四

A ratio spectra derivative spectrophotometry for simultaneous determination of quaternary mixture of aminopyrine, phenobarbital, caffeine and phenacetin was studied.

提出了可应用于四元混合体系同时测定的比光谱-导数分光光度法，阐述了该方法的基本原理，并将其应用于氨基比林、苯巴比妥、咖啡因和非那西丁四元混合体系中各组分的同时测定。

The anionic polymerization of octamethylcyclotetrasiloxane (D4) catalyzed by tetramethyl ammonium hydroxide in the presence of water under conditions of high temperature and oxygen-off was investigated.

以八甲基环四硅氧烷为单体，四甲基氢氧化铵为催化剂，微量水为链封端剂，进行有水条件下环硅氧烷阴离子开环聚合。

A novel synthetic approach of 3,3'-azobis(6-amino-1,2,4,5-tetrazine) was firstly devised. Taking 3,6-bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine as a primary material, DAAT was synthesized by high pressure ammonolysis and potassium permanganate oxidation. Compared with the four-step reaction in the literature, this new approach was reduced to two steps with a yield of 58.1%. The intermediate and DAAT were characterized by elemental analysis, IR and NMR spectra.

自行设计了3，3'-偶氮双(6-氨基-1，2，4，5-四嗪)新合成路线、采用3，5-双(3，5-二甲基吡唑-1-基)-1，2，4，5-四嗪为原料，由文献报道的4步反应缩减为2步，经高压氨解、高锰酸钾氧化合成了DAAT，总收率大幅提高，达到58.1%，并采用元素分析、红外光谱、核磁共振光谱等进行了结构表征。

The researchers tested four healthy individuals and four amnesic patients.

研究者测试了四个健康的人和四个失忆症患者。

After getting these four line-of-sight vectors, we inverse these data in special observation coordinate based on space analytical geometry, then we can get the vector that has three components on every coordinate, this vector will be treated as the total wind profile in the three-dimensional observation field, the result of this four-point method can basically reflect all the spatial and temporal variation of the atmospheric wind.

在得到视线方向风速矢量后，从选定的三维观测坐标系对这四个矢量进行空间解析几何的运算，可得到观测坐标系的各坐标轴上四个测量矢量的各坐标分量的标量和。从而以这个在三个坐标轴上都有分量的矢量作为在观测视场内的总的风场的风速矢量。

Four different pathways of androgenesis have been observed:Pathway of vege...

在雄核发育的研究中，观察到有营养细胞发育途径，生殖细胞发育途径，营养细胞和生殖细胞混合发育途径，以及均等分裂发育途径等四种类型，并对这四种途径进行了讨论。

The main work and the originality points of this dissertation could be concluded as the following parts:(1) To analyze systematically the mathematical model of LES of air flow in great space, under the case of isothermal and non-isothermal, as well as the combined action of buoyancy and strain. Some basic problems are studied about the LES application into airflow simulation of great space, such as boundary conditions, spatial difference scheme and time advancing scheme, time step etc., which creates the basis for the LES application to indoor airflow simulation.(2) Both the instantaneous and time averaged flow field of great space with multiple jets under isothermal and non-isothermal cases are explored with large eddy simulation method, and also discussed the dynamic characteristics and the law of fluidflow in the great space.(3) Based on the results of LES of the great space and the Fanger thermal comfort indexes, it is brought forward the concept of the series of dynamic thermal comfort evaluating indexes, which could be divided into thermal comfort index with time averaged properties PD, PPD, PMV, thermal comfort index with instantaneous properties IPD, IPPD, IPMV, and time averaged thermal comfort indexes TAPD, TAPPD, TAPMV, and transient situations time averaged thermal comfort indexes TTAPD, TTAPPD, TTAPMV. The differences among them and the calculation methods are discussed, and the four kinds of indexes are calculated with the thermal comfort index PD as an example.(4) Based on the LES results it is discussed the hot air stratification phenomena in air-conditioned buildings in the case with air supply and return registers on the ceiling and the case on the sidewall. The fundamentals of the hot air stratification are studied and the relations of estimating hot air stratification are brought forward.(5) With the advanced apparatus such as hot wire film anemometer IFA300 and laser particle field anemoscope, corresponding model test and site measurements have been done, which are compared with the simulation results and LES is proved a very promising method in air flow simulation indoor.

