和硫

Under the condition that coking process and ratio of coal,rank of coal were in a relative stable condition,qualitative analysis was done to the relationship among ammonia yield and residual ammonia exhausted gas entering into saturator or not,gas desulfurization unit location,the primary cooling way,blending moisture,gas collection temperature and so on,the various factors affecting degree to the yield of ammonia were concluded,in order to organize production scientifically and rationally,and provide a reference to the same industry to solve the problem of the ammonia output fluctuation.

通过对焦化厂硫铵工序的长期跟踪研究，明确了造成硫铵产率波动的主要因素，在焦化流程和配煤比、煤种相对稳定的情况下，对硫铵产率与剩余氨水蒸氨尾气是否进入饱和器、煤气脱硫装置位置、煤气初冷方式、配煤水分、煤气集合温度等因素之间的关系进行了定性分析，得出了以上各种因素对硫铵产率的影响程度的结论，以便科学合理地安排硫铵的生产计划，并为同行业解决硫铵产量波动的问题提供参考。

The dissipation rate constants of malathion and methyl parathion with a concentration of 3mg/L and ethion, dicofol and cyhalothrin with a concentration of 0.5mg/L in 2000ml of 55-60g canna planted water sulution were respectively increased by 77. 66％, 117. 44％, 64. 80％, 38. 11％ and 15. 35％ compared to those in unplanted water solutions.

与不种植植物的对照相比，50-60g美人蕉对2000ml分别含有3mg/L的马拉硫磷、甲基对硫磷及0.5mg/L乙硫磷、三氯杀螨醇和三氟氯氰菊酯培养液中的马拉硫磷、甲基对硫磷、乙硫磷、三氯杀螨醇和三氟氯氰菊酯的消解速率依次分别提高了77.66％、117.44％、64.80％、38.11％和15.35％。

In this paper, a series of 4,5-dithiacrown ether annulated 1,3-dithiole-2-thiones 8a~8d were prepared via condensing 4,5-bis-1,3-dithiole-2-thione (7) with 1,ω-dimercapto polyglycol derivatives in high dilution. The obvious template effect was found during the synthesis of 8c-8d.

在高度稀释条件下，经4，5-二溴甲基-1，3-二硫杂环戊烯-2-硫酮(7)和多缩乙二醇的1，ω-二巯基衍生物的缩合反应，方便地合成了4，5-位带二硫杂冠醚残基的2-硫代-1，3-二硫杂环戊烯的衍生物8a~8d，中间体硫杂冠醚8c~8d的合成中有明显的&模板效应&。

In this paper, a series of 4,5-dithiacrown ether annulated 1,3-dithiole-2-thiones 8a~8d were prepared via condensing 4,5-bis-1,3-dithiole-2-thione (7) with 1,ω-dimercapto polyglycol derivatives in high dilution. The obvious template effect was found during the synthesis of 8c-8d.

在高度稀释条件下，经4，5-二溴甲基-1，3-二硫杂环戊烯-2-硫酮(7)和多缩乙二醇的1，ω-二巰基衍生物的缩合反应，方便地合成了4，5-位带二硫杂冠醚残基的2-硫代-1，3-二硫杂环戊烯的衍生物8a~8d，中间体硫杂冠醚8c~8d的合成中有明显的&模板效应&。

Ergothioneine is a kind of precious amino acid, and it is also a natural antioxidant. It plays an important role to prevent the oxidative damage in organism. Ergothioneine cannot be biosynthesized in humans, only can be absorbed from the diet. In recently the research discovered the high content of ergothioneine in the mushroom. Content of ergothioneine of Pleurotus eryngii is the highest from 28 kinds of mushrooms, therefore the research untilized P. eryngii to make the products of P. eryngii-fermented adlay and P. eryngii-fermented buckwheat which content high ergothioneine. Also, we analyzed their proximate composition, nutritional components, taste and physiologically active components, antioxidant properties and evaluation of anti-imflammatory effect.

中文摘要麦角硫因为一种稀有的胺基酸，也是天然的抗氧化剂，其在生物体内对氧化压力伤害之预防扮演著重要角色，麦角硫因不能在动物体内合成，仅能由食物中摄取，近年来发现在菇类中含有高含量的麦角硫因，从28种食药用菇类中筛选出麦角硫因含量较高的菌种，以杏鲍菇子实体最高(1521.6 mg/g dw)，因此本论文以杏鲍菇为媒介，利用固态发酵方式，制备出高麦角硫因之杏鲍菇薏仁和杏鲍菇荞麦，并针对薏仁、杏鲍菇薏仁、荞麦、杏鲍菇荞麦和杏鲍菇菌丝体，进行一般成分、营养、物性、呈味、生理活性物质、抗氧化性质之分析及抗发炎反应之评估。

Glucosinolates and myrosinase are present in the vacuoles and in the de finite protosome in intact cell and tissues respectively. but when tissues and c ells are damaged, myrosinase will release and hydrolyze glucosinolates to genera te degraded products, such as isothiocyanates and so on.

