咪唑

The improved method selects the absorbing wavelength of 618 nm and the reaction time of 40 min, uses the NH4Cl-NH3 buffer solution (pH=8.0) and BTB alcohol solution (0.4 g/L) respectively of 5 ml and 1.5 ml in the 50 ml volumetric flask, and can test the concentration of imidazolinyl-quaternary-ammonium-salts in range of 0 mg/L to 80 mg/L.

利用改进的显色反应法检测时，吸收波长选择618 nm，显色时间40 min， 5 ml容量瓶中NH4Cl-NH：缓冲液(pH=8.0)和BTB乙醇溶液(0.4 g/L)的添加量分别为 5 ml、15 ml，适用检测的咪唑啉季铵盐浓度为0~80 mg/L。

In this process, we have discovered a three-component tandem reaction leading to the formation of 6-vinyl-1,3a-diazapentalene derivatives.

实验结果表明，在形成可能的中间体B以后，由于烯酮取代基的作用，Michael加成被抑制，进而发生一个三组分串联反应，得到吡咯并咪唑衍生物。

Methods In the study,experimental animals were divided into three groups. Thiamazole was used to replicate the model of maternal pregnant hypothyroidism. The infant rats were innate hypothyroidism. T4 substitution group rats were administrated with T4 from postnatal 0 day as well as the same days normal neonatal rats as control. TdT-mediated dUTP nick end labeling was carried out to detect the positive cells of PCD in cortex and hippocampus of postnatal 7,14 and 21 days rats. Immunohistochemical staining technique was employed to detect Bcl-2 and Bax proteins in relevant sections. Experimental data were statistically analysed by One-Way ANOVA, SNK-q test and Spearman rank correlation analysis.

本研究实验动物分为三组，采用甲巯咪唑复制甲状腺功能减退孕鼠模型，出生后仔鼠为先天甲减鼠，T4替代组于仔鼠出生后即日起腹腔注射T4，剂量为20μg∕，同时设一正常对照组；应用原位末端标记方法检测出生后7、14、21d仔鼠大脑皮层、海马PCD阳性细胞，并应用免疫组化SP法检测相应部位Bcl-2及Bax蛋白；用单因素方差分析（One-Way ANOVA）、SNK-q检验及Spearman等级相关分析进行统计处理。

A new method of extracting and separating rutin in an aqueous two-phase system formed from water-soluble ionic liquid BF4 (1-butyl-3-methylimidazoliumtetrafluoroborate) and phase-forming salt NaH2PO4 at room temperature was studied.

建立了室温离子液体四氟硼酸1-丁基－3-甲基咪唑(BF4)和NaH2PO4组成的双水相萃取体系并用于对芦丁的萃取分离研究。

Ingredients: ginseng root extract, lavender extract, gingko, peony bark, tea tree oil, taraxacum, red-rooted salvia, forsythia, honeysuckle, Philippine violet herb extract, vitamin D, HA, squalane, PEG-20 methyl glycoside sesquistearate, mamushi oil, bi imidazolidinyl urea etc.

成 分：去离子水、人参根提取物、薰衣草提取物、银杏叶提取物、丹皮、茶树油、蒲公英提取物、丹参提取物、连翘果提取物、金银花、紫花地丁、水杨酸、羟乙基纤维素、双咪唑烷基脲、透明质酸。

Ingredients: ginseng root extract, lavender extract, gingko, peony bark, tea tree oil, taraxacum, red-rooted salvia, forsythia, honeysuckle, Philippine violet herb extract, vitamin D, HA, squalane, PEG-20 methyl glycoside sesquistearate, mamushi oil, bi imidazolidinyl urea etc.

成 分：去离子水，丙二醇，甘油，矿油、矿脂、角鲨烷，甲基葡萄糖倍半硬脂酸酯，PEG-20甲基葡萄糖倍半硬脂酸酯，褐斑蝮蛇油、人参根提取物、薰衣草提取物、银杏叶提取物、丹皮、茶树油、蒲公英提取物、丹参提取物、连翘果提取物、金银花、紫花地丁、卡波姆，尿囊素，双咪唑烷基脲，透明质酸。

We report here a novel method for condensation of unprotected saccharides with o-phenylenediamines using iodine in acetic acid solution to form aldo-benzimidazoles.

我们在这里描述了一个新的方法，用碘在醋酸的环境下，可以将未保护的醣用邻苯二胺修饰得到咪唑化合物。

The result showed simple imidazolium based ionic liquids had excellent catalytic activity, especially when under mild conditions with 0.5 equiv. EMIMBr / K_2CO_3(1 /1.1) in CH_2Cl_2, the desired benzoin was obtained in yield of 86%.

结果表明简单咪唑基离子液体对安息香缩合反应具有比较高的催化活性，当在CH_2Cl_2中，50mo1%EMIMBr/K_2CO_3(1/1.1)时，苯偶姻产率可达86%。

The one-carbon unit transfer reaction is carried out by reacting with Grignard reagent, provided new synthetic method for 5 class of 19 kinds of ketone, and the influence factors, for example, the reacting mechanism, the condition, etc.

单、双苯并咪唑盐和单、双Grignard试剂的变换组合实现的系列一碳单元转移反应，为多类型酮化合物提供了开阔的合成视野。

After the failure of achieving good enatioselectivity in asymmetric Baylis-Hillman reaction, we turned our attention to traditional chiral Lewis base catalyzed asymmetric Baylis-Hillman reaction.

我们还发现，用咪唑与-脯氨酸共催化醛和丁烯酮的Baylis-Hillman反应，但产物的e.e值还是很低，因此又回到了传统的用手性Lewis碱催化不对称Baylis-Hillman反应研究中。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。