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Geochemical analyses include 'total'(concentrated HNO3 -HCl digestion) and chemical forms (three step sequential digestion, reducible, oxidizable and residual forms) of heavy metals Cu, Zn, Pb, Cr,Fe and Mn, iron oxides dithionite-citrate-bicarbonate (DCB and ammonium in the dark extraction as the estimation of total and amorphous iron oxides, respectively, total sulfur and organic matter.

化学分析包括重金属(Cu、Zn、Pb、Cr和Fe、Mn)"总量"(浓HNO3、HCl提取,非严格的总量)、形态(三步提取法,可还原态、可氧化态和残渣态)、氧化铁(连二亚硫酸钠-柠檬酸钠-重碳酸钠提取和草酸铵提取分别估计总氧化铁和无定形氧化铁)、总硫和有机质,并比较了DCB提取前后样品磁性特征的变化。

Two representative compounds have been determined by X-ray crystallography. The best ratio of reactants, the adequate reaction temperature and solvent have been found by contrast experiments.4. The better photoreaction conditions and irridation times have been confirmed through the different photoreaction results. It is the first time that fifty quinazoline derivatives with biological activity and four photooxidation products with urea functional groups have been obtained by photochemistry method. Two representative compounds, quinazoline derivatives and photooxidation products, have been determined by X-ray crystallography, respectively.

通过实验对比我们找到了较佳的反应物的投料比、反应温度和反应所用的溶剂。4、根据不同条件下的光反应结果,确定了硫脲衍生物的相对较好的光反应条件和光照时间,首次利用光化学手段成功得到50个具有生物活性的喹唑啉衍生物和4个具有脲基官能团的光氧化的产物,测定了两个具有代表性的喹唑啉和光氧化的产物的晶体结构。

The advantage of stopcock used as pitch valve;2. The results showed that the failure of stopcock was corrosive wear and abrasive .

采用金相显微镜和扫描电镜对在碱性介质中发生泄漏的不锈钢旋塞阀进行了宏微观形貌和金相组织分析;并采用光电直读光谱仪、EDS、红外碳硫分析仪和NHO分析仪对旋塞阀材质和表面沉积物进行了系统的表征分析。

The book introduces the animal models representing natural infections ranging from uni- to multicellular and from endo- to ectoparasites in fish, chickens and mammals, including structural and physiological aspects of cell death; Role of apoptosis in non-mammalian host-parasite relationships; thionine-positive cells in relation to parasites; animal models for the study of innate immunity; interaction between sea lice and their hosts; pathophysiology of salmonids cryptobiosis and glossina-transmitted mammalian trypanosomiasis in livestock; avian coccidiosis; interactions betweem fish hosts and monogeneans.

该书介绍了鱼类,小鸡和哺乳动物从单细胞到多细胞和从内寄生虫到外寄生虫的天然传染的动物模型,包括细胞死亡的结构和生理学方向;非哺乳动物宿主和寄生虫关系中细胞凋亡的作用;硫堇阳性细胞与寄生虫的关系;用于先天免疫研究的动物模型;海虱与其宿主的相互作用;鲑鱼隐生想象的生理病理学和家畜中舌蝇传播的哺乳动物锥虫病;鸟类球虫病;鱼类宿主与单殖亚纲动物的相互作用。

Sulfur corrodible sites and their characteristics were introduced of the prefractionation system, air preheaters of heating furnace and product air coolers etc,and chlorine corrodible sites and their characteristics were also presented of the thermocouple casing tubes, product air coolers and fire arrestors of heating furnace etc in the catalytic reforming and diesel hydrogenated unit s.

介绍了中国石油哈尔滨石化公司催化重整及柴油加氢装置在预分馏系统、加热炉空气预热器、加氢装置反应产物空冷器等处易发生硫腐蚀和在预加氢热偶套管、加氢反应产物空冷器、加热炉阻火器等处易发生氯腐蚀的部位及其表现特征,指出装置在低温(不高于120℃)、含水、容易被堵塞的部位易形成HCl-H2S-H2O腐蚀体系,分析了腐蚀原因和介质来源,总结和提出了开好原油的电脱盐、采用脱氯技术、加强对加热炉的排烟温度控制和腐蚀介质的精制与净化、加大空冷器的注水量等针对性防腐经验和措施。

The multi-copy expression vector pZM is a shuttle plasmid which can replicate in Escherichia coli, Streptomyces and S. erythraea. It contains PermE promoter, fd terminator, multiple clone site, thiostrepton and ampicillin resistance genes, and ColE1 ori and pJV1 ori replicons which make the vector replicate in E.