在完整的植物中，硫代葡萄糖苷存在于细胞的液泡中，葡萄糖硫苷酶存在于特定的蛋白体中，两者相互分离，但当组织和细胞受到损伤时，葡萄糖硫苷酶就会被释放出来，葡萄糖硫苷酶将硫代葡萄糖苷水解，产生异硫代氰酸盐等降解产物。

In the first part, five new 4-acyl pyrazolone 4-ethyl-thiosemicarbazones compounds: 1-Phenyl-3-methyl-4-(4-bromo)benzal-pyrazol-5-one N(4)-ethyl-thiosemicarbazone (PM4Br BP-ETSC), 1-Phenyl-3-methyl-4-(4-methyl)benzal-pyrazol-5-one N(4)-ethyl-thiosemicarbaz -one (PM4MBP-ETSC), 1-Phenyl-3-methyl-4-benzal-pyrazol-5-one N(4)-ethyl-thiosemicarba -zone, 1,3-diphenyl-4-benzal-pyrazol-5-one N(4)-ethyl-thiosemicarbazone and 1-Phenyl-3-methyl-4-phenylacetyl-pyrazol-5-one N(4)-ethyl-thiosemi -carbazone have been synthesized and characterized by elemental analyses, IR, 1H NMR spectra and single-crystal XRD.

第一部分合成了五个4-酰基吡唑啉酮缩4-乙基-氨基硫脲化合物：1-苯基-3-甲基-4-（4-溴）苯甲酰基-5-吡唑啉酮缩4-乙基-氨基硫脲(PM4BrBP-ETSC)，1-苯基-3-甲基-4-(4-甲基)苯甲酰基-5-吡唑啉酮缩4-乙基-氨基硫脲(PM4MBP-ETSC)，1-苯基-3-甲基-4-苯甲酰基-5-吡唑啉酮缩4-乙基-氨基硫脲，1，3-二苯基-4-苯甲酰基-5-吡唑啉酮缩4-乙基-氨基硫脲和1-苯基-3-甲基-4-苯乙酰基-5-吡唑啉酮缩4-乙基-氨基硫脲，其中前四个具有光致变色性质。

It is necessary to carry out a thorough study on pest control technology with DMDS, with an expectation of obtaining a new fumigant of methyl bromide alternative.2. Investigation of the toxicity of fumigation on adult and mixed stages of the three most tolerant insect species -- Sitophilus oryzae, Rhyzopertha dominica and Tribolium castaneum -- under a range of EtF、DMS and DMDS doses in a Flow-through Fumigation System shows that the FTFS procedure offers a constant concentration of fumigant with low CO2 concentrations and ensures that the fumigant toxicity is effectively not compromised by CO2. In comparison with chamber fumigation method, the toxicity data of EtF、DMS and DMDS obtained from this experiment is more accurate by using FTFS.

主要研究结果如下：1、甲酸乙酯和二甲基二硫对仓储害虫具有良好的控制作用，应加快甲酸乙酯替代溴甲烷防治仓储害虫开发应用，同时，二甲基二硫是很有潜力的仓储害虫防治熏蒸剂，要深入进行二甲基二硫控制有害生物的技术研究，以期获得新的溴甲烷替代熏蒸剂。2、利用循环熏蒸系统测定了甲酸乙酯、二甲基二硫和甲硫醚对米象Sitophilus oryzaeL。

By the bio-assay directed fractionation of the volative constituents.dimethyl disulfide,allyl methyl trisulfide,allyl methyl sulfide and diallyl disulfide were found to increase the beating rate and beating amplitude in a standard medium,but the compund 2-pentanone without sulfide did not affect either of them.

从具有生物活性的挥发性提取物中分离得到的二甲基二硫、烯丙基甲基三硫、烯丙基甲基硫醚和二烯丙基二硫对培养心肌细胞心率和振幅均有不同程度的增强作用，而不含硫的2-戊酮则没有作用。

According to the research of Pb isotopic, the metallogenetic material mainly originated from the Permian basalts; the study of sulfur isotopic find that the sulfur of the basalt-type copper deposits and carbonaceous sedimentary interlayers-type copper deposits originated from both Permian basalts and evaporate of sedimentary section, S in bauxitic mudstone-type copper deposits originated from evaporate of sedimentary layers.

研究区三种类型铜矿的铅同位素示踪研究，成矿物质主要来自于邻近的二叠纪玄武岩；硫同位素研究结果显示，玄武岩型铜矿和含碳沉积岩夹层型铜矿中的硫有两种来源：二叠纪玄武岩和蒸发岩中的硫；而铝土质泥岩铜矿中的硫主要来源于沉积地层中蒸发岩的硫。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。