四

The development of synthesis technology, industrial production, market demand and consumption structure of pentaerythritol were reviewed. Some suggestions to domestic production of pentaerythritol were given.

全面阐述了季戊四醇的合成技术和发展现状，对国内外季戊四醇的生产、需求以及消费结构进行了分析，提出了我国今后季戊四醇生产的一些建议。

Condensation of cyclohexanone and pentaerythritol catalyzed by iodine supported on activated carbon was investigated.

为了研究活性炭负载单质碘催化合成季戊四醇双缩酮催化活性，以季戊四醇和环己酮为原料，合成环己酮季戊四醇双缩酮。

The following conclusions have been gotten from a large amount of experiments and determinations: Triiodide, pentaiodide, heptaiodide, nonaiodide, undecaiodide of solid tetra-n-butyl ammonium polyiodides and tetrabutyl ammonium bromide polyiodides can be synthesized by solid phase process which is a economic easy way, while its not suitable for synthesizing solid tetramethyl ammonium polyiodides; Solution polyiodides of triiodide, pentaiodide can be synthesized through the complexation process, and TX-10 is a better complexing agent; Triiodide, pentaiodide, heptaiodide resinic polyiodides were synthesized by ion-exchange of resinifying process, and that is a viable easy way.

在大量实验和分析的基础上，可得到以下结论：用固相法可以合成出碘三、碘五、碘七、碘九和碘十一形式的正四丁基多碘化铵固体高聚碘和四丁基多碘化溴化铵固体高聚碘系列化合物，是制备高聚碘的经济、方便的合成方法，但此法对合成四甲基多碘化铵固体高聚碘系列化合物并不适用；TX-10是合成溶液高聚碘较佳的络合剂，通过其络合作用可以合成出碘三和碘五形式的溶液高聚碘；采用树脂法，通过离子交换，合成出了碘三、碘五和碘七形式的树脂高聚碘，此法简单可行。

Two kinds of new intermolecular complex antioxidants 3-(3, 5-di-butyl-4-hydroxyphenyl) propionyl pentaerythritol phosphate and octstearic pentaerythritol tetra- phosphite were synthesized by one-pot and two steps transesterification.

分别采用一锅法和两步酯交换法合成了两种新型分子内复合型抗氧剂，即3-(3，5-二叔丁基-4-羟基苯基)丙酰亚磷酸季戊四醇酯和八硬脂基季戊四醇四亚磷酸酯。

The colon temperatures were measured by a thermistor and the cytosolic free calcium concentration ([Ca2+]i) in dissociated brain cells was measured by Fura 2-AM. The results demonstrated that the pyretic action of egtazic acid (0.6 μmol, icv) was markedly inhibited by DEX (5 mg/kg,iv), but DEX (60-120 μmol/L) did′t affect [Ca2+]i in dissociated hypothalamus cells. Actinomycin D, which interferes with gene transcription (3 nmol, icv), completely abolished the antipyretic action of DEX on egtazic acid-induced fever.

结果发现：脑室灌注乙二醇双(2-氨基乙醚)四乙酸(0.6 nmol)引起家兔结肠温度明显升高，静脉注射地塞米松(5 mg/kg)显著抑制家兔乙二醇双(2-氨基乙醚)四乙酸性发热，地塞米松(60-120 μmol/L)并不影响下丘脑细胞内[Ca2+]i，而事先脑室灌注抑制基因转录的放线菌素D(3 nmol)则完全取消了地塞米松对乙二醇双(2-氨基乙醚)四乙酸性发热的解热作用。

Synthesis of tetraoctyl pyromellitate from pyromellitic dianhydride and isooctyl alcohol on solid super acid catalyst SO 2-_4/TiO_2-Al_2O_3 was studied.

以SO2-4/TiO2-Al2O3固体酸为催化剂、均苯四甲酸二酐和异辛醇为原料合成均苯四甲酸四异辛酯。

By using the methods of complex representation of quaternion matrices and companion vector, we study and simplify the numerical calculation methods of quaterinon matrices, and establish new aigebraic methods in quaternionic quantum mechanics.

我们通过四元数的复表示和友向量方法，研究并解决了四元数矩阵的一系列数值计算问题，给出一套四元数量子力学中的数值计算方法。

In addition, we improve Nivens method and our new method to solve the equation more quickly.2 Complete Solution Structure: We obtain that the whole solutions of real quaternionic polynomial equation are just composed of some quaternion equivalence classes and some isolated points.

另外，从新方法及四元数带余除法理论出发，进一步改进了新方法和Niven的传统方法。 2解的完整结构：由求解的新方法得到四元数多项式方程全体解的完整结构为四元数等价类与孤立点的集合，以往的结果成为其自然推论。

One type of students are those who are short of study motion. This type of students can be divided into four situation. That is the contradiction between demands and realities, the repound after pressure, they have ever been defeated, they negate the value of study, Another type of students are those whose knowledge is not enough. Their previous knowledge can't catch up with the teaching demands of a vocational school. The third type of students are those who have no suitable study methods and good learning habits. The fourth type of students are the synthesis of all above.

其次从学生主观角度分析，其化学学习障碍产生的原因可分为四种类型：一是学习动力不足，这类学生又可大致分为四种情况，即需求的倒错、压力的反弹、心理曾经受挫和否定学习的价值；二是先备知识不足，表现在其先备知识与中专教学要求的不相称上；三是学习方法和习惯不好；四是综合体现上述三种原因。

Four laser beams used for ~ 40 K and ~ 87 Rb cooling and repump lights are obtained by using acoustic optic modulators to offset the frequencies from the three external cavity diode lasers.

三台ECDL通过声光调制器产生四束光，分别作为40K和87Rb原子的冷却光和再抽运光，四束不同频率成分的激光分别注入锁定四台从激光器，然后Rb冷却光、K冷却光和K再抽运光再同时注入半导体激光放大器进行放大。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。