游离型多拷贝表达载体pZM是可以在大肠杆菌、链霉菌和糖多孢红霉菌中扩增的穿梭型质粒,带有PermE启动子、fd终止子、多克隆位点、硫链丝菌肽和氨苄青霉素抗性基因以及在大肠杆菌和糖多孢红霉菌中复制的ColE1 ori和pJV1 ori复制子,载体大小9880bp。

Wherein X is an oxygen atom or a sulfur atom; C*, C** and C*** are asymmetric carbons; R 1 , R 2 , R 4 , R 5 , R 8 , R 9 and R 10 are each a lower alkyl group optionally having substituent and the like, or R 4 and R 5 and the like in combination optionally form a homocyclic ring optionally having substituent and the like; R 3 is an aryl group optionally having substituent and the like; R 6 and R 7 are each a hydrogen atom and the like; Nu is -CR 16 (COR 17 )(COR 18 ) wherein R 16 , R 17 and R 18 are each a lower alkyl group optionally having substituent and the like, and the like; and EWG is an electron withdrawing group.

通式中,X代表氧或硫;C *、C **和C ***分别表示不对称碳;R 1 、R 2 、R 4 、R 5 、R 8 、R 9 和R 10 分别代表任选取代的低级烷基等,条件是例如R 4 和R 5 可以相互结合形成任选取代的同素环等;R 3 代表任选取代的芳基等;R 6 和R 7 分别代表氢原子等;Nu表示-CR 16 (COR 17 )(COR 18 )(其中R 16 、R 17 和R 18 分别代表任选取代的低级烷基等)等;并且EWG表示吸电子基团。

Considering the merits of in vivo studies in biotransformation i. e. activation or inactivation, protein-binding such as sex hormone binding protein , toxicokinetics, and more evaluative in hazard identification and risk assessment, we selected a battery of short-term and long-term in vivo studies, including uterotrophic assay in weaning mice and ovariectomized adult mice, an in vivo multiple endpoints assay, and a gestational and lactational exposure assay to identify the estrogenic effects of endosulfan on the offspring.

考虑到体内试验在代谢转化、血浆蛋白如性激素结合蛋白的结合、代谢动力学等方面比体外试验优越,在危害鉴定和危险度评定中更有价值,我们选择了多项体内试验,包括对幼年小鼠和卵巢切除成年小鼠的子宫增殖作用、对成年去势小鼠的体内多终点观察以及大鼠孕期和哺乳期接触对雄性子代生殖系统结构和功能的改变,即去雄性化或雌性化作用等,来验证硫丹的体内雌激素样作用。

In this research, two novel compounds in which alkylenedithiomethylene Malonic acid act as the main coordination agents and the compounds containing N atom (such as pyridine, Phenanthroline Ethanediamine and 4,4'-Bipyridinyl) act as the associating coordination agents have been synthesized by the means of solution and solid-liquid diffusing reactions. 9 coordination complexes and polymers have been designed and synthesized in which the transition metals Cu and Zn acted as the centre ions. These compounds have been characterized by X-ray single crystal diffraction analysis, and some properties of them have been tested and analyzed.

本论文设计合成了两种结构新颖的含有二硫缩烯酮结构的丙二酸类化合物,以此为主要配体,以含氮化合物(吡啶、邻菲罗啉、乙二胺和4,4'-联吡啶)为辅助配体,采用常规溶液合成和固-液相扩散等方法,设计合成了9个过渡金属Cu和Zn离子配合物和配位聚合物,采用单晶X-射线衍射等技术对晶体结构表征,并对其部分性质进行了测试和分析。

In this thesis, the advantages and disadvantages of potentiodynamic polarization curve, electrochemical impedance spectroscope and coulostatic method for studying corrosion inhibitors in acidic mediums were compared. And then the effect of three popular acid corrosion inhibitors such as thiourea, dodecylamine and propargyl alcohol on the corrosion inhibition behaviors of Q235 steel in acidic solutions were investigated by these techniques. The anodic desorption behavior and extreme value phenomenon of concentration were surveyed thoroughly as well.

本文讨论了动电位极化曲线、电化学阻抗谱和恒电量测量方法在酸性介质缓蚀剂研究中的优势和不足,在此基础上,研究了硫脲、十二胺和丙炔醇等三种常见酸性介质缓蚀剂对Q235钢在酸性溶液中的缓蚀行为和机理,并深入探讨了缓蚀剂的阳极脱附和浓度极值现象。

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In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是,在否定句或疑问句里,这种带有"do"的方法表达的效果却没有什么强调的意思。

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