本文主要工作既创新点体现在以下几个方面：(1)系统分析了等温、非等温和考虑剪切力与浮升力综合作用的高大空间大涡模拟数学模型，并研究了高大空间大涡模拟在室内气流仿真应用中的一些基本问题，如边界条件、空间离散格式和时间推进格式、时间步长选择等问题，为大涡模拟在室内气流计算中的广泛应用打下了基础；(2)首次用大涡模拟方法研究了高雷诺数下高大空间多射流在等温、非等温情况下的瞬时流场和时均流场分布，并探讨了多射流流场的动态特性和流动规律；(3)基于大涡模拟的动态仿真结果和Fanger的热舒适指标，首次系统地提出了动态热舒适评价指标体系的概念：即基于时间平均参数的热舒适指标PD、PPD、PMV；基于瞬时参数的瞬时热指标IPD、IPPD、IPMV；基于时间平均热舒适指标TAPD、TAPPD、TAPMV；以及沿行动迹线的时间平均热舒适指标TTAPD、TTAPPD、TTAPMV，并分析了四类热舒适指标的差异性和计算方法，还以PD值为例对四类指标分别进行了计算；(4)基于数十种工况下空调房间大涡模拟的结果，研究了空调建筑上送上回和侧送侧回两种情况下热分层现象，并探讨了热分层的基本规律，首次提出了避免热分层现象的判断公式；(5)在暖通空调领域，首次使用IFA300热线风速仪、激光粒子速度场仪等先进设备，完成了与大涡模拟相对应的模型试验，并把实测结果与仿真结果进行了对比，说明LES在室内气流仿真方面是一种很有前景的方法。

Proposed a new method of determining the cell thickness and the twist angle of twisted nematic liquid crystal cells, a quarter-wave plate was inserted between the liquid crystal cell and the analyzer, a stepper motor rotated the Retarder by , and measured the light intensity of every modulated point, solved the stokes parameters of polarization light exiting from the liquid crystal cell using Fourier analysis method, thereby determining the cell thickness and the twist angle.

本文提出了一种测量扭曲向列相液晶盒盒厚与扭曲角的新方法，在液晶盒和检偏器之间放置四分之一波片，通过旋转此四分之一波片，测量各个调制点的光强，用傅里叶分析法计算线偏振光穿过液晶盒后的stokes矢量，从而求出液晶盒盒厚以及扭曲角。

This chapter is divided into three sections, section I, as a "Creative intention of practical", which runs through the Qing Dynasty,"Lao Zi" annotation in the face of "Dao De Jing", and to explore the practical in the point of view of social values; The second section as "The study of the inherit in the relationship between Confucius and Lao Zi", explain that the Qing Dynasty "Dao De Jing" annotator since the Song and Ming inherited "The merge of Confucianism and Taoism" concept, from the clarification of the relationship between the Confucianism and Taoism to of sure the value of "Dao De Jing"; the third section for the "Merger of three religions and integration of China and Western Academic" explain the harmonization is the characteristics of Chinese culture.

本章共分为四节，第一节为「经世致用的创作意图」，由此贯串清代《老子》注家在面对《老子》一书的主要面向，以入世、实用的角度发掘老子的社会价值；第二节为「孔老关系的承袭论述」，说明清代《老子》注家承袭宋明以来「孔老会通」的观念，由儒、老之间关系的厘清与定位，肯定《老子》一书的价值；第三节为「佛老思想的交融互释」，突显此时以佛解老的注作大多依附於三教思想的汇流之中；第四节为「三教融合与中西会通」，说明融通是中国文化的特色，在三教融合的思想承继之上，此时的知识份子在西方武力与文化的侵略之下，开始以西学为参照，探寻《老子》的现代化意涵。

Under the special transitional pattern, that is the separation of politics and economy, the economy as the forerunner, incremental reform, and experimental units as antecedence, resolute goal and "blurred" advancement, the transition of the social insurance system inevitably depends on the "historical" road and on the "realistic" road.

在回答这四个问题以前，本论文对国内、国际时代背景和文献背景情况做了全面、清晰的概括，它既是本文选题的依据，也是回答前面四个问题的前提和基础。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。