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Based on seed-emulsion polymerization, the stable silicon-acralyte core/shell latex with little coagulum were synthesized at lower temperature with potassuim persulphate, sodium formaldehyde sulfoxylate and V-044 as composite initiators.

选用过硫酸钾、甲醛合次亚硫酸氢钠和2, 2'-偶氮二[2-(2-咪唑啉-2-代)丙烷]二氢氯化物(V-O44)为复合引发剂,在低温下通过种子乳液聚合技术合成了生成凝聚物少的硅-丙核/壳乳液。

The major part of this thesis is about the syntheses and EPR studies of a series of radical pair precursors (55, 56 and 57) which contain 1-toluene sulphonyl benzimidazoles as the key components.

本篇论文主要的部分为一系列自由基对前驱物1-对甲苯磺醯基-苯咪唑及其衍生物55、56、57的合成与低温EPR光谱之研究。

To economize cost of S03H-functionalized ionic liquids,extend their range of application in chemistry reaction,fifteen of ionic liquids have been synthesized by using methylimidazole,tri-alkylamine,pyridine with industrial materials 1,4-butane-sultone and 1,3-propane sultone as source in this paper.The ionic liquids were synthesized by tri-alkylamine have not been reported and yields are higher than 98%.

为了降低SO_3H-功能化离子液体的成本,使其应用范围更加广泛,本论文利用N-甲基咪唑、三烷基胺、吡啶和廉价工业级原料1,3-丙烷磺内酯、1,4-丁烷磺内酯为原料来源,合成十五种SO_3H-功能化离子液体,三甲胺为原料合成的SO_3H-功能化离子液体还未见文献报道,收率大于98%。

Supraspinal Anesthesia: Behavioral and Electroencephalographic Effects of Intracerebroventricularly Infused Pentobarbital, Propofol, Fentanyl, and Midazolam.

脊髓水平以上麻醉:脑室内给予戊巴比妥,异丙酚,芬太尼和咪唑安定对于行为和脑电图的影响。

The mechanism of clonidine conformational isomerization and tautomeric reaction has been studied and the geometric parameters of transition states have been located by B3LYP/6-31G**.

为了考察氯苯的共轭效应对可乐定互变异构体稳定性的影响,在B3LYP/6-31G**水平上,研究了2-氨基-2-咪唑啉的互变异构化反应机理。

Tetrahydrofolatecoenzyme,Benzimidazoline,One-carbontransfer,Mannichalkali,Tetrahydroisoquinoline,Tetrahydro-β-carboline

四氢叶酸辅酶,苯并咪唑烷,一碳转移,Mannich碱,四氢异喹啉,四氢-β-咔啉

But the electrochemical results show that complexes exhibitcompletely irreversible redox behaviour which is different from thatfound in diiron proteins. 1.3 To obtain the diiron species which are stable to elec-trochemical reduction, a series of new tetranuclear cage ironspecies containing two 〓 cores, with using hexadentatepolybenzimidazole ligands, were synthesized and characterized by vari-ous spectroscopic methods. Their physical properties have been investi-gated. The crystal structures of 〓〓tetrakis (benzimidazol-2-ylmethyl)-1, 4-diaminobutane and 〓,〓-tetrakis ( N-ethylbenzimidazol-2-ylmethyl )-1, 4-diaminobutane were determined. They contain two 〓 cores which arelinked to each other by -〓-chain in the ligands.

1.3为了获得电化学还原稳定双核氧桥联Fe化合物,使用六齿配体合成了一系列含有两个〓单元四核笼状化合物,并用各种谱学手段表征了它们,还研究了它们的物理化学性质确定了〓L=N,N,N',N'-四(苯骈咪唑基-1,4-丁二胺和〓,〓四-1,4-丁二胺化合物的晶体结构,它们含有两个〓单元,其中两个〓单元是通过配体的〓链桥联成四核笼状结构。

In addition, we have discovered a new reaction, it is that Dy/SiCl_4 can promote imines to give imidazolidines and tetrasubstituted hydrazines.

Dy/SiCl_4体系具有另外一个重要特性,就是我们发现它能够促进亚胺一步生成五取代的咪唑烷和四取代的肼,这是用其它自由基或直接用稀土金属和亚胺反应无法得到的。

Nickel sulfate was the most frequent sensitizer, followed by Thimerosal, Potassium dichromate, Fragrance mix and Formaldehyde. Frequencies of contact allergy to Thiuram mix, Mercapto mix, Imidazolidinyl urea, and bronopol were relatively low.

结果: 1 129 例受试者中,阳性反应747例,阳性反应率较高的变应原依次是:硫酸镍、硫柳汞、重铬酸钾、芳香混合物、甲醛,阳性反应率较低的变应原有:秋兰姆混合物、硫氢基混合物、咪唑烷基尿素、溴硝丙二醇。

The first step was to synthesize imidazoline. The mole ratio of oleic acid and diethylene triamine was 1:1.2, the xylene was 30%. Temperature was controlled in about 160 ℃ on this stage, timing for acylation reaction was about 1.5 hours.

第一步咪唑啉的合成:油酸和二乙烯三胺摩尔比为1:1.2,以二甲苯为携水剂,反应温度控制在160℃酰化反应1.5小时,然后升温至220℃环化反应,反应时间6.5小时。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。