGA was also tested.

以正硅酸乙酯和钛酸四丁酯为前驱体，采用两相原位同步法制备一系列不同含量及重量比的聚酰亚胺／SiO2-TiO2杂化薄膜，利用红外光谱、扫描电镜和XRD观察了薄膜的化学结构和微观结构，并测试了薄膜的热稳定性。

A series of polyimide/SiO2-TiO2 hybrid films with different contents and weight ratio of inorganic particle were fabricated using tetraethoxyl silicane and tetrabutyl titanate as precursor by situ method .

以正硅酸乙酯和钛酸四丁酯为前驱体，采用两相原位同步法制备一系列不同含量及重量比的聚酰亚胺/SiO2-TiO2杂化薄膜，利用红外光谱、扫描电镜和XRD观察了薄膜的化学结构和微观结构，并测试了薄膜的热稳定性。

The typical broken fan texture and sanded texture of smectic phase can be observed.

四。所有配体加热至各自的熔点以上都能形成液晶态，在液晶态可观察到近晶相的破碎扇形织构和沙地织构。

The typical mosaic texture, sanded texture of smectic phase and schlieren texture, ball granul textre of nematic phase can be observed.

四。所有配体加热至各自的熔点以上都能形成液晶态，在液晶态可观察到近晶相的破碎扇形织构和沙地织构。

About a year after pollination, the generative cell of the four-celled male gametophyte undergoes division, giving rise to two kinds of cells—a sterile cell and a spermatogenous cell.

在授粉后大约一年，四个中生殖细胞-细胞男性的配偶体接受区分，引起细胞的二个类型-一个不毛的细胞和一个 spermatogenous 细胞。

Sixteen ( 15 new) amphibian and twenty-two ( 11 new) squamate species have been reported across China, including the oldest Chinese tetrapod Sinostega pani from the Late Devonian of Ningxia Hui Autonomous Region, the large stereospondyl amphibian Yuanansuchus laticeps from the Middle Triassic of Hubei Province, Late Jurassic/Early Cretaceous lissamphibians ( e. G., the anurans Callobatrachus sanyanensis and Mesophryne beipiaoensis, the caudates Jeholotriton paradoxus and Laccotriton subsolanus) from Northeast China, Paleogene lizards (e. G., Brevidensilacerta xichuanensis and Tinosaurus yuanquensis) from North China, and numerous lizards from the Late Cretaceous of Nei Mongol Autonomous Region.

共报道了16种两栖类和22种有鳞类，其中15种两栖类和11种有鳞类为新种，包括我国最古老的四足动物宁夏晚泥盆世的潘氏中国螈，湖北中三叠世的大型全椎两栖类宽头远安鲵，东北晚侏罗世/早白垩世的多种滑体两栖类(如无尾类三燕丽蟾和北票中蟾，有尾类奇异热河螈和东方塘螈)，华北古近纪的蜥蜴类(如淅川短齿蜥和垣曲响蜥)，以及内蒙古晚白垩世的多种蜥蜴类等。

Work 工作:(1) feasible process development for high-pure tetraalkyphosphonium salt as catalysts for polymerizations, potential sale 2-4 million us$;(2) simple and feasible preparation process for phosphonium salt as ionic liquids, biocides and phase transfer catalysts;(3) new and industrially feasible processes for highly sterically hindered alkylphosphines as catalyst ligands, these include tricyclohexyl-phosphine, phosphorinanes and dsmphos2,3- bis(9-phosphabicyclononylbutane;(4) sterically hindered dialkylphosphinic acid as new generation of co/ni extractant;(5) alkylphosphonium wittig reagents and the wittig reactions with them;(6) exploration of the application of borane chemistry in the synthesis of highly sterocally hindered organophosphines;(7) customer preparation of samples of a variety of organophosphorus compounds for customers all over the world.

用作高分子聚合反应催化剂的高纯度四烷基瞵盐的实用生产流程。产品销售前景 2-4 百万美元；(2)用作离子化液体，杀菌剂和相转移催化剂的烷基瞵盐的简单实用合成方法；(3)高位阻烷基磷化氢催化剂配体的工业实用合成路线的研究，这包括，三环己烷基磷， phosphorinanes 和 dsmphos 2，3-bis(9-phosphabicyclononylbutane ；(4)高位阻二烷基膦酸金属萃取剂的工业实用合成路线的研究；(5)烷基膦 wittig 反应试剂的研究；(6)硼化学在高位阻烷基磷化氢合成中的应用；(7)为世界各地提供顾客合成服务。

Veined,stockwork and alteration-sheathed gold ores have been found in the area,belonging to four genetic types:the volcanic hydrothermal ores related to early—middle Carboniferous volcanism; subvolcanic hydrothermal ores related to intermediate—acidic porphyry intrusions; hydrothermal ores to the granitic intrusion and dynamo- hydrothermal ores related to regional dynamic metamorphism along the faults.

矿石类型有含金石英大脉型、石英网脉型和蚀变岩型。矿床成因类型有4种：一为火山热液型，其成因与区内早—中石炭世火山作用有关；二为潜火山热液型，与中酸性斑岩体侵位有关；三为岩浆热液型，与花岗质岩浆的侵位有关；四为动力变质热液型，沿断裂带分布于蚀变玄武岩中，系区域动力变质作用的产物。

Veined,stockwork and alteration-sheathed gold ores have been found in the area, belonging to four genetic types: the volcanic hydrothermal ores related to early-middle Carboniferous volcanism; subvolcanic hydrothermal ores related to intermediate-acidic porphyry intrusions; hydrothermal ores to the granitic intrusion and dynamo- hydrothermal ores related to regional dynamic metamorphism along the faults .

矿床成因类型有4种：一为火山热液型，其成因与区内早-中石炭世火山作用有关；二为潜火山热液型，与中酸性斑岩体侵位有关；三为岩浆热液型，与花岗质岩浆的侵位有关；四为动力变质热液型，沿断裂带分布于蚀变玄武岩中，系区域动力变质作用的产物。